CA2908710A1 - Method for the purification of acetic acid and acrylic acid - Google Patents
Method for the purification of acetic acid and acrylic acidInfo
- Publication number
- CA2908710A1 CA2908710A1 CA2908710A CA2908710A CA2908710A1 CA 2908710 A1 CA2908710 A1 CA 2908710A1 CA 2908710 A CA2908710 A CA 2908710A CA 2908710 A CA2908710 A CA 2908710A CA 2908710 A1 CA2908710 A1 CA 2908710A1
- Authority
- CA
- Canada
- Prior art keywords
- boiling solvent
- mixture
- crude product
- inhibitor
- acrylic acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
- C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
- C07C51/215—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of saturated hydrocarbyl groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
- C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
- C07C51/46—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation by azeotropic distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201361825205P | 2013-05-20 | 2013-05-20 | |
| US61/825,205 | 2013-05-20 | ||
| PCT/US2014/038573 WO2014189829A1 (en) | 2013-05-20 | 2014-05-19 | Method for the purification of acetic acid and acrylic acid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA2908710A1 true CA2908710A1 (en) | 2014-11-27 |
Family
ID=50942932
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2908710A Abandoned CA2908710A1 (en) | 2013-05-20 | 2014-05-19 | Method for the purification of acetic acid and acrylic acid |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US9944582B2 (https=) |
| EP (1) | EP2999686A1 (https=) |
| JP (1) | JP2016520096A (https=) |
| KR (1) | KR20160009598A (https=) |
| CN (1) | CN105263895B (https=) |
| AU (1) | AU2014268860B2 (https=) |
| CA (1) | CA2908710A1 (https=) |
| WO (1) | WO2014189829A1 (https=) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10239815B2 (en) | 2015-02-05 | 2019-03-26 | Nippon Shokubai Co., Ltd. | Method for producing acrylic acid |
| WO2017114831A1 (en) * | 2015-12-29 | 2017-07-06 | Shell Internationale Research Maatschappij B.V. | Process for converting alkanes and/or alkenes to alkenes and carboxylic acids |
| KR102079775B1 (ko) * | 2016-11-25 | 2020-02-20 | 주식회사 엘지화학 | (메트)아크릴산의 연속 회수 방법 및 장치 |
| FR3060000B1 (fr) * | 2016-12-08 | 2020-05-01 | Arkema France | Procede pour eviter le depot de polymeres dans un procede de purification d'acide (meth)acrylique. |
Family Cites Families (50)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2748159A (en) | 1952-09-08 | 1956-05-29 | Goodyear Tire & Rubber | Purification and decolorization of esters |
| GB783463A (en) | 1955-05-10 | 1957-09-25 | Distillers Co Yeast Ltd | Esters purification process |
| US2862958A (en) | 1955-10-13 | 1958-12-02 | Hercules Powder Co Ltd | Method of improving electrical properties of plasticizers by treatment with magnesium silicate |
