CN1115196C - 双金属氰化物催化剂的快速活化方法 - Google Patents

双金属氰化物催化剂的快速活化方法 Download PDF

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Publication number
CN1115196C
CN1115196C CN98805078A CN98805078A CN1115196C CN 1115196 C CN1115196 C CN 1115196C CN 98805078 A CN98805078 A CN 98805078A CN 98805078 A CN98805078 A CN 98805078A CN 1115196 C CN1115196 C CN 1115196C
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CN
China
Prior art keywords
catalyst
stripping
vacuum
mixture
feedstock
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
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CN98805078A
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English (en)
Chinese (zh)
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CN1259887A (zh
Inventor
J·E·哈耶斯
L·J·朗斯多尔夫
B·H·伊萨尔斯
F·J·阿梅利尼
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Koth A Ltd By Share Ltd
Link Chemical Technologies
Bayer Antwerpen NV
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Arco Chemical Technology LP
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Publication of CN1259887A publication Critical patent/CN1259887A/zh
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/24—Nitrogen compounds
    • B01J27/26—Cyanides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645—Metals or compounds thereof, e.g. salts
    • C08G65/2663—Metal cyanide catalysts, i.e. DMC's
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2696—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the process or apparatus used

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Toxicology (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Polyethers (AREA)
  • Polyurethanes Or Polyureas (AREA)
CN98805078A 1997-05-16 1998-04-09 双金属氰化物催化剂的快速活化方法 Expired - Lifetime CN1115196C (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US08/857,998 US5844070A (en) 1997-05-16 1997-05-16 Process for rapid activation of double metal cyanide catalysts
US08/857998 1997-05-16
US08/857,998 1997-05-16

Publications (2)

Publication Number Publication Date
CN1259887A CN1259887A (zh) 2000-07-12
CN1115196C true CN1115196C (zh) 2003-07-23

Family

ID=25327204

Family Applications (1)

Application Number Title Priority Date Filing Date
CN98805078A Expired - Lifetime CN1115196C (zh) 1997-05-16 1998-04-09 双金属氰化物催化剂的快速活化方法

Country Status (13)

Country Link
US (1) US5844070A (https=)
EP (1) EP0981407B2 (https=)
JP (1) JP4368427B2 (https=)
KR (1) KR100537910B1 (https=)
CN (1) CN1115196C (https=)
AU (1) AU7642798A (https=)
BR (1) BR9809835A (https=)
CA (1) CA2287247C (https=)
DE (1) DE69812348T3 (https=)
ES (1) ES2195341T5 (https=)
ID (1) ID22969A (https=)
TW (1) TW530070B (https=)
WO (1) WO1998052689A1 (https=)

