CN101677538B - 制备高纯度D‑(‑)‑N,N‑二乙基‑2‑(α‑萘氧基)丙酰胺的方法 - Google Patents

制备高纯度D‑(‑)‑N,N‑二乙基‑2‑(α‑萘氧基)丙酰胺的方法 Download PDF

Info

Publication number
CN101677538B
CN101677538B CN200880014709.XA CN200880014709A CN101677538B CN 101677538 B CN101677538 B CN 101677538B CN 200880014709 A CN200880014709 A CN 200880014709A CN 101677538 B CN101677538 B CN 101677538B
Authority
CN
China
Prior art keywords
diethyl
propionamide
purity
reaction
alpha
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN200880014709.XA
Other languages
English (en)
Chinese (zh)
Other versions
CN101677538A (zh
Inventor
拉吉尼坎塔·杰得夫·什罗夫
拉吉尼坎塔·维克拉姆·什罗夫
普拉首塔姆·娜仁扎·卡瑞姆贝卡
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
UPL Ltd
Original Assignee
United Phosphorus Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=40226628&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=CN101677538(B) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by United Phosphorus Ltd filed Critical United Phosphorus Ltd
Publication of CN101677538A publication Critical patent/CN101677538A/zh
Application granted granted Critical
Publication of CN101677538B publication Critical patent/CN101677538B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/12—Preparation of carboxylic acid amides by reactions not involving the formation of carboxamide groups
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00—Carboxylic acid amides
    • C07C233/01—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C233/02—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
    • C07C233/04—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with carbon atoms of carboxamide groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
    • C07C233/05—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with carbon atoms of carboxamide groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton having the nitrogen atoms of the carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C235/00—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by oxygen atoms
    • C07C235/02—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by oxygen atoms having carbon atoms of carboxamide groups bound to acyclic carbon atoms and singly-bound oxygen atoms bound to the same carbon skeleton
    • C07C235/04—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by oxygen atoms having carbon atoms of carboxamide groups bound to acyclic carbon atoms and singly-bound oxygen atoms bound to the same carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C235/06—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by oxygen atoms having carbon atoms of carboxamide groups bound to acyclic carbon atoms and singly-bound oxygen atoms bound to the same carbon skeleton the carbon skeleton being acyclic and saturated having the nitrogen atoms of the carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Dentistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
CN200880014709.XA 2007-05-04 2008-05-05 制备高纯度D‑(‑)‑N,N‑二乙基‑2‑(α‑萘氧基)丙酰胺的方法 Active CN101677538B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
IN858MU2007 2007-05-04
IN858/MUM/2007 2007-05-04
PCT/IN2008/000284 WO2009004642A2 (en) 2007-05-04 2008-05-05 PROCESS FOR MANUFACTURE OF HIGH PURITY D-(-)-N, N-DIETHYL-2-(α- NAPHTHOXY) PROPIONAMIDE

Publications (2)

Publication Number Publication Date
CN101677538A CN101677538A (zh) 2010-03-24
CN101677538B true CN101677538B (zh) 2017-06-06

Family

ID=40226628

Family Applications (1)

Application Number Title Priority Date Filing Date
CN200880014709.XA Active CN101677538B (zh) 2007-05-04 2008-05-05 制备高纯度D‑(‑)‑N,N‑二乙基‑2‑(α‑萘氧基)丙酰胺的方法

Country Status (11)

