CN102803242B - 用于制备支化单羧酸的缩水甘油酯的方法 - Google Patents
用于制备支化单羧酸的缩水甘油酯的方法 Download PDFInfo
- Publication number
- CN102803242B CN102803242B CN201080025488.3A CN201080025488A CN102803242B CN 102803242 B CN102803242 B CN 102803242B CN 201080025488 A CN201080025488 A CN 201080025488A CN 102803242 B CN102803242 B CN 102803242B
- Authority
- CN
- China
- Prior art keywords
- reaction
- acid
- halide
- monocarboxylic acid
- epoxyalkyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
- C07D303/16—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by esterified hydroxyl radicals
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Epoxy Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP09075264A EP2261220A1 (en) | 2009-06-11 | 2009-06-11 | Process for preparing glycidyl esters of branched monocarboxylic acids |
| EP09075264.3 | 2009-06-11 | ||
| PCT/EP2010/003334 WO2010142396A1 (en) | 2009-06-11 | 2010-06-02 | Process for preparing glycidyl esters of branched monocarboxylic acids |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102803242A CN102803242A (zh) | 2012-11-28 |
| CN102803242B true CN102803242B (zh) | 2015-09-23 |
Family
ID=41100757
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201080025488.3A Active CN102803242B (zh) | 2009-06-11 | 2010-06-02 | 用于制备支化单羧酸的缩水甘油酯的方法 |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US8802872B2 (https=) |
| EP (2) | EP2261220A1 (https=) |
| JP (1) | JP5726180B2 (https=) |
| KR (1) | KR101384835B1 (https=) |
| CN (1) | CN102803242B (https=) |
| BR (1) | BRPI1013046A2 (https=) |
| MX (1) | MX2011013037A (https=) |
| RU (2) | RU2560877C2 (https=) |
| TW (1) | TWI405758B (https=) |
| WO (1) | WO2010142396A1 (https=) |
Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2476672A1 (en) | 2010-12-22 | 2012-07-18 | Momentive Specialty Chemicals Research Belgium S.A. | Glycidyl esters of alpha , alpha branched acids compositions |
| EP2474537A1 (en) * | 2010-12-22 | 2012-07-11 | Momentive Specialty Chemicals Research Belgium S.A. | glycidyl esters of alpha, alpha branched acids compositions |
| CN103890036A (zh) | 2011-10-19 | 2014-06-25 | 迈图专业化学股份有限公司 | 丙烯酸多元醇树脂组合物 |
| PL2768903T3 (pl) | 2011-10-19 | 2021-02-08 | Hexion Research Belgium Sa | Kompozycje żywic polieteropoliolowych |
| BR112014009484A8 (pt) | 2011-10-19 | 2018-02-06 | Hexion Inc | Composição de resinas acrílicas com função hidroxila, processo para preparar uma composição, composição aglutinante, substrato de metal ou de plástico, poliol acrílico, resina de copolímero de poliol acrílico, e, composição de revestimento |
| WO2013072481A1 (de) * | 2011-11-17 | 2013-05-23 | Basf Coatings Gmbh | Glyceroldiester, verfahren zu deren herstellung und deren verwendung in beschichtungsmitteln |
| WO2013075805A2 (en) * | 2011-11-25 | 2013-05-30 | Momentive Specialty Chemicals Research Beigium S.A. | Epoxy compositions |
| CN102924407A (zh) * | 2012-11-30 | 2013-02-13 | 西南化工研究设计院有限公司 | 一种一元羧酸缩水甘油酯的精制方法 |
| KR101650528B1 (ko) * | 2015-04-24 | 2016-08-23 | 대달산업주식회사 | 알파-분지형 지방족 모노카르복시산의 글리시딜 에스테르의 제조 방법 |
| EP3115409A1 (en) * | 2015-07-10 | 2017-01-11 | Hexion Research Belgium SA | Odorless polyester stabilizer compositions |
| KR20170112515A (ko) | 2016-03-31 | 2017-10-12 | 코오롱인더스트리 주식회사 | 글리시딜에스테르 화합물의 제조방법 |
| WO2018009355A1 (en) | 2016-07-08 | 2018-01-11 | Resinate Materials Group, Inc. | Sustainable polyol blends for high-performance coatings |
| US20190119510A1 (en) * | 2017-10-23 | 2019-04-25 | Hexion Inc. | Glycidyl esters of alpha, alpha branched acids compositions |
