CN1093700A - 2-烷基-6-甲基-n-(1'-甲氧基-2'-丙基)-苯胺和它们的n-氯乙酰苯胺的制备方法 - Google Patents
2-烷基-6-甲基-n-(1'-甲氧基-2'-丙基)-苯胺和它们的n-氯乙酰苯胺的制备方法 Download PDFInfo
- Publication number
- CN1093700A CN1093700A CN93121226A CN93121226A CN1093700A CN 1093700 A CN1093700 A CN 1093700A CN 93121226 A CN93121226 A CN 93121226A CN 93121226 A CN93121226 A CN 93121226A CN 1093700 A CN1093700 A CN 1093700A
- Authority
- CN
- China
- Prior art keywords
- reaction
- methyl
- catalyzer
- hydrogenation
- aniline
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
- C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/24—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds
- C07C209/26—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds by reduction with hydrogen
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C07C213/02—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reactions involving the formation of amino groups from compounds containing hydroxy groups or etherified or esterified hydroxy groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Description
Claims (34)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US99803092A | 1992-12-29 | 1992-12-29 | |
US07/998,030 | 1992-12-29 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1093700A true CN1093700A (zh) | 1994-10-19 |
CN1039994C CN1039994C (zh) | 1998-09-30 |
Family
ID=25544671
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN93121226A Expired - Lifetime CN1039994C (zh) | 1992-12-29 | 1993-12-27 | 2-烷基-6-甲基-n-(1'-甲氧基-2'-丙基)-苯胺和它们的n-氯乙酰苯胺的制备方法 |
Country Status (34)
Country | Link |
---|---|
US (1) | US5430188A (zh) |
EP (1) | EP0605363B1 (zh) |
JP (1) | JP3521285B2 (zh) |
KR (1) | KR100271775B1 (zh) |
CN (1) | CN1039994C (zh) |
AT (1) | ATE139223T1 (zh) |
AU (1) | AU667989B2 (zh) |
BG (1) | BG61481B1 (zh) |
BR (1) | BR9305272A (zh) |
CA (1) | CA2112416C (zh) |
CZ (1) | CZ286376B6 (zh) |
DE (1) | DE69303155T2 (zh) |
DK (1) | DK0605363T3 (zh) |
EE (1) | EE03069B1 (zh) |
FI (1) | FI113639B (zh) |
GE (1) | GEP19991732B (zh) |
GR (1) | GR3020221T3 (zh) |
HR (1) | HRP931521B1 (zh) |
HU (2) | HU216027B (zh) |
IL (1) | IL108204A (zh) |
LT (1) | LT3260B (zh) |
LV (1) | LV10859B (zh) |
MX (1) | MX9307814A (zh) |
MY (1) | MY109091A (zh) |
NO (2) | NO180536C (zh) |
NZ (1) | NZ250549A (zh) |
PH (1) | PH29918A (zh) |
PL (1) | PL177669B1 (zh) |
RO (2) | RO117018B1 (zh) |
RU (1) | RU2127253C1 (zh) |
SI (1) | SI9300692B (zh) |
SK (1) | SK280155B6 (zh) |
TR (1) | TR27179A (zh) |
ZA (1) | ZA939720B (zh) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102887832A (zh) * | 2012-09-29 | 2013-01-23 | 西安近代化学研究所 | 一种水相反应合成大位阻氯乙酰胺化合物的方法 |
CN104445068A (zh) * | 2014-11-21 | 2015-03-25 | 山东侨昌化学有限公司 | 一种异丙甲草胺生产过程中副产氢气的回收方法 |
CN115784909A (zh) * | 2022-11-30 | 2023-03-14 | 浙江工业大学 | 一种合成2-乙基-n-(2-甲氧基-1-甲基乙基)-6-甲基苯胺的方法 |
Families Citing this family (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
HRP960295A2 (en) * | 1995-07-06 | 1997-08-31 | Ciba Geigy Ag | Process for the hydrogenation of imines in the presence of immobilized iridium-diphosphine catalysts |
HRP960302A2 (en) * | 1995-07-26 | 1998-04-30 | Ciba Geigy Ag | Process for the hydrogenation of imines |