Country Link
US (1) US8309765B2 (enExample)
EP (1) EP2146574B2 (enExample)
JP (1) JP2010526059A (enExample)
KR (3) KR101174962B1 (enExample)
CN (1) CN101677538B (enExample)
ES (1) ES2556230T5 (enExample)
HU (1) HUE026533T2 (enExample)
PL (1) PL2146574T5 (enExample)
RU (1) RU2458047C2 (enExample)
UA (1) UA103460C2 (enExample)
WO (1) WO2009004642A2 (enExample)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8557293B2 (en) * 2010-08-26 2013-10-15 Scott May Sunscreen compositions for application to plants
CN102887832B (zh) * 2012-09-29 2014-07-16 西安近代化学研究所 一种水相反应合成大位阻氯乙酰胺化合物的方法
EP4327660A3 (en) 2013-03-15 2025-04-02 UPL Limited Selective weed control using d-napropamide
US9307765B2 (en) * 2013-03-15 2016-04-12 Upl Limited Selective weed control using D-napropamide
JP2017533892A (ja) * 2014-10-03 2017-11-16 ピュラック バイオケム ビー． ブイ． Ｎ，ｎ−ジアルキルラクトアミドの製造法
CN106397240A (zh) * 2015-07-29 2017-02-15 国药集团化学试剂有限公司 2-卤代乙酰胺的合成方法
EA202191368A1 (ru) 2018-12-21 2021-07-29 Юпл Лимитед Гербицид
US20250081966A1 (en) 2021-12-29 2025-03-13 UPL Corporation Limited Herbicide combinations
WO2025012825A1 (en) 2023-07-11 2025-01-16 Upl Mauritius Limited Herbicide safener combinations and compositions

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3718455A (en) * 1970-07-20 1973-02-27 Stauffer Chemical Co Method of combatting weeds with {60 -naphthoxy acetamides
US3998880A (en) * 1975-08-15 1976-12-21 Stauffer Chemical Company Production of N,N-diethyl 2(α-naphthoxy)propionamide
US4668628A (en) * 1985-04-01 1987-05-26 Stauffer Chemical Company Resolution of racemic mixtures of aliphatic acid esters
US4766220A (en) * 1979-06-29 1988-08-23 Rhone-Poulenc Agrochimie Process for the preparation of optically active aryloxyalkanoic acid compounds

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU102735A1 (ru) * 1952-06-14 1955-11-30 А.П. Арендарук Способ получени пара-нитро-альфа-ацетил-амино-бета-оксипропиофенона
US3480671A (en) 1969-01-16 1969-11-25 Stauffer Chemical Co Alpha-naphthoxy acetamide compositions
US4358612A (en) 1981-01-02 1982-11-09 Stauffer Chemical Company Process for production of α-haloalkylamides
US4548641A (en) 1982-11-15 1985-10-22 Stauffer Chemical Company Herbicides: N,N-dialkyl-2-(4-substituted-1-naphthoxy) propionamides
EP0298177B1 (fr) * 1987-07-07 1992-04-15 Rhone-Poulenc Sante Nouveau procédé de préparation de dérivés de la pristinamycine IIB
JPH01168638A (ja) * 1987-12-25 1989-07-04 Mitsui Toatsu Chem Inc 光学活性２−クロロプロピオン酸の製造方法
CN1315868C (zh) * 2005-10-14 2007-05-16 邢将军 丙－谷二肽的制造方法

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3718455A (en) * 1970-07-20 1973-02-27 Stauffer Chemical Co Method of combatting weeds with {60 -naphthoxy acetamides
US3998880A (en) * 1975-08-15 1976-12-21 Stauffer Chemical Company Production of N,N-diethyl 2(α-naphthoxy)propionamide
US4766220A (en) * 1979-06-29 1988-08-23 Rhone-Poulenc Agrochimie Process for the preparation of optically active aryloxyalkanoic acid compounds
US4668628A (en) * 1985-04-01 1987-05-26 Stauffer Chemical Company Resolution of racemic mixtures of aliphatic acid esters

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Synthesis and herbicidal activity of N,N-diethyl-2-(1-naphthyloxy)propionamide and its optical isomers;James H. H. Chan et al.，;《J. Agric. Food Chem.》;19750531;第23卷(第5期);第1009页右栏第4段 *

