CA2788157C - Lubricating greases containing lignin sulfonate, production and use thereof - Google Patents
Lubricating greases containing lignin sulfonate, production and use thereof Download PDFInfo
- Publication number
- CA2788157C CA2788157C CA2788157A CA2788157A CA2788157C CA 2788157 C CA2788157 C CA 2788157C CA 2788157 A CA2788157 A CA 2788157A CA 2788157 A CA2788157 A CA 2788157A CA 2788157 C CA2788157 C CA 2788157C
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- Prior art keywords
- calcium
- process according
- salt
- composition according
- carbon atoms
- Prior art date
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- 230000001050 lubricating effect Effects 0.000 title claims abstract description 61
- 229920001732 Lignosulfonate Polymers 0.000 title claims abstract description 43
- 238000004519 manufacturing process Methods 0.000 title description 10
- 239000004519 grease Substances 0.000 claims abstract description 74
- 239000011575 calcium Substances 0.000 claims abstract description 54
- 238000000034 method Methods 0.000 claims abstract description 54
- 230000008569 process Effects 0.000 claims abstract description 47
- 229910052791 calcium Inorganic materials 0.000 claims abstract description 46
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims abstract description 45
- 239000002199 base oil Substances 0.000 claims abstract description 43
- 239000000654 additive Substances 0.000 claims abstract description 40
- 239000000344 soap Substances 0.000 claims abstract description 35
- RYAGRZNBULDMBW-UHFFFAOYSA-L calcium;3-(2-hydroxy-3-methoxyphenyl)-2-[2-methoxy-4-(3-sulfonatopropyl)phenoxy]propane-1-sulfonate Chemical compound [Ca+2].COC1=CC=CC(CC(CS([O-])(=O)=O)OC=2C(=CC(CCCS([O-])(=O)=O)=CC=2)OC)=C1O RYAGRZNBULDMBW-UHFFFAOYSA-L 0.000 claims abstract description 34
- 238000001816 cooling Methods 0.000 claims abstract description 14
- 238000002156 mixing Methods 0.000 claims abstract description 9
- 238000010438 heat treatment Methods 0.000 claims abstract description 7
- 238000009835 boiling Methods 0.000 claims abstract description 5
- 239000000203 mixture Substances 0.000 claims description 80
- 239000002585 base Substances 0.000 claims description 43
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 39
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims description 31
- 239000000920 calcium hydroxide Substances 0.000 claims description 31
- 235000011116 calcium hydroxide Nutrition 0.000 claims description 31
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims description 31
- 239000008139 complexing agent Substances 0.000 claims description 30
- 125000004432 carbon atom Chemical group C* 0.000 claims description 28
- -1 - 0 to 40 wt % Substances 0.000 claims description 26
- 239000000314 lubricant Substances 0.000 claims description 21
- 150000003839 salts Chemical class 0.000 claims description 20
- 229920006395 saturated elastomer Polymers 0.000 claims description 20
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 19
- 239000000194 fatty acid Substances 0.000 claims description 19
- 229930195729 fatty acid Natural products 0.000 claims description 19
- 239000007787 solid Substances 0.000 claims description 19
- 238000006243 chemical reaction Methods 0.000 claims description 18
- 150000002763 monocarboxylic acids Chemical class 0.000 claims description 18
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 claims description 17
- 150000002148 esters Chemical class 0.000 claims description 17
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 15
- 150000004665 fatty acids Chemical class 0.000 claims description 13
- 229910052717 sulfur Inorganic materials 0.000 claims description 13
- 239000011593 sulfur Substances 0.000 claims description 13
- 230000035515 penetration Effects 0.000 claims description 12
- 239000002994 raw material Substances 0.000 claims description 12
- 159000000007 calcium salts Chemical class 0.000 claims description 11
- 150000001875 compounds Chemical class 0.000 claims description 11
- 238000011156 evaluation Methods 0.000 claims description 11
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims description 10