US6140538A (en) | 1998-05-18 | 2000-10-31 | Flexsys America L.P. | Process for preparing 4-aminodiphenylamines |
GB2372716B (en) | 1999-12-17 | 2003-07-16 | Warner Lambert Res & Dev Ie | An apparatus for removing pyrophoric catalyst |
BRPI0520066A2 (pt) * | 2005-03-28 | 2009-04-14 | Albemarle Corp | diimina aromática, diamina aromática secundária, processo para formar uma diamina secundária, processo para formar uma diimina, formulação, processo para produzir um poliuretano |
US8076518B2 (en) | 2005-03-28 | 2011-12-13 | Albemarle Corporation | Chain extenders |
US7964695B2 (en) * | 2005-03-28 | 2011-06-21 | Albemarle Corporation | Chain extenders |
EA200870136A1 (ru) * | 2005-12-30 | 2009-12-30 | Альбемарл Корпорейшн | Диамины, имеющие уменьшенную окраску |
US8143365B2 (en) * | 2007-01-10 | 2012-03-27 | Albemarle Corporation | Formulations for reaction injection molding and for spray systems |
RU2476422C2 (ru) * | 2008-04-17 | 2013-02-27 | Юнайтед Фосфорус Лимитед | Гидрирование иминов |
EP2892877B1 (en) | 2012-09-06 | 2017-06-21 | Council of Scientific and Industrial Research | Process for the preparation of (s)-2-ethyl-n-(1-methoxypropan -2-yl)-6-methyl aniline |
CN104803875A (zh) * | 2015-03-27 | 2015-07-29 | 江苏长青农化南通有限公司 | 一种s-异丙甲草胺的合成方法 |
CN105461580B (zh) * | 2015-11-12 | 2018-04-20 | 上虞颖泰精细化工有限公司 | 一种异丙甲草胺的合成方法 |
CN109280012A (zh) * | 2017-07-19 | 2019-01-29 | 山东侨昌化学有限公司 | 一种无溶剂合成异丙甲草胺中间体2-乙基-6-甲基-n-(1’-甲氧基-2’-丙基)苯胺的方法 |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4200451A (en) * | 1972-06-06 | 1980-04-29 | Ciba-Geigy Corporation | Plant growth regulating agent |
US3937730A (en) | 1972-06-06 | 1976-02-10 | Ciba-Geigy Corporation | Plant growth regulating agent |
US3929855A (en) * | 1974-10-10 | 1975-12-30 | Monsanto Co | N-1,3-Dimethylbutyl-N{40 -1,4-dimethylpentyl-p-phenylenediamine antiozonants |
US4463191A (en) * | 1983-09-26 | 1984-07-31 | The Goodyear Tire & Rubber Company | Process for the reductive alkylation of aromatic nitro-containing compounds with ketones or aldehydes |
CS270548B1 (en) | 1989-01-20 | 1990-07-12 | Beska Emanuel | Method of 2-ethyl-6-methyl-n-/1 -methoxy-2-propyl/aniline preparation |
-
1993
- 1993-12-02 MY MYPI93002557A patent/MY109091A/en unknown
- 1993-12-10 MX MX9307814A patent/MX9307814A/es unknown
- 1993-12-10 LT LTIP1586A patent/LT3260B/lt not_active IP Right Cessation
- 1993-12-15 US US08/168,034 patent/US5430188A/en not_active Expired - Lifetime
- 1993-12-17 GE GEAP19931688D patent/GEP19991732B/en unknown
- 1993-12-21 DK DK93810895.8T patent/DK0605363T3/da active
- 1993-12-21 DE DE69303155T patent/DE69303155T2/de not_active Expired - Lifetime
- 1993-12-21 EP EP93810895A patent/EP0605363B1/en not_active Expired - Lifetime
- 1993-12-21 AT AT93810895T patent/ATE139223T1/de not_active IP Right Cessation
- 1993-12-22 NZ NZ250549A patent/NZ250549A/en not_active IP Right Cessation
- 1993-12-23 RU RU93056851A patent/RU2127253C1/ru active
- 1993-12-24 AU AU52681/93A patent/AU667989B2/en not_active Expired
- 1993-12-24 KR KR1019930030083A patent/KR100271775B1/ko not_active IP Right Cessation
- 1993-12-24 CA CA002112416A patent/CA2112416C/en not_active Expired - Lifetime
- 1993-12-27 CN CN93121226A patent/CN1039994C/zh not_active Expired - Lifetime