Families Citing this family (56)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19918726C2 (de) * 1999-04-24 2002-04-11 Bayer Ag Offenzellige Polyurethanhartschaumstoffe
AU5920800A (en) * 1999-07-09 2001-01-30 Dow Chemical Company, The Method for fractionating poly(ethylene oxide) formed using metallic cyanide catalyst
DE19956119A1 (de) * 1999-11-22 2001-06-07 Bayer Ag Verfahren zur Herstellung von Polyetherpolyolen
US6642171B2 (en) 2000-04-28 2003-11-04 Synuthane International, Inc. Double metal cyanide catalysts containing polyglycol ether complexing agents
DE10137628A1 (de) * 2001-08-03 2003-02-27 Basf Ag Verfahren zur Herstellung von Polyurethan-Weichschaumstoffen
DE10205086A1 (de) * 2002-02-07 2003-08-21 Basf Ag Verfahren zur Aktivierung von Doppelmetallcyanid-Verbindungen
ES2199666B1 (es) 2002-02-25 2005-06-01 Repsol Quimica, S.A. Procedimiento de produccion de polioleteres.
US6835801B2 (en) * 2002-07-19 2004-12-28 Bayer Antwerp, N.V. Activated starter mixtures and the processes related thereto
US7001634B2 (en) * 2002-11-07 2006-02-21 Bayer Materialscience Llc Process for suppressing the foaming of an aqueous system
US6806348B2 (en) 2003-02-11 2004-10-19 Basf Corporation Process for removing and regenerating a double metal cyanide (DMC) catalyst from a polymer polyol
US6713599B1 (en) 2003-03-31 2004-03-30 Basf Corporation Formation of polymer polyols with a narrow polydispersity using double metal cyanide (DMC) catalysts
US7223890B2 (en) * 2003-10-10 2007-05-29 Bayer Materialscience Llc Isocyanate reactive mixture and process for preparing same
EP1756198B2 (en) * 2004-06-09 2011-02-23 Shell Internationale Research Maatschappij B.V. Process of preparing odour-lean polyether polyol
JP2007284586A (ja) * 2006-04-18 2007-11-01 Asahi Glass Co Ltd ポリエーテルモノオールの製造方法
DE102006024025A1 (de) 2006-05-23 2007-11-29 Bayer Materialscience Ag Verfahren zur Herstellung von Polyetherpolyolen
DE102007057145A1 (de) 2007-11-28 2009-06-04 Evonik Goldschmidt Gmbh Verfahren zur Herstellung von Polyetheralkoholen mit DMC-Katalysatoren unter Verwendung von SiH-Gruppen tragenden Verbindungen als Additive
DE102007057146A1 (de) * 2007-11-28 2009-06-04 Evonik Goldschmidt Gmbh Verfahren zur Herstellung von Polyetheralkoholen mit DMC-Katalysatoren unter Verwendung von speziellen Additiven mit aromatischer Hydroxy-Funktionalisierung
DE102007057147A1 (de) 2007-11-28 2009-06-04 Evonik Goldschmidt Gmbh Verfahren zur Alkoxylierung mit DMC-Katalysatoren im Schlaufenreaktor mit Strahlsauger
JP5624324B2 (ja) * 2008-01-25 2014-11-12 株式会社カネカ ポリアルキレンオキシドの製造方法
EP2238195B1 (de) 2008-01-29 2015-03-18 Basf Se Verfahren zur herstellung von polyetheralkoholen
DE102008000360A1 (de) 2008-02-21 2009-08-27 Evonik Goldschmidt Gmbh Neue Alkoxysilylgruppen tragende Polyetheralkohole durch Alkoxylierung epoxidfunktioneller Alkoxysilane an Doppelmetallcyanid (DMC)-Katalysatoren, sowie Verfahren zu deren Herstellung
DE102008000903A1 (de) 2008-04-01 2009-10-08 Evonik Goldschmidt Gmbh Neue Organosiloxangruppen tragende Polyetheralkohole durch Alkoxylierung epoxidfunktioneller (Poly)Organosiloxane an Doppelmetallcyanid (DMC)-Katalysatoren, sowie Verfahren zu deren Herstellung
DE102008002713A1 (de) 2008-06-27 2009-12-31 Evonik Goldschmidt Gmbh Neue Polyethersiloxane enthaltende Alkoxylierungsprodukte durch direkte Alkoxylierung organomodifizierter alpha, omega-Dihydroxysiloxane an Doppelmetallcyanid (DMC)-Katalysatoren, sowie Verfahren zu deren Herstellung
CN101684184A (zh) 2008-09-27 2010-03-31 巴斯夫欧洲公司 可通过使用可再生的原料获得的聚氨酯鞋底
DE102008043245A1 (de) 2008-10-29 2010-05-06 Evonik Goldschmidt Gmbh Siliconpolyether-Copolymersysteme sowie Verfahren zu deren Herstellung durch Alkoxylierungsreaktion
DE102009002371A1 (de) 2009-04-15 2010-10-21 Evonik Goldschmidt Gmbh Verfahren zur Herstellung von geruchlosen Polyetheralkoholen mittels DMC-Katalysatoren und deren Verwendung in kosmetischen und/oder dermatologischen Zubereitungen
CN102498145B (zh) 2009-07-10 2013-10-23 巴斯夫欧洲公司 基于可再生资源生产多元醇的方法
KR20120069681A (ko) * 2009-09-17 2012-06-28 아사히 가라스 가부시키가이샤 폴리에테르류의 제조 방법
KR20120128130A (ko) 2010-01-20 2012-11-26 바이엘 인텔렉쳐 프로퍼티 게엠베하 폴리에테르 카르보네이트 폴리올의 제조를 위한 이중 금속 시아나이드 촉매의 활성화 방법
