CN101434700B - 改性氰酸酯树脂及其制备方法 - Google Patents
改性氰酸酯树脂及其制备方法 Download PDFInfo
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- CN101434700B CN101434700B CN2008102437830A CN200810243783A CN101434700B CN 101434700 B CN101434700 B CN 101434700B CN 2008102437830 A CN2008102437830 A CN 2008102437830A CN 200810243783 A CN200810243783 A CN 200810243783A CN 101434700 B CN101434700 B CN 101434700B
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- Prior art keywords
- resin
- cyanate
- acid ester
- cyanic acid
- ester resin
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- 229920005989 resin Polymers 0.000 title claims abstract description 80
- 239000011347 resin Substances 0.000 title claims abstract description 80
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 125000000816 ethylene group Chemical group [H]C([H])([*:1])C([H])([H])[*:2] 0.000 title 1
- XLJMAIOERFSOGZ-UHFFFAOYSA-M cyanate Chemical compound [O-]C#N XLJMAIOERFSOGZ-UHFFFAOYSA-M 0.000 claims abstract description 61
- -1 polysiloxane Polymers 0.000 claims abstract description 22
- 150000001913 cyanates Chemical class 0.000 claims abstract description 10
- 239000012153 distilled water Substances 0.000 claims abstract description 6
- 238000001291 vacuum drying Methods 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- AHZMUXQJTGRNHT-UHFFFAOYSA-N [4-[2-(4-cyanatophenyl)propan-2-yl]phenyl] cyanate Chemical compound C=1C=C(OC#N)C=CC=1C(C)(C)C1=CC=C(OC#N)C=C1 AHZMUXQJTGRNHT-UHFFFAOYSA-N 0.000 claims description 18
- 238000013019 agitation Methods 0.000 claims description 12
- 238000006243 chemical reaction Methods 0.000 claims description 6
- XDLMVUHYZWKMMD-UHFFFAOYSA-N 3-trimethoxysilylpropyl 2-methylprop-2-enoate Chemical compound CO[Si](OC)(OC)CCCOC(=O)C(C)=C XDLMVUHYZWKMMD-UHFFFAOYSA-N 0.000 claims description 5
- 238000010792 warming Methods 0.000 claims description 5
- 125000000524 functional group Chemical group 0.000 claims description 4
- 239000000178 monomer Substances 0.000 claims description 4
- 238000000034 method Methods 0.000 abstract description 10
- 230000008569 process Effects 0.000 abstract description 3
- 229920001296 polysiloxane Polymers 0.000 abstract 2
- GLZPKHIDCKLLFQ-UHFFFAOYSA-N [dimethoxy(propyl)silyl]oxymethanol Chemical compound CCC[Si](OC)(OC)OCO GLZPKHIDCKLLFQ-UHFFFAOYSA-N 0.000 abstract 1
- 230000004048 modification Effects 0.000 description 24
- 238000012986 modification Methods 0.000 description 24
- 238000005303 weighing Methods 0.000 description 11
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 9
- 230000000052 comparative effect Effects 0.000 description 7
- 230000008023 solidification Effects 0.000 description 7
- 238000007711 solidification Methods 0.000 description 6
- 238000001816 cooling Methods 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 5
- 238000010586 diagram Methods 0.000 description 4
- 230000003197 catalytic effect Effects 0.000 description 3
- 230000035939 shock Effects 0.000 description 3
- 229920001187 thermosetting polymer Polymers 0.000 description 3
- 230000007812 deficiency Effects 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 229930185605 Bisphenol Natural products 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 230000002860 competitive effect Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000007334 copolymerization reaction Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- NRZTVPSNPGMAGH-UHFFFAOYSA-N cyanic acid cyclopenta-1,3-diene Chemical compound OC#N.C1C=CC=C1 NRZTVPSNPGMAGH-UHFFFAOYSA-N 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000008204 material by function Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 238000011017 operating method Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000003014 reinforcing effect Effects 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 229920005992 thermoplastic resin Polymers 0.000 description 1
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- Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
Abstract
Description
Claims (3)
Priority Applications (1)
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CN2008102437830A CN101434700B (zh) | 2008-12-15 | 2008-12-15 | 改性氰酸酯树脂及其制备方法 |
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CN2008102437830A CN101434700B (zh) | 2008-12-15 | 2008-12-15 | 改性氰酸酯树脂及其制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN101434700A CN101434700A (zh) | 2009-05-20 |
CN101434700B true CN101434700B (zh) | 2010-12-08 |
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CN2008102437830A Expired - Fee Related CN101434700B (zh) | 2008-12-15 | 2008-12-15 | 改性氰酸酯树脂及其制备方法 |
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CN (1) | CN101434700B (zh) |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103951829B (zh) * | 2014-04-21 | 2016-09-07 | 苏州大学 | 一种超支化聚硅氧烷液晶改性热固性树脂及其制备方法 |
CN106221213B (zh) * | 2016-07-29 | 2018-08-31 | 苏州巨峰电气绝缘系统股份有限公司 | 一种核电驱动机构用耐高温绝缘结构件及其制备方法 |
CN107722266B (zh) * | 2017-10-19 | 2020-06-16 | 苏州大学 | 一种超支化聚硅氧烷/氰酸酯树脂及其制备方法 |
CN107556479B (zh) * | 2017-10-19 | 2020-07-21 | 苏州大学 | 一种超支化聚硅氧烷及其制备方法 |
CN107903864B (zh) * | 2017-11-23 | 2021-03-30 | 艾艾精密工业输送系统(上海)股份有限公司 | 一种耐湿热超支化聚硅氧烷改性胶黏剂及其制备方法 |
CN108571018A (zh) * | 2018-05-04 | 2018-09-25 | 于连正 | 一种应用自粘结含镓防水材料的地下防水工程施工方法 |
CN110372861B (zh) * | 2019-06-27 | 2020-04-28 | 扬州天启新材料股份有限公司 | 具有低吸湿性的改性双环戊二烯型氰酸酯树脂的制备方法 |
CN111484516A (zh) * | 2020-04-26 | 2020-08-04 | 扬州天启新材料股份有限公司 | 一种具有超疏水性能的硅基氰酸酯树脂 |
CN112341827B (zh) * | 2020-11-23 | 2022-04-29 | 航天特种材料及工艺技术研究所 | 一种超支化聚硅氧烷改性氰酸酯树脂复合材料及其制备方法 |
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- 2008-12-15 CN CN2008102437830A patent/CN101434700B/zh not_active Expired - Fee Related
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CN101434700A (zh) | 2009-05-20 |
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EE01 | Entry into force of recordation of patent licensing contract |
Application publication date: 20090520 Assignee: Yangzhou Tianqi Chemical Co.,Ltd. Assignor: Soochow University Contract record no.: 2014320000159 Denomination of invention: Modified cyanate ester resin and preparation method and uses thereof Granted publication date: 20101208 License type: Exclusive License Record date: 20140306 |
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Address after: Suzhou City, Jiangsu province 215137 Xiangcheng District Ji Road No. 8 Patentee after: Soochow University Address before: 215123 Suzhou City, Suzhou Province Industrial Park, No. love road, No. 199 Patentee before: Soochow University |
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Change date: 20150907 Contract record no.: 2014320000159 Assignee after: YANGZHOU TECHIA MATERIAL CO., LTD. Assignee before: Yangzhou Tianqi Chemical Co.,Ltd. |
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Granted publication date: 20101208 Termination date: 20171215 |
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