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 10
- CWQXQMHSOZUFJS-UHFFFAOYSA-N molybdenum disulfide Chemical compound S=[Mo]=S CWQXQMHSOZUFJS-UHFFFAOYSA-N 0.000 claims description 9
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 9
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 8
- 239000003963 antioxidant agent Substances 0.000 claims description 8
- 150000001991 dicarboxylic acids Chemical class 0.000 claims description 8
- 229920000642 polymer Polymers 0.000 claims description 8
- 239000000843 powder Substances 0.000 claims description 8
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 7
- 150000001447 alkali salts Chemical class 0.000 claims description 7
- 239000003795 chemical substances by application Substances 0.000 claims description 7
- 239000010439 graphite Substances 0.000 claims description 7
- 229910002804 graphite Inorganic materials 0.000 claims description 7
- 239000000463 material Substances 0.000 claims description 7
- 229910052751 metal Inorganic materials 0.000 claims description 7
- 239000002184 metal Substances 0.000 claims description 7
- 239000000047 product Substances 0.000 claims description 7
- 229910052708 sodium Inorganic materials 0.000 claims description 7
- VLCLHFYFMCKBRP-UHFFFAOYSA-N tricalcium;diborate Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]B([O-])[O-].[O-]B([O-])[O-] VLCLHFYFMCKBRP-UHFFFAOYSA-N 0.000 claims description 7
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 6
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims description 6
- 239000003513 alkali Substances 0.000 claims description 6
- 159000000013 aluminium salts Chemical class 0.000 claims description 6
- 229910000329 aluminium sulfate Inorganic materials 0.000 claims description 6
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical class OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 claims description 6
- 238000005461 lubrication Methods 0.000 claims description 6
- 229910052982 molybdenum disulfide Inorganic materials 0.000 claims description 6
- 229920000570 polyether Polymers 0.000 claims description 6
- 239000004721 Polyphenylene oxide Substances 0.000 claims description 5
- 230000000996 additive effect Effects 0.000 claims description 5
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims description 5
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 5
- 239000007866 anti-wear additive Substances 0.000 claims description 5
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims description 5
- 239000004327 boric acid Substances 0.000 claims description 5
- 239000012990 dithiocarbamate Substances 0.000 claims description 5
- 238000011065 in-situ storage Methods 0.000 claims description 5
- 229910052961 molybdenite Inorganic materials 0.000 claims description 5
- 239000001488 sodium phosphate Substances 0.000 claims description 5
- 159000000000 sodium salts Chemical class 0.000 claims description 5
- 241001465754 Metazoa Species 0.000 claims description 4
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims description 4
- 150000001342 alkaline earth metals Chemical class 0.000 claims description 4
- 239000007795 chemical reaction product Substances 0.000 claims description 4
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 4
- 229910052976 metal sulfide Inorganic materials 0.000 claims description 4
- 229910052750 molybdenum Inorganic materials 0.000 claims description 4
- 239000011733 molybdenum Substances 0.000 claims description 4
- 239000004810 polytetrafluoroethylene Substances 0.000 claims description 4
- 229920001343 polytetrafluoroethylene Polymers 0.000 claims description 4
- LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 claims description 4
- 229920001169 thermoplastic Polymers 0.000 claims description 4
- 239000004416 thermosoftening plastic Substances 0.000 claims description 4
- WMYJOZQKDZZHAC-UHFFFAOYSA-H trizinc;dioxido-sulfanylidene-sulfido-$l^{5}-phosphane Chemical compound [Zn+2].[Zn+2].[Zn+2].[O-]P([O-])([S-])=S.[O-]P([O-])([S-])=S WMYJOZQKDZZHAC-UHFFFAOYSA-H 0.000 claims description 4
- 229910052582 BN Inorganic materials 0.000 claims description 3