US9115246B2 (en) 2010-04-30 2015-08-25 Basf Se Polyether polyols, process for preparing polyether polyols and their use for producing polyurethanes
MX2012012596A (es) 2010-04-30 2013-05-06 Basf Se Polioles de polieter, proceso para preparar polioles de polieter y su uso para producir poliuretanos.
DE102010038768A1 (de) 2010-08-02 2012-02-02 Evonik Goldschmidt Gmbh Modifizierte Alkoxylierungsprodukte mit mindestens einer nicht-terminalen Alkoxysilylgruppe mit erhöhter Lagerstabilität und erhöhter Dehnbarkeit der unter deren Verwendung hergestellten Polymere
DE102010038774A1 (de) 2010-08-02 2012-02-02 Evonik Goldschmidt Gmbh Modifizierte Alkoxylierungsprodukte, die zumindest eine nicht-terminale Alkoxysilylgruppe aufweisen, mit erhöhter Lagerstabilität und erhöhter Dehnbarkeit der unter deren Verwendung hergestellten Polymere
SG191340A1 (en) 2010-12-27 2013-08-30 Dow Global Technologies Llc Alkylene oxide polymerization using a double metal cyanide catalyst complex and a magnesium, group 3-group 15 metal or lanthanide series metal compound
ES2537891T3 (es) * 2011-06-30 2015-06-15 Bayer Intellectual Property Gmbh Procedimiento para la preparación de polieterpolioles de peso molecular alto
EP2548906A1 (de) * 2011-07-18 2013-01-23 Bayer MaterialScience AG Verfahren zur Aktivierung von Doppelmetallcyanidkatalysatoren zur Herstellung von Polyetherpolyolen
EP2548905A1 (de) * 2011-07-18 2013-01-23 Bayer MaterialScience AG Verfahren zur Aktivierung von Doppelmetallcyanidkatalysatoren zur Herstellung von Polyetherpolyolen
EP2548908A1 (de) 2011-07-18 2013-01-23 Bayer MaterialScience AG Verfahren zur Herstellung von Polyetherpolyolen
EP2548907A1 (de) * 2011-07-18 2013-01-23 Bayer MaterialScience AG Verfahren zur Herstellung von Polyetherpolyolen
DE102012203737A1 (de) 2012-03-09 2013-09-12 Evonik Goldschmidt Gmbh Modifizierte Alkoxylierungsprodukte, die zumindest eine nicht-terminale Alkoxysilylgruppe aufweisen und mehrere Urethangruppen enthalten und deren Verwendung
CN103871823A (zh) * 2012-12-12 2014-06-18 中国科学院大连化学物理研究所 一种掺杂有机溶剂的膜进样离子迁移谱仪
DE102013206883A1 (de) 2013-04-17 2014-10-23 Evonik Industries Ag Alkoxysilylhaltige Klebdichtstoffe mit intrinsisch reduzierter Viskosität
RU2532429C1 (ru) * 2013-07-25 2014-11-10 Общество с ограниченной ответственностью Научно-производственное предприятие "Макромер" Способ получения простых полиэфирополиолов
DE102013216751A1 (de) 2013-08-23 2015-02-26 Evonik Industries Ag Modifizierte Alkoxylierungsprodukte, die Alkoxysilylgruppen aufweisen und Urethangruppen enthalten und deren Verwendung
DE102013224708A1 (de) 2013-12-03 2015-06-03 Evonik Industries Ag Alkoxysilylhaltige Klebdichtstoffe mit intrinsisch reduzierter Viskosität
DE102014209408A1 (de) 2014-05-19 2015-11-19 Evonik Degussa Gmbh Ethoxylatherstellung unter Verwendung hoch aktiver Doppelmetallcyanid-Katalysatoren
DE102014217790A1 (de) 2014-09-05 2016-03-10 Evonik Degussa Gmbh Verfahren zur Herstellung von hydrosilylierbaren Eugenol-Polyethern und Eugenol-Polyethersiloxanen sowie deren Verwendung
DK3050910T3 (en) 2015-01-28 2017-02-27 Evonik Degussa Gmbh MODIFIED ALCOXYLING PRODUCTS, WHICH HAVE AT LEAST A NON-TERMINAL ALCOXYSILYL GROUP, WITH INCREASED STOCK STABILITY AND IMPROVED EXTENSION, AND THE POLYMES USED THEREOF
EP3106221A1 (en) 2015-06-15 2016-12-21 Universität Hamburg Process for preparing double metal cyanide catalysts and their use in polymerization reactions
DK3202816T3 (en) 2016-02-04 2019-01-21 Evonik Degussa Gmbh ALCOXYSILYLY ADHESIVE TENSIONS WITH IMPROVED TIRE STRENGTH
JP6931362B2 (ja) * 2016-05-13 2021-09-01 コベストロ、ドイチュラント、アクチエンゲゼルシャフトＣｏｖｅｓｔｒｏ Ｄｅｕｔｓｃｈｌａｎｄ Ａｇ ポリオキシアルキレンポリオールの製造方法
CN113348191B (zh) * 2019-01-31 2023-06-30 陶氏环球技术有限责任公司 无雾聚氨酯制剂
CN113087892B (zh) * 2019-12-23 2022-07-12 万华化学集团股份有限公司 一种制备聚醚多元醇的方法和装置
CN112094404A (zh) * 2020-09-30 2020-12-18 浙江皇马科技股份有限公司 一种低钾钠含量的烯丙醇聚醚制备工艺
JP7681766B1 (ja) * 2024-07-05 2025-05-22 Ａｇｃ株式会社 組成物
WO2026077748A1 (de) 2024-10-09 2026-04-16 Evonik Operations Gmbh Dispergiermittel auf basis von amidierten polyaminen und/oder polyiminen mit carbonsäureesterfunktionellen polyethern