| GB813867A (en) | 1956-12-27 | 1959-05-27 | Distillers Co Yeast Ltd | Purification of esters of dicarboxylic acids |
| DE1173473B (de) | 1962-06-29 | 1964-07-09 | Reichhold Chemie Ag | Verfahren zum Herstellen von aliphatischen oder aromatischen Carbonsaeureestern |
| DE1264762B (de) | 1963-09-03 | 1968-03-28 | Reichhold Chemie Ag | Weichmacher fuer organische Polymere |
| US3433831A (en) | 1965-06-30 | 1969-03-18 | Asahi Chemical Ind | Separation and purification of acrylic acid from acetic acid by solvent extraction and azeotropic distillation with a two component solvent-entrainer system |
| JPS5011364B1 (https=) * | 1965-06-30 | 1975-04-30 | ||
| BE706512A (https=) * | 1966-11-14 | 1968-05-14 | ||
| US3422831A (en) * | 1967-02-20 | 1969-01-21 | Gen Electric | Turbine control system |
| US3666632A (en) * | 1968-10-08 | 1972-05-30 | Asahi Chemical Ind | Method for the separation of acrylic acid from aqueous solution containing acrylic acid and acetic acid |
| JPS4946942B1 (https=) | 1971-04-05 | 1974-12-12 | ||
| JPS5522462B2 (https=) | 1972-05-24 | 1980-06-17 | ||
| JPS4995918A (https=) | 1973-01-24 | 1974-09-11 | ||
| JPS5011364A (https=) | 1973-05-30 | 1975-02-05 | ||
| US5243069A (en) * | 1981-12-11 | 1993-09-07 | Rohm And Haas Company | Ester of Michael addition homopolymers of acrylic acid |
| JPS62267341A (ja) | 1986-05-16 | 1987-11-20 | Mitsubishi Kasei Vinyl Co | 可塑剤の製造法 |
| JPH0341051A (ja) | 1989-07-07 | 1991-02-21 | Idemitsu Petrochem Co Ltd | アクリル酸エステル又はメタクリル酸エステルの製造方法 |
| US5198580A (en) | 1991-11-18 | 1993-03-30 | The Standard Oil Company | Process for oxidation of propane |
| JPH089567B2 (ja) | 1992-01-09 | 1996-01-31 | 株式会社日本触媒 | アクリル酸製造においてアクリル酸を高純度に精製する方法 |
| TW295580B (https=) * | 1992-01-09 | 1997-01-11 | Nippon Catalytic Chem Ind | |
| JP3832868B2 (ja) | 1994-07-27 | 2006-10-11 | 三菱化学株式会社 | アクリル酸の精製法 |
| JP3937462B2 (ja) | 1994-08-04 | 2007-06-27 | 三菱化学株式会社 | アクリル酸精製法 |
| JP3202150B2 (ja) | 1995-08-04 | 2001-08-27 | 昭和電工株式会社 | 酢酸の精製方法 |
| JP3219682B2 (ja) * | 1995-09-29 | 2001-10-15 | 昭和電工株式会社 | 酢酸の精製方法、及び酢酸の製造方法 |
| JP3028925B2 (ja) | 1995-12-05 | 2000-04-04 | 株式会社日本触媒 | アクリル酸の製造方法 |
| JPH09263566A (ja) | 1996-03-29 | 1997-10-07 | Cosmo Sogo Kenkyusho:Kk | 粗ベンゼンジカルボン酸の精製方法、精製に使用する触媒およびその製造方法 |
| FR2753445B1 (fr) * | 1996-09-16 | 1998-10-30 | Atochem Elf Sa | Procede perfectionne de purification de l'acide acrylique |
| JP3880128B2 (ja) | 1997-05-08 | 2007-02-14 | 株式会社日本触媒 | アクリル酸の回収方法 |
| JP3937495B2 (ja) | 1997-02-28 | 2007-06-27 | 株式会社日本触媒 | アクリル酸の回収方法 |
| US6084127A (en) | 1997-02-28 | 2000-07-04 | Nippon Shokubai Co Ltd | Method for recovering acrylic acid |
| US5880310A (en) | 1997-05-21 | 1999-03-09 | Mitsubishi Gas Chemical Company, Inc. | Process for producing plasticizer esters |
| US6114278A (en) | 1998-11-16 | 2000-09-05 | Saudi Basic Industries Corporation | Catalysts for catalytic oxidation of propane to acrylic acid, methods of making and using the same |