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 claims description 3
- 229920002367 Polyisobutene Polymers 0.000 claims description 3
- 239000004793 Polystyrene Substances 0.000 claims description 3
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 3
- 239000004411 aluminium Substances 0.000 claims description 3
- 229910052782 aluminium Inorganic materials 0.000 claims description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 3
- 239000006227 byproduct Substances 0.000 claims description 3
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 3
- 239000003623 enhancer Substances 0.000 claims description 3
- 229920001002 functional polymer Polymers 0.000 claims description 3
- 229920000193 polymethacrylate Polymers 0.000 claims description 3
- ITRNXVSDJBHYNJ-UHFFFAOYSA-N tungsten disulfide Chemical compound S=[W]=S ITRNXVSDJBHYNJ-UHFFFAOYSA-N 0.000 claims description 3
- 229910052725 zinc Inorganic materials 0.000 claims description 3
- 239000011701 zinc Substances 0.000 claims description 3
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 2
- 239000004952 Polyamide Substances 0.000 claims description 2
- 239000004642 Polyimide Substances 0.000 claims description 2
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims description 2
- 150000001408 amides Chemical class 0.000 claims description 2
- 239000010775 animal oil Substances 0.000 claims description 2
- 150000004982 aromatic amines Chemical class 0.000 claims description 2
- QRUDEWIWKLJBPS-UHFFFAOYSA-N benzotriazole Chemical compound C1=CC=C2N[N][N]C2=C1 QRUDEWIWKLJBPS-UHFFFAOYSA-N 0.000 claims description 2
- 229910052797 bismuth Inorganic materials 0.000 claims description 2
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 claims description 2
- 150000001622 bismuth compounds Chemical class 0.000 claims description 2
- 239000001506 calcium phosphate Substances 0.000 claims description 2
- 235000011010 calcium phosphates Nutrition 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims description 2
- 229910003002 lithium salt Inorganic materials 0.000 claims description 2
- 159000000002 lithium salts Chemical group 0.000 claims description 2
- 229910044991 metal oxide Inorganic materials 0.000 claims description 2
- 150000004706 metal oxides Chemical class 0.000 claims description 2
- 150000004045 organic chlorine compounds Chemical class 0.000 claims description 2
- 239000003208 petroleum Substances 0.000 claims description 2
- 150000002989 phenols Chemical class 0.000 claims description 2
- 239000011574 phosphorus Substances 0.000 claims description 2
- 229910052698 phosphorus Inorganic materials 0.000 claims description 2
- 229920002647 polyamide Polymers 0.000 claims description 2
- 229920001721 polyimide Polymers 0.000 claims description 2
- 229920005862 polyol Polymers 0.000 claims description 2
- 229920002223 polystyrene Polymers 0.000 claims description 2
- 235000010288 sodium nitrite Nutrition 0.000 claims description 2
- 229910052718 tin Inorganic materials 0.000 claims description 2
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical class [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 claims description 2
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 claims description 2
- 229910052721 tungsten Inorganic materials 0.000 claims description 2
- 239000010937 tungsten Substances 0.000 claims description 2
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 2
- 239000008158 vegetable oil Substances 0.000 claims description 2
- MBBWTVUFIXOUBE-UHFFFAOYSA-L zinc;dicarbamodithioate Chemical compound [Zn+2].NC([S-])=S.NC([S-])=S MBBWTVUFIXOUBE-UHFFFAOYSA-L 0.000 claims description 2
- 150000008064 anhydrides Chemical class 0.000 claims 3
- 150000001732 carboxylic acid derivatives Chemical class 0.000 claims 2
- 150000004659 dithiocarbamates Chemical class 0.000 claims 2
- GVTKMJAHUBVMKD-UHFFFAOYSA-N C(CCCCCCCC)C=1C(C(C2=CC=CC=C2C=1)=O)CCCCCCCCC Chemical compound C(CCCCCCCC)C=1C(C(C2=CC=CC=C2C=1)=O)CCCCCCCCC GVTKMJAHUBVMKD-UHFFFAOYSA-N 0.000 claims 1
- PEFNMPZKHOCMSW-UHFFFAOYSA-H [Al+3].[Al+3].[O-]O[O-].[O-]O[O-].[O-]O[O-] Chemical class [Al+3].[Al+3].[O-]O[O-].[O-]O[O-].[O-]O[O-] PEFNMPZKHOCMSW-UHFFFAOYSA-H 0.000 claims 1