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3278457A (en) * 1963-02-14 1966-10-11 Gen Tire & Rubber Co Method of making a polyether using a double metal cyanide complex compound
US3427256A (en) † 1963-02-14 1969-02-11 Gen Tire & Rubber Co Double metal cyanide complex compounds
US3278459A (en) * 1963-02-14 1966-10-11 Gen Tire & Rubber Co Method of making a polyether using a double metal cyanide complex compound
US3829505A (en) * 1970-02-24 1974-08-13 Gen Tire & Rubber Co Polyethers and method for making the same
US3941849A (en) * 1972-07-07 1976-03-02 The General Tire & Rubber Company Polyethers and method for making the same
AU552988B2 (en) * 1982-03-31 1986-06-26 Shell Internationale Research Maatschappij B.V. Polymerizing epoxides and catalyst suspensions for this
AU551979B2 (en) † 1982-03-31 1986-05-15 Shell Internationale Research Maatschappij B.V. Epoxy polymerisation catalysts
US5110970A (en) * 1991-03-29 1992-05-05 Union Carbide Chemicals & Plastics Technology Corporation Process for the manufacture of certain new silicone polyether copolymers for polyurethane foam manufacture
US5158922A (en) * 1992-02-04 1992-10-27 Arco Chemical Technology, L.P. Process for preparing metal cyanide complex catalyst
US5470813A (en) * 1993-11-23 1995-11-28 Arco Chemical Technology, L.P. Double metal cyanide complex catalysts
US5426081A (en) * 1993-12-23 1995-06-20 Arco Chemical Technology, L.P. Polyurethane foam-supported double metal cyanide catalysts for polyol synthesis
US5416241A (en) * 1994-01-27 1995-05-16 Arco Chemical Technology, L.P. Method for purifying polyether polyols made with double metal cyanide catalysts
US5482908A (en) * 1994-09-08 1996-01-09 Arco Chemical Technology, L.P. Highly active double metal cyanide catalysts
US5489617A (en) * 1994-11-17 1996-02-06 Osi Specialties, Inc. High viscosity surfactants for the manufacture of polyurethane foams
US5525640A (en) * 1995-09-13 1996-06-11 Osi Specialties, Inc. Silicone surfactants for use in inert gas blown polyurethane foams

Also Published As

Publication number Publication date
ES2195341T3 (es) 2003-12-01
CA2287247C (en) 2007-08-21
CA2287247A1 (en) 1998-11-26
ID22969A (id) 1999-12-23
DE69812348T3 (de) 2007-03-15
WO1998052689A1 (en) 1998-11-26
BR9809835A (pt) 2000-06-20
JP4368427B2 (ja) 2009-11-18
EP0981407B2 (en) 2006-10-11
DE69812348T2 (de) 2003-11-06
TW530070B (en) 2003-05-01
EP0981407A1 (en) 2000-03-01
DE69812348D1 (de) 2003-04-24
ES2195341T5 (es) 2007-05-16
KR100537910B1 (ko) 2005-12-21
KR20010012446A (ko) 2001-02-15
CN1259887A (zh) 2000-07-12
JP2001525878A (ja) 2001-12-11
AU7642798A (en) 1998-12-11
US5844070A (en) 1998-12-01
EP0981407B1 (en) 2003-03-19

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