Also Published As

Publication number Publication date
EP2146574A2 (en) 2010-01-27
KR20090131679A (ko) 2009-12-29
PL2146574T5 (pl) 2023-06-12
KR20130087610A (ko) 2013-08-06
HUE026533T2 (en) 2016-06-28
EP2146574B2 (en) 2022-11-02
JP2010526059A (ja) 2010-07-29
WO2009004642A2 (en) 2009-01-08
EP2146574A4 (en) 2012-02-29
KR101335861B1 (ko) 2013-12-02
RU2458047C2 (ru) 2012-08-10
US8309765B2 (en) 2012-11-13
ES2556230T3 (es) 2016-01-14
UA103460C2 (ru) 2013-10-25
WO2009004642A3 (en) 2009-07-02
EP2146574B1 (en) 2015-11-04
KR101174962B1 (ko) 2012-08-20
RU2009144977A (ru) 2011-06-10
US20100144532A1 (en) 2010-06-10
KR20120055724A (ko) 2012-05-31
ES2556230T5 (es) 2023-01-04
PL2146574T3 (pl) 2016-03-31
CN101677538A (zh) 2010-03-24

Similar Documents

Publication Publication Date Title
CN101677538B (zh) 制备高纯度D‑(‑)‑N,N‑二乙基‑2‑(α‑萘氧基)丙酰胺的方法
JP2625544B2 (ja) Ｎ―（ｒ）―（１―（４―クロロ―フェニル）―エチル）―２，２―ジクロロ―１―エチル―３―メチルシクロプロパンカルボキサミドの立体異性体
HU230485B1 (hu) Optikailag aktív, herbicid hatású (R)-fenoxi-propionsav-N-metil-N-(2-fluor-fenil)-amid
CN103261187A (zh) 制备四唑取代的邻氨基苯甲酰胺衍生物的方法以及这些衍生物的新的晶体多形体
PL125937B1 (en) Plant pollen disactivating agent and method of obtaining azethydine derivatives
JPS5910321B2 (ja) 有害微生物防除剤及びその製法
JPH0672977A (ja) 殺菌性フェニルベンズアミド及びその製造方法
JPH01221371A (ja) 環状オキシアミン誘導体の製造方法
JPH03148265A (ja) ５，７―ジフェニル―４，６―ジアザインダン誘導体、その製造法およびそれを有効成分とする除草剤
US4992471A (en) Molluscicides
JP2002512217A (ja) Ｎ−（１−シアノアルキル）−２−フェノキシプロピオンアミド誘導体の改良された製造方法
US4382954A (en) Fungicidal N-1-substituted cyclopropyl-N-acyl-2,6-dialkylaniline
JP2553335B2 (ja) 光学活性シクロプロパンカルボキサミド類及び該活性体とその鏡像異性体との鏡像異性体対、並びに農業用殺菌剤
CN118026924A (zh) 4-氨基-3,5-二氯-6-氟-吡啶-2-氧乙酸衍生物及其制备方法和应用
JPH08193011A (ja) 除草性スルホンアミド化合物
KR820000926B1 (ko) 페녹시페녹시-알칸카복실산 유도체의 제조방법
JPH0442376B2 (enExample)
JPS6277366A (ja) インド−ル酢酸誘導体及びその製法
JPS6021135B2 (ja) トルイル酸アニリド類及びその製造方法並びにそれを含有する農園芸用殺菌剤
BR112021006119A2 (pt) derivado de carboxamida de tiofeno e agente de controle de doenças de plantas compreendendo o mesmo
JPH03251575A (ja) ４−置換５−クロル−２−ヒドラジノチアゾール及びその製造用の中間体
JPS59101403A (ja) カルボン酸２，２−ジクロル−３，３−ジメチル−シクロプロピルメチルエステル誘導体及び農業用殺菌剤
JPH0826009B2 (ja) 選択性除草剤として有用な新規１，２，４―オキサジアゾール誘導体
JPH0784426B2 (ja) シクロプロパンカルボキサミド及び農業用殺菌剤
JPS6241705B2 (enExample)

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C53 Correction of patent of invention or patent application
CB02 Change of applicant information

Address after: India, Gujarat

Applicant after: UNITED PHOSPHORUS LIMITED

Address before: India, Gujarat

Applicant before: United Phosphorus Ltd.

COR Change of bibliographic data

Free format text: CORRECT: APPLICANT; FROM: UNITED PHOSPHORUS LTD. TO: UPL LTD.

GR01 Patent grant
GR01 Patent grant