| EP1035103B1 (en) | 1999-03-05 | 2003-10-15 | Rohm And Haas Company | Process for preparing acrylic acid |
| JP5073129B2 (ja) | 1999-03-31 | 2012-11-14 | 株式会社日本触媒 | (メタ)アクリル酸の精製方法 |
| JP4809532B2 (ja) | 1999-11-15 | 2011-11-09 | サウディ ベーシック インダストリーズ コーポレイション | プロパンのアクリル酸への接触酸化用触媒、その製造法及び使用法 |
| CN1209332C (zh) * | 2000-06-14 | 2005-07-06 | 巴斯福股份公司 | 丙烯醛和/或丙烯酸的制备方法 |
| JP2005232008A (ja) | 2001-12-27 | 2005-09-02 | Mitsubishi Chemicals Corp | (メタ)アクリル酸の蒸留方法 |
| WO2003064367A1 (en) | 2002-01-29 | 2003-08-07 | Mitsubishi Chemical Corporation | Process for production of (meth)acrylic acid |
| GB0320206D0 (en) | 2003-08-29 | 2003-10-01 | Exxonmobil Chem Patents Inc | Improvements in or relating to plasticiser |
| FR2861724B1 (fr) | 2003-11-04 | 2005-12-30 | Arkema | Procede de purification de l'acide (meth)acrylique obtenu par oxydation d'un substrat gazeux |
| JP2005179352A (ja) * | 2003-11-28 | 2005-07-07 | Mitsubishi Chemicals Corp | (メタ)アクリル酸の精製方法 |
| WO2005051883A1 (ja) | 2003-11-28 | 2005-06-09 | Mitsubishi Chemical Corporation | (メタ)アクリル酸の精製方法 |
| JP4333471B2 (ja) | 2004-05-11 | 2009-09-16 | 新日本理化株式会社 | ジカルボン酸ジエステルの製造方法 |
| JP4621174B2 (ja) | 2006-06-19 | 2011-01-26 | 株式会社日本触媒 | (メタ)アクリル酸および/またはそのエステルの蒸留方法 |
| CN1884249A (zh) | 2006-07-11 | 2006-12-27 | 天津天溶化工有限公司 | 邻苯二甲酸二辛酯清洁生产方法 |
| CN101269899B (zh) | 2008-05-13 | 2011-05-11 | 吉林大学 | 一种丙烯酸废水的综合处理方法 |
| CN101367720A (zh) | 2008-09-18 | 2009-02-18 | 中国石油大学(华东) | 一种隔壁共沸精馏塔提纯丙烯酸的工艺方法及装置 |
| CN101530780B (zh) | 2009-04-21 | 2011-08-24 | 浙江工商大学 | 一种两步分离提纯柱及其应用 |
| EP3004046A1 (en) | 2013-06-07 | 2016-04-13 | Saudi Basic Industries Corporation | Method for purifying dioctyl phthalate |
-
2014
- 2014-05-19 WO PCT/US2014/038573 patent/WO2014189829A1/en not_active Ceased
- 2014-05-19 US US14/787,683 patent/US9944582B2/en not_active Expired - Fee Related
- 2014-05-19 AU AU2014268860A patent/AU2014268860B2/en not_active Ceased
- 2014-05-19 EP EP14730395.2A patent/EP2999686A1/en not_active Ceased
- 2014-05-19 KR KR1020157034638A patent/KR20160009598A/ko not_active Withdrawn
- 2014-05-19 JP JP2016514987A patent/JP2016520096A/ja not_active Ceased
- 2014-05-19 CN CN201480029153.7A patent/CN105263895B/zh not_active Expired - Fee Related
- 2014-05-19 CA CA2908710A patent/CA2908710A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| AU2014268860A1 (en) | 2015-10-22 |
| JP2016520096A (ja) | 2016-07-11 |
| WO2014189829A1 (en) | 2014-11-27 |
| CN105263895B (zh) | 2018-04-10 |
| CN105263895A (zh) | 2016-01-20 |
| US9944582B2 (en) | 2018-04-17 |
| KR20160009598A (ko) | 2016-01-26 |
| AU2014268860B2 (en) | 2017-02-02 |
| EP2999686A1 (en) | 2016-03-30 |
| US20160075630A1 (en) | 2016-03-17 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request |
Effective date: 20151001 |
|
| FZDE | Discontinued |
Effective date: 20210831 |