| EP3808823A1 (en) * | 2019-10-14 | 2021-04-21 | Hexion Research Belgium SA | Glycidyl esters of alpha, alpha branched acids from renewable sources and formulation thereof |
| CN110683996A (zh) * | 2019-11-01 | 2020-01-14 | 于翔 | 一种叔碳酸缩水甘油酯的制备方法 |
| KR20220152321A (ko) * | 2020-03-20 | 2022-11-15 | 인제비티 사우스 캐롤라이나, 엘엘씨 | 톨유 유래 글리시딜 에스테르 및 그 제조 방법 |
| CN111978502B (zh) * | 2020-08-18 | 2022-04-22 | 北京化工大学常州先进材料研究院 | 一种氨酯油丙烯酸酯光固化树脂及其制备方法 |
| CN117777060B (zh) * | 2023-12-26 | 2024-07-30 | 同宇新材料(广东)股份有限公司 | 一种亚麻油酸缩水甘油酯的制备方法 |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3178454A (en) * | 1959-05-19 | 1965-04-13 | Shell Oil Co | Epoxy esters of alpha, alpha-dialkyl monocarboxylic acids |
| US3275583A (en) * | 1959-05-19 | 1966-09-27 | Shell Oil Co | Alkyd resins prepared from epoxy esters of monocarboxylic acids and process for theproduction of same |
| CN1325392A (zh) * | 1998-09-23 | 2001-12-05 | 荷兰解决方案研究有限公司 | 制备支链羧酸的缩水甘油酯的方法 |
| CN101085764A (zh) * | 2007-07-09 | 2007-12-12 | 南京林业大学 | (甲基)丙烯酸缩水甘油酯的合成方法 |
| CN101220134A (zh) * | 2007-12-14 | 2008-07-16 | 中国科学院广州化学研究所 | 聚合松香二缩水甘油酯环氧树脂及其制备方法 |
| CN101245053A (zh) * | 2007-02-15 | 2008-08-20 | 天津市四友精细化学品有限公司 | 叔碳酸缩水甘油酯的制备方法 |
| WO2009000839A1 (de) * | 2007-06-28 | 2008-12-31 | Basf Se | C10 alkansäureglycidester und ihre verwendung |
Family Cites Families (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3075999A (en) | 1963-01-29 | Glycidyl esteks | ||
| GB763559A (en) | 1953-11-23 | 1956-12-12 | Bataafsche Petroleum | A process for preparing epoxy esters |
| US2992239A (en) | 1957-08-01 | 1961-07-11 | American Cyanamid Co | Preparing glycidyl esters of higher fatty acids |
| DE1219481B (de) | 1958-12-29 | 1966-06-23 | Shell Int Research | Verfahren zur Herstellung von Carbonsaeureglycidylestern |
| DE1211177B (de) | 1964-08-27 | 1966-02-24 | Bayer Ag | Verfahren zur Herstellung von Epoxyalkylestern von hydroaromatischen Mono- und Polycarbonsaeuren |
| US3859314A (en) | 1967-06-29 | 1975-01-07 | Celanese Coatings Co | Process for preparing glycidyl esters of polycarboxylic acids |
| JPS49815B1 (https=) * | 1970-10-27 | 1974-01-10 | ||
| DE2127699C3 (de) | 1971-06-04 | 1979-08-23 | Chemische Werke Huels Ag, 4370 Marl | Verfahren zur Herstellung von hydrolyseresistenten Glycidylestern |
| SU431162A1 (ru) * | 1972-06-23 | 1974-06-05 | Способ получения глицидиловых эфиров карбоновых кислот | |
| JPS5133528B2 (https=) * | 1972-09-19 | 1976-09-20 | ||
| JPS53147018A (en) * | 1977-05-26 | 1978-12-21 | Nippon Oil & Fats Co Ltd | Preparation of carboxylic acid glycidyl ester |
| JPS57130980A (en) * | 1981-02-07 | 1982-08-13 | Toto Kasei Kk | Preparation of epoxyalkyl ester |
| JPS57203077A (en) | 1981-06-06 | 1982-12-13 | New Japan Chem Co Ltd | Production of alpha-branched saturated fatty acid glycidyl ester |
| EP0475238A3 (en) | 1990-09-13 | 1994-05-25 | Dow Chemical Co | Mesogenic glycidyl esters |
| JPH0578340A (ja) * | 1991-09-19 | 1993-03-30 | Nippon Oil & Fats Co Ltd | グリシジルエステルの製造方法及びこの方法により得られた多価グリシジルエステル |
| AU714033B2 (en) | 1996-07-19 | 1999-12-16 | Nissan Chemical Industries Ltd. | Method for producing purified epoxy compound |
| US6570028B1 (en) | 2000-02-25 | 2003-05-27 | Resolution Performance Products Llc | Process for the preparation of glycidylesters of branched carboxylic acids |
| JP2003171371A (ja) | 2001-12-10 | 2003-06-20 | Yokkaichi Chem Co Ltd | α−モノ分岐飽和脂肪族カルボン酸グリシジルエステルの製造方法 |