- 1993-12-27 RO RO93-01795A patent/RO117018B1/ro unknown
- 1993-12-27 SK SK1488-93A patent/SK280155B6/sk not_active IP Right Cessation
- 1993-12-27 FI FI935886A patent/FI113639B/fi not_active IP Right Cessation
- 1993-12-27 CZ CZ19932902A patent/CZ286376B6/cs not_active IP Right Cessation
- 1993-12-27 PL PL93301650A patent/PL177669B1/pl unknown
- 1993-12-27 RO ROA200100609A patent/RO117320B1/ro unknown
- 1993-12-28 BR BR9305272A patent/BR9305272A/pt not_active IP Right Cessation
- 1993-12-28 HU HUP9603419A patent/HU216027B/hu unknown
- 1993-12-28 TR TR01225/93A patent/TR27179A/xx unknown
- 1993-12-28 JP JP35319893A patent/JP3521285B2/ja not_active Expired - Fee Related
- 1993-12-28 PH PH47562A patent/PH29918A/en unknown
- 1993-12-28 ZA ZA939720A patent/ZA939720B/xx unknown
- 1993-12-28 HR HR07/998,030A patent/HRP931521B1/xx not_active IP Right Cessation
- 1993-12-28 IL IL108204A patent/IL108204A/xx not_active IP Right Cessation
- 1993-12-28 NO NO934861A patent/NO180536C/no not_active IP Right Cessation
- 1993-12-28 BG BG98337A patent/BG61481B1/bg unknown
- 1993-12-28 HU HU9303775A patent/HU213259B/hu unknown
- 1993-12-28 LV LVP-93-1381A patent/LV10859B/en unknown
- 1993-12-29 SI SI9300692A patent/SI9300692B/sl unknown
-
1994
- 1994-11-17 EE EE9400329A patent/EE03069B1/xx unknown
-
1996
- 1996-06-13 GR GR960401462T patent/GR3020221T3/el unknown
- 1996-07-15 NO NO962959A patent/NO301418B1/no not_active IP Right Cessation
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102887832A (zh) * | 2012-09-29 | 2013-01-23 | 西安近代化学研究所 | 一种水相反应合成大位阻氯乙酰胺化合物的方法 |
CN102887832B (zh) * | 2012-09-29 | 2014-07-16 | 西安近代化学研究所 | 一种水相反应合成大位阻氯乙酰胺化合物的方法 |
CN104445068A (zh) * | 2014-11-21 | 2015-03-25 | 山东侨昌化学有限公司 | 一种异丙甲草胺生产过程中副产氢气的回收方法 |
CN104445068B (zh) * | 2014-11-21 | 2016-09-28 | 山东侨昌化学有限公司 | 一种异丙甲草胺生产过程中副产氢气的回收方法 |
CN115784909A (zh) * | 2022-11-30 | 2023-03-14 | 浙江工业大学 | 一种合成2-乙基-n-(2-甲氧基-1-甲基乙基)-6-甲基苯胺的方法 |
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Legal Events
Date | Code | Title | Description |
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C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C53 | Correction of patent of invention or patent application | ||
COR | Change of bibliographic data |
Free format text: CORRECT: APPLICANT; FROM: CIBA-GEIGY AG TO: NOVANNIS COMPANY |
|
CP01 | Change in the name or title of a patent holder |
Address after: Basel Applicant after: Novartis AG Address before: Basel Applicant before: Ciba-Geigy AG |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
ASS | Succession or assignment of patent right |
Owner name: SINGENTA PARTICIPATION AG Free format text: FORMER OWNER: NOVANNIS COMPANY Effective date: 20021108 |
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C41 | Transfer of patent application or patent right or utility model | ||
TR01 | Transfer of patent right |
Effective date of registration: 20021108 Patentee after: Xingenta Shara Co., Ltd. Patentee before: Novartis AG |
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C17 | Cessation of patent right | ||
CX01 | Expiry of patent term |
Expiration termination date: 20131227 Granted publication date: 19980930 |