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims 1
- 229910021502 aluminium hydroxide Inorganic materials 0.000 claims 1
- 230000005540 biological transmission Effects 0.000 claims 1
- 235000010216 calcium carbonate Nutrition 0.000 claims 1
- 229910017053 inorganic salt Inorganic materials 0.000 claims 1
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 claims 1
- 239000000347 magnesium hydroxide Substances 0.000 claims 1
- 229910001862 magnesium hydroxide Inorganic materials 0.000 claims 1
- 239000003607 modifier Substances 0.000 claims 1
- KHYKFSXXGRUKRE-UHFFFAOYSA-J molybdenum(4+) tetracarbamodithioate Chemical compound C(N)([S-])=S.[Mo+4].C(N)([S-])=S.C(N)([S-])=S.C(N)([S-])=S KHYKFSXXGRUKRE-UHFFFAOYSA-J 0.000 claims 1
- 150000002894 organic compounds Chemical class 0.000 claims 1
- 235000011008 sodium phosphates Nutrition 0.000 claims 1
- 150000004763 sulfides Chemical class 0.000 claims 1
- 229960005069 calcium Drugs 0.000 description 32
- 235000001465 calcium Nutrition 0.000 description 31
- 239000000306 component Substances 0.000 description 18
- 229920005610 lignin Polymers 0.000 description 17
- 238000009472 formulation Methods 0.000 description 12
- CXMXRPHRNRROMY-UHFFFAOYSA-N sebacic acid Chemical compound OC(=O)CCCCCCCCC(O)=O CXMXRPHRNRROMY-UHFFFAOYSA-N 0.000 description 12
- 239000002562 thickening agent Substances 0.000 description 12
- VSGNNIFQASZAOI-UHFFFAOYSA-L calcium acetate Chemical compound [Ca+2].CC([O-])=O.CC([O-])=O VSGNNIFQASZAOI-UHFFFAOYSA-L 0.000 description 11
- 239000001639 calcium acetate Substances 0.000 description 11
- 235000011092 calcium acetate Nutrition 0.000 description 11
- 229960005147 calcium acetate Drugs 0.000 description 11
- 229940095643 calcium hydroxide Drugs 0.000 description 10
- 238000005260 corrosion Methods 0.000 description 10
- 230000007797 corrosion Effects 0.000 description 10
- 239000003921 oil Substances 0.000 description 10
- 235000019198 oils Nutrition 0.000 description 10
- ULQISTXYYBZJSJ-UHFFFAOYSA-N 12-hydroxyoctadecanoic acid Chemical compound CCCCCCC(O)CCCCCCCCCCC(O)=O ULQISTXYYBZJSJ-UHFFFAOYSA-N 0.000 description 9
- 230000000694 effects Effects 0.000 description 9
- 229910052744 lithium Inorganic materials 0.000 description 9
- 238000005096 rolling process Methods 0.000 description 9
- 239000012467 final product Substances 0.000 description 8
- 238000003756 stirring Methods 0.000 description 8
- 239000003760 tallow Substances 0.000 description 8
- 239000000126 substance Substances 0.000 description 7
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
- 239000000084 colloidal system Substances 0.000 description 6
- 239000002480 mineral oil Substances 0.000 description 6
- 238000000926 separation method Methods 0.000 description 6
- 239000011734 sodium Substances 0.000 description 6
- BTBUEUYNUDRHOZ-UHFFFAOYSA-N Borate Chemical compound [O-]B([O-])[O-] BTBUEUYNUDRHOZ-UHFFFAOYSA-N 0.000 description 5
- 230000008859 change Effects 0.000 description 5
- 230000000875 corresponding effect Effects 0.000 description 5
- 150000002762 monocarboxylic acid derivatives Chemical class 0.000 description 5
- 229940114072 12-hydroxystearic acid Drugs 0.000 description 4
- WXTMDXOMEHJXQO-UHFFFAOYSA-N 2,5-dihydroxybenzoic acid Chemical compound OC(=O)C1=CC(O)=CC=C1O WXTMDXOMEHJXQO-UHFFFAOYSA-N 0.000 description 4
- 239000002253 acid Substances 0.000 description 4
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 4
- 238000003483 aging Methods 0.000 description 4
- 230000032683 aging Effects 0.000 description 4
- 125000003118 aryl group Chemical group 0.000 description 4
- 235000015278 beef Nutrition 0.000 description 4
- QYDYPVFESGNLHU-UHFFFAOYSA-N elaidic acid methyl ester Natural products CCCCCCCCC=CCCCCCCCC(=O)OC QYDYPVFESGNLHU-UHFFFAOYSA-N 0.000 description 4
- 150000004679 hydroxides Chemical class 0.000 description 4
- 229940073769 methyl oleate Drugs 0.000 description 4
- BDJRBEYXGGNYIS-UHFFFAOYSA-N nonanedioic acid Chemical compound OC(=O)CCCCCCCC(O)=O BDJRBEYXGGNYIS-UHFFFAOYSA-N 0.000 description 4
- 125000001273 sulfonato group Chemical class [O-]S(*)(=O)=O 0.000 description 4
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 4
- 229910000406 trisodium phosphate Inorganic materials 0.000 description 4
- 235000019801 trisodium phosphate Nutrition 0.000 description 4
- 239000002023 wood Substances 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 3
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 3
- 229910019142 PO4 Inorganic materials 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000001361 adipic acid Substances 0.000 description 3
- 230000003078 antioxidant effect Effects 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- RXPKHKBYUIHIGL-UHFFFAOYSA-L calcium;12-hydroxyoctadecanoate Chemical compound [Ca+2].CCCCCCC(O)CCCCCCCCCCC([O-])=O.CCCCCCC(O)CCCCCCCCCCC([O-])=O RXPKHKBYUIHIGL-UHFFFAOYSA-L 0.000 description 3
- 239000003638 chemical reducing agent Substances 0.000 description 3
- 229920001971 elastomer Polymers 0.000 description 3
- 239000003879 lubricant additive Substances 0.000 description 3
- 239000011777 magnesium Substances 0.000 description 3
- 229910052749 magnesium Inorganic materials 0.000 description 3
- 235000021317 phosphate Nutrition 0.000 description 3
- 150000003013 phosphoric acid derivatives Chemical class 0.000 description 3
- 230000003068 static effect Effects 0.000 description 3
- 150000003626 triacylglycerols Chemical class 0.000 description 3
- KGRVJHAUYBGFFP-UHFFFAOYSA-N 2,2'-Methylenebis(4-methyl-6-tert-butylphenol) Chemical compound CC(C)(C)C1=CC(C)=CC(CC=2C(=C(C=C(C)C=2)C(C)(C)C)O)=C1O KGRVJHAUYBGFFP-UHFFFAOYSA-N 0.000 description 2
- IJFXRHURBJZNAO-UHFFFAOYSA-N 3-hydroxybenzoic acid Chemical compound OC(=O)C1=CC=CC(O)=C1 IJFXRHURBJZNAO-UHFFFAOYSA-N 0.000 description 2
- FJKROLUGYXJWQN-UHFFFAOYSA-N 4-hydroxybenzoic acid Chemical compound OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 description 2
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- 239000008186 active pharmaceutical agent Substances 0.000 description 2
- 235000011037 adipic acid Nutrition 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 2
- 229910001854 alkali hydroxide Inorganic materials 0.000 description 2
- 150000008044 alkali metal hydroxides Chemical class 0.000 description 2
- 125000000217 alkyl group Chemical group 0.000 description 2
- 229910000323 aluminium silicate Inorganic materials 0.000 description 2
- 235000012216 bentonite Nutrition 0.000 description 2
- LVGQIQHJMRUCRM-UHFFFAOYSA-L calcium bisulfite Chemical compound [Ca+2].OS([O-])=O.OS([O-])=O LVGQIQHJMRUCRM-UHFFFAOYSA-L 0.000 description 2
- 235000010260 calcium hydrogen sulphite Nutrition 0.000 description 2
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 2
- 239000001913 cellulose Substances 0.000 description 2
- 229920002678 cellulose Polymers 0.000 description 2
- JMFRWRFFLBVWSI-NSCUHMNNSA-N coniferol Chemical compound COC1=CC(\C=C\CO)=CC=C1O JMFRWRFFLBVWSI-NSCUHMNNSA-N 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 238000004132 cross linking Methods 0.000 description 2
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- UKMSUNONTOPOIO-UHFFFAOYSA-N docosanoic acid Chemical compound CCCCCCCCCCCCCCCCCCCCCC(O)=O UKMSUNONTOPOIO-UHFFFAOYSA-N 0.000 description 2
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 2
- 230000006870 function Effects 0.000 description 2
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000010687 lubricating oil Substances 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 238000005649 metathesis reaction Methods 0.000 description 2
- 235000010446 mineral oil Nutrition 0.000 description 2
- 125000002293 monolignol group Chemical group 0.000 description 2
- 239000000178 monomer Substances 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- 229920003023 plastic Polymers 0.000 description 2
- 239000005060 rubber Substances 0.000 description 2
- 238000010008 shearing Methods 0.000 description 2
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 2
- 235000012239 silicon dioxide Nutrition 0.000 description 2
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Classifications
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M135/00—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing sulfur, selenium or tellurium
- C10M135/08—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing sulfur, selenium or tellurium containing a sulfur-to-oxygen bond
- C10M135/10—Sulfonic acids or derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M141/00—Lubricating compositions characterised by the additive being a mixture of two or more compounds covered by more than one of the main groups C10M125/00 - C10M139/00, each of these compounds being essential
- C10M141/08—Lubricating compositions characterised by the additive being a mixture of two or more compounds covered by more than one of the main groups C10M125/00 - C10M139/00, each of these compounds being essential at least one of them being an organic sulfur-, selenium- or tellurium-containing compound
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M159/00—Lubricating compositions characterised by the additive being of unknown or incompletely defined constitution
- C10M159/12—Reaction products
- C10M159/20—Reaction mixtures having an excess of neutralising base, e.g. so-called overbasic or highly basic products
- C10M159/24—Reaction mixtures having an excess of neutralising base, e.g. so-called overbasic or highly basic products containing sulfonic radicals
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/04—Elements
- C10M2201/041—Carbon; Graphite; Carbon black
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/06—Metal compounds
- C10M2201/065—Sulfides; Selenides; Tellurides
- C10M2201/066—Molybdenum sulfide
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/10—Carboxylix acids; Neutral salts thereof
- C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
- C10M2207/127—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids polycarboxylic
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2010/00—Metal present as such or in compounds
- C10N2010/02—Groups 1 or 11
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2010/00—Metal present as such or in compounds
- C10N2010/04—Groups 2 or 12
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/02—Pour-point; Viscosity index
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/26—Waterproofing or water resistance
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/36—Seal compatibility, e.g. with rubber
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/02—Bearings
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2050/00—Form in which the lubricant is applied to the material being lubricated
- C10N2050/10—Semi-solids; greasy
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Lubricants (AREA)
- Rolling Contact Bearings (AREA)
- Sliding-Contact Bearings (AREA)
- General Details Of Gearings (AREA)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102010006745A DE102010006745A1 (de) | 2010-02-02 | 2010-02-02 | Schmierfette enthaltend Ligninsulfonat, deren Herstellung und Verwendung |
DE102010006745.8 | 2010-02-02 | ||
PCT/DE2011/000087 WO2011095155A1 (de) | 2010-02-02 | 2011-01-31 | Schmierfette enthaltend ligninsulfonat, deren herstellung und verwendung |
Publications (2)
Publication Number | Publication Date |
---|---|
CA2788157A1 CA2788157A1 (en) | 2011-08-11 |
CA2788157C true CA2788157C (en) | 2018-06-26 |
Family
ID=43983746
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA2788157A Active CA2788157C (en) | 2010-02-02 | 2011-01-31 | Lubricating greases containing lignin sulfonate, production and use thereof |
Country Status (20)
Country | Link |
---|---|
US (1) | US20120302472A1 (de) |
EP (1) | EP2531587B9 (de) |
JP (1) | JP5856078B2 (de) |
KR (1) | KR101833854B1 (de) |
CN (1) | CN102770513B (de) |
AU (1) | AU2011212763B2 (de) |
BR (1) | BR112012019181B1 (de) |
CA (1) | CA2788157C (de) |
DE (1) | DE102010006745A1 (de) |
DK (1) | DK2531587T3 (de) |
ES (1) | ES2561821T3 (de) |
HR (1) | HRP20160072T1 (de) |
HU (1) | HUE026690T2 (de) |
MX (1) | MX2012008960A (de) |
PL (1) | PL2531587T3 (de) |
PT (1) | PT2531587E (de) |
RS (1) | RS54610B1 (de) |
RU (1) | RU2554873C2 (de) |
SI (1) | SI2531587T1 (de) |
WO (1) | WO2011095155A1 (de) |
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JPS6265910A (ja) * | 1985-09-13 | 1987-03-25 | Nippon Cement Co Ltd | 窒化けい素・炭化けい素複合粉末の製造方法 |
US8507421B2 (en) | 2010-02-02 | 2013-08-13 | Fuchs Lubricants Co. | Lubricating greases and process for their production |
CN102433189A (zh) * | 2011-10-24 | 2012-05-02 | 中国石油化工股份有限公司 | 一种复合磺酸钙基润滑脂的组合物及制备方法 |
US9222050B1 (en) * | 2012-02-29 | 2015-12-29 | Rand Innovations, Llc | Lubricant composition, method of preparing the same, and firearm cleaner including the same |
JP5659390B2 (ja) * | 2012-09-21 | 2015-01-28 | 住鉱潤滑剤株式会社 | 潤滑剤組成物 |
JP5704574B2 (ja) * | 2012-09-24 | 2015-04-22 | 住鉱潤滑剤株式会社 | 潤滑剤組成物 |
US9228151B1 (en) * | 2012-11-07 | 2016-01-05 | Rand Innovations, Llc | Lubricant additive composition, lubricant, and method of preparing the same |
JP5916654B2 (ja) * | 2013-03-28 | 2016-05-11 | 住鉱潤滑剤株式会社 | 等速ジョイント用グリース組成物、並びに等速ジョイント |
JP5889823B2 (ja) * | 2013-03-28 | 2016-03-22 | 住鉱潤滑剤株式会社 | 等速ジョイント用グリース組成物、並びに等速ジョイント |
JP6051097B2 (ja) * | 2013-04-26 | 2016-12-27 | 出光興産株式会社 | グリースの製造方法 |
US20160145522A1 (en) * | 2013-06-12 | 2016-05-26 | Nsk Ltd. | Grease composition and rolling bearing |
US9765821B2 (en) * | 2013-07-19 | 2017-09-19 | Ntn Corporation | Rolling bearing |
CA2922387C (en) * | 2013-09-02 | 2017-09-26 | Nippon Steel & Sumitomo Metal Corporation | Lubricant film-forming composition and screw joint for steel pipe |
JP6223863B2 (ja) * | 2014-02-27 | 2017-11-01 | 昭和シェル石油株式会社 | グリース組成物 |
JP6274435B2 (ja) * | 2014-09-22 | 2018-02-07 | 住鉱潤滑剤株式会社 | 潤滑剤組成物 |
WO2016124653A1 (en) * | 2015-02-06 | 2016-08-11 | Shell Internationale Research Maatschappij B.V. | Grease composition |
CN107250328B (zh) * | 2015-02-11 | 2021-05-07 | 国际壳牌研究有限公司 | 润滑脂组合物 |
DE102015103440A1 (de) * | 2015-03-09 | 2016-09-15 | Fuchs Petrolub Se | Verfahren zur Herstellung von Polyharnstoff-verdickten Schmierfetten auf Basis von Lignin-Derivaten, derartige Schmierfette und deren Verwendung |
JP6903677B2 (ja) | 2015-11-04 | 2021-07-14 | ヘンケル・アクチェンゲゼルシャフト・ウント・コムパニー・コマンディットゲゼルシャフト・アウフ・アクチェンHenkel AG & Co. KGaA | 脂肪酸および脂肪酸グリセリドに基づく粉末潤滑剤ならびにその使用 |
EP3165589A1 (de) | 2015-11-04 | 2017-05-10 | Henkel AG & Co. KGaA | Pulverförmiges schmiermittel auf basis von zinksalzen von fettsäuren und verwendung davon |
CN105419912A (zh) * | 2015-11-27 | 2016-03-23 | 蚌埠海明压铸机有限公司 | 一种抗磨润滑油 |
CN105441166A (zh) * | 2015-11-27 | 2016-03-30 | 蚌埠海明压铸机有限公司 | 一种发动机用润滑油 |
CN105441167A (zh) * | 2015-11-27 | 2016-03-30 | 蚌埠海明压铸机有限公司 | 一种抗氧抗腐润滑油 |
CN105441165A (zh) * | 2015-11-27 | 2016-03-30 | 蚌埠海明压铸机有限公司 | 一种耐用发动机用润滑油 |
CN105441169A (zh) * | 2015-11-30 | 2016-03-30 | 蚌埠市华科机电有限责任公司 | 一种抗磨发动机用润滑油 |
CN105441170A (zh) * | 2015-11-30 | 2016-03-30 | 蚌埠市华科机电有限责任公司 | 一种防锈型润滑油 |
JP2016084483A (ja) * | 2016-02-16 | 2016-05-19 | 住鉱潤滑剤株式会社 | グリース組成物、並びに等速ジョイント |
JP2016130318A (ja) * | 2016-03-16 | 2016-07-21 | 住鉱潤滑剤株式会社 | グリース組成物、並びに等速ジョイント |
CN107236581A (zh) * | 2017-07-06 | 2017-10-10 | 广西柳工机械股份有限公司 | 高性能石墨烯复合润滑脂 |
US10626343B1 (en) * | 2017-11-17 | 2020-04-21 | Brave Response Shooting, LLC | Animal-based hydrocarbon firearm lubricant |
CN108531248A (zh) * | 2018-06-05 | 2018-09-14 | 朱东洋 | 一种耐磨抗硬化润滑脂的制备方法 |
DE102018008362A1 (de) * | 2018-07-09 | 2020-01-09 | Klüber Lubrication München Se & Co. Kg | Umweltverträgliches Schmierfett für Stahlseile |
RU2688928C1 (ru) * | 2018-10-01 | 2019-05-23 | Федеральное государственное бюджетное образовательное учреждение высшего образования Иркутский государственный университет путей сообщения (ФГБОУ ВО ИрГУПС) | Способ получения противозадирной присадки для тяжелонагруженных узлов трения |
CN109825345B (zh) * | 2019-02-19 | 2021-12-24 | 上海金兆节能科技有限公司 | 耐高温润滑剂及其制备方法 |
RU2698457C1 (ru) * | 2019-06-21 | 2019-08-27 | Публичное акционерное общество "НК "Роснефть" - МЗ "Нефтепродукт" | Многоцелевая комплексная пластичная смазка |
DE102020008047A1 (de) | 2020-07-03 | 2022-01-05 | Fuchs Petrolub Se | Polyharnstoff-Schmierfette enthaltend Carbonate und deren Verwendung |
DE102020117671B4 (de) | 2020-07-03 | 2022-06-09 | Fuchs Petrolub Se | Schmierstellen aufweisend eine Polyharnstoff-Schmierfett-Zusammensetzung und eine Dichtung umfassend ein Dichtmaterial aus fluorierten Elastomeren und die Verwendung der Polyharnstoff-Schmierfett-Zusammensetzung für eine Schmierstelle umfassend eine derartige Dichtung |
CN112410101A (zh) * | 2020-11-30 | 2021-02-26 | 新乡市恒星科技有限责任公司 | 一种精密高分子特种润滑脂及其制备方法 |
CN113122354B (zh) * | 2021-04-20 | 2023-08-15 | 中国石油化工股份有限公司 | 一种复合钙基润滑脂及其制备方法 |
CN113355148B (zh) * | 2021-05-28 | 2022-12-20 | 中国石油化工股份有限公司 | 一种用于汽车驱动轴轮毂轴承结合面的润滑剂及其制法 |
CN113403127A (zh) * | 2021-06-08 | 2021-09-17 | 郑州市欧普士科技有限公司 | 一种用于架空导线的环保型防腐脂及其制备方法 |
DE102021133469B3 (de) | 2021-12-16 | 2022-08-25 | Fuchs Petrolub Se | Verfahren zur Herstellung von Lithiumkomplexseifen- und Lithium-Calciumkomplexseifen-Schmierfetten |
CN114540106A (zh) * | 2022-03-02 | 2022-05-27 | 北京市政建设集团有限责任公司 | 一种用于盾构机主轴承的密封油脂及其制备方法 |
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US2976242A (en) * | 1955-04-01 | 1961-03-21 | Exxon Research Engineering Co | Lubricating grease compositions |
US3249537A (en) * | 1963-05-16 | 1966-05-03 | Exxon Research Engineering Co | Lignosulfonate lubricants |
US4409112A (en) * | 1981-12-23 | 1983-10-11 | Dresser Industries, Inc. | Lubricant, slow speed, high load |
CA2027241A1 (en) * | 1989-10-24 | 1991-04-25 | Andrew B. Law | Stabilized metal salt/3-isothiazolone combinations |
JPH11131086A (ja) * | 1997-10-28 | 1999-05-18 | Nippon Koyu:Kk | 潤滑グリ−ス組成物 |
RU2224011C1 (ru) * | 2002-12-02 | 2004-02-20 | Федеральное государственное унитарное предприятие "Московское машиностроительное производственное предприятие "Салют" | Смазка для заготовок при горячей или полугорячей обработке металлов давлением |
CN100404655C (zh) * | 2003-11-13 | 2008-07-23 | 中国石油化工股份有限公司 | 复合锂基润滑脂及其制备方法 |
CN100549147C (zh) * | 2006-07-31 | 2009-10-14 | 中国石油化工股份有限公司 | 润滑脂组合物 |
JP5101374B2 (ja) * | 2008-04-02 | 2012-12-19 | 中央油化株式会社 | カルシウムコンプレックスグリース |
-
2010
- 2010-02-02 DE DE102010006745A patent/DE102010006745A1/de not_active Ceased
-
2011
- 2011-01-31 EP EP11711018.9A patent/EP2531587B9/de active Active
- 2011-01-31 US US13/576,857 patent/US20120302472A1/en not_active Abandoned
- 2011-01-31 HU HUE11711018A patent/HUE026690T2/en unknown
- 2011-01-31 CA CA2788157A patent/CA2788157C/en active Active
- 2011-01-31 KR KR1020127023089A patent/KR101833854B1/ko active IP Right Grant
- 2011-01-31 SI SI201130721T patent/SI2531587T1/sl unknown
- 2011-01-31 ES ES11711018.9T patent/ES2561821T3/es active Active
- 2011-01-31 PL PL11711018T patent/PL2531587T3/pl unknown
- 2011-01-31 BR BR112012019181A patent/BR112012019181B1/pt active IP Right Grant
- 2011-01-31 DK DK11711018.9T patent/DK2531587T3/en active
- 2011-01-31 PT PT117110189T patent/PT2531587E/pt unknown
- 2011-01-31 JP JP2012550318A patent/JP5856078B2/ja active Active
- 2011-01-31 AU AU2011212763A patent/AU2011212763B2/en not_active Ceased
- 2011-01-31 RS RS20160037A patent/RS54610B1/en unknown
- 2011-01-31 CN CN201180008171.3A patent/CN102770513B/zh active Active
- 2011-01-31 MX MX2012008960A patent/MX2012008960A/es active IP Right Grant
- 2011-01-31 WO PCT/DE2011/000087 patent/WO2011095155A1/de active Application Filing
- 2011-01-31 RU RU2012136909/04A patent/RU2554873C2/ru active
-
2016
- 2016-01-22 HR HRP20160072TT patent/HRP20160072T1/hr unknown
Also Published As
Publication number | Publication date |
---|---|
WO2011095155A1 (de) | 2011-08-11 |
BR112012019181B1 (pt) | 2018-09-11 |
RU2554873C2 (ru) | 2015-06-27 |
AU2011212763B2 (en) | 2013-10-17 |
RS54610B1 (en) | 2016-08-31 |
DK2531587T3 (en) | 2016-01-25 |
BR112012019181A2 (pt) | 2018-03-27 |
CA2788157A1 (en) | 2011-08-11 |
CN102770513B (zh) | 2015-09-30 |
US20120302472A1 (en) | 2012-11-29 |
HUE026690T2 (en) | 2016-07-28 |
PT2531587E (pt) | 2016-02-26 |
JP5856078B2 (ja) | 2016-02-09 |
ES2561821T3 (es) | 2016-03-01 |
DE102010006745A1 (de) | 2011-08-04 |
JP2013518929A (ja) | 2013-05-23 |
KR101833854B1 (ko) | 2018-03-05 |
AU2011212763A1 (en) | 2012-09-06 |
PL2531587T3 (pl) | 2016-06-30 |
HRP20160072T1 (hr) | 2016-04-08 |
EP2531587B9 (de) | 2016-10-05 |
EP2531587B1 (de) | 2015-11-04 |
SI2531587T1 (sl) | 2016-04-29 |
KR20120139730A (ko) | 2012-12-27 |
EP2531587A1 (de) | 2012-12-12 |
RU2012136909A (ru) | 2014-03-10 |
MX2012008960A (es) | 2012-10-15 |
CN102770513A (zh) | 2012-11-07 |
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