| CN1425729A (zh) | 2002-12-30 | 2003-06-25 | 中国科学院广州化学研究所 | 丙烯海松酸二缩水甘油酯及其环氧树脂和它们的制法 |
| CN101245033A (zh) | 2007-02-16 | 2008-08-20 | 上海天伟生物制药有限公司 | 异丝氨酸酯衍生物及其制备方法 |
-
2009
- 2009-06-11 EP EP09075264A patent/EP2261220A1/en not_active Withdrawn
-
2010
- 2010-06-02 CN CN201080025488.3A patent/CN102803242B/zh active Active
- 2010-06-02 EP EP10739480.1A patent/EP2440539B1/en active Active
- 2010-06-02 JP JP2012514373A patent/JP5726180B2/ja active Active
- 2010-06-02 US US13/377,470 patent/US8802872B2/en active Active
- 2010-06-02 RU RU2014102706/04A patent/RU2560877C2/ru active
- 2010-06-02 RU RU2012100273/04A patent/RU2515897C2/ru active
- 2010-06-02 KR KR1020127000517A patent/KR101384835B1/ko active Active
- 2010-06-02 BR BRPI1013046A patent/BRPI1013046A2/pt not_active Application Discontinuation
- 2010-06-02 WO PCT/EP2010/003334 patent/WO2010142396A1/en not_active Ceased
- 2010-06-02 MX MX2011013037A patent/MX2011013037A/es active IP Right Grant
- 2010-06-11 TW TW099119175A patent/TWI405758B/zh active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3178454A (en) * | 1959-05-19 | 1965-04-13 | Shell Oil Co | Epoxy esters of alpha, alpha-dialkyl monocarboxylic acids |
| US3275583A (en) * | 1959-05-19 | 1966-09-27 | Shell Oil Co | Alkyd resins prepared from epoxy esters of monocarboxylic acids and process for theproduction of same |
| CN1325392A (zh) * | 1998-09-23 | 2001-12-05 | 荷兰解决方案研究有限公司 | 制备支链羧酸的缩水甘油酯的方法 |
| CN101245053A (zh) * | 2007-02-15 | 2008-08-20 | 天津市四友精细化学品有限公司 | 叔碳酸缩水甘油酯的制备方法 |
| WO2009000839A1 (de) * | 2007-06-28 | 2008-12-31 | Basf Se | C10 alkansäureglycidester und ihre verwendung |
| CN101085764A (zh) * | 2007-07-09 | 2007-12-12 | 南京林业大学 | (甲基)丙烯酸缩水甘油酯的合成方法 |
| CN101220134A (zh) * | 2007-12-14 | 2008-07-16 | 中国科学院广州化学研究所 | 聚合松香二缩水甘油酯环氧树脂及其制备方法 |
Non-Patent Citations (2)
| Title |
|---|
| Thermally depolymerizable polycarbonates. 2. Synthesis of novel linear tertiary copolycarbonates by phase-transfer catalysis;F. M. Houlihan,等;《Macromolecules》;19860131;第19卷(第1期);13-19 * |
| 叔碳酸缩水甘油酯的制备;项庆安 等;《涂料工业》;19821231(第2期);1-3、25 * |
Also Published As
| Publication number | Publication date |
|---|---|
| RU2515897C2 (ru) | 2014-05-20 |
| BRPI1013046A2 (pt) | 2015-09-15 |
| WO2010142396A1 (en) | 2010-12-16 |
| RU2560877C2 (ru) | 2015-08-20 |
| US8802872B2 (en) | 2014-08-12 |
| KR101384835B1 (ko) | 2014-04-15 |
| CN102803242A (zh) | 2012-11-28 |
| EP2440539B1 (en) | 2017-10-04 |
| MX2011013037A (es) | 2012-02-21 |
| TW201114751A (en) | 2011-05-01 |
| RU2012100273A (ru) | 2013-07-20 |
| JP5726180B2 (ja) | 2015-05-27 |
| TWI405758B (zh) | 2013-08-21 |
| JP2012529447A (ja) | 2012-11-22 |
| RU2014102706A (ru) | 2015-06-27 |
| KR20120016313A (ko) | 2012-02-23 |
| EP2440539A1 (en) | 2012-04-18 |
| US20120095244A1 (en) | 2012-04-19 |
| EP2261220A1 (en) | 2010-12-15 |
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Legal Events
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| C06 | Publication | ||
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| SE01 | Entry into force of request for substantive examination | ||
| CB02 | Change of applicant information |
Address after: American Ohio Applicant after: Hexion company Address before: American Ohio Applicant before: Momentive Specialty Chemicals Research S. A. |
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| COR | Change of bibliographic data |
Free format text: CORRECT: APPLICANT; FROM: MOMENTIVE SPECIALTY CHEMICALS INC. TO: HANDSOME COMPANY |
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |