AU2014268860B2 - Method for the purification of acetic acid and acrylic acid - Google Patents

Method for the purification of acetic acid and acrylic acid Download PDF

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Publication number
AU2014268860B2
AU2014268860B2 AU2014268860A AU2014268860A AU2014268860B2 AU 2014268860 B2 AU2014268860 B2 AU 2014268860B2 AU 2014268860 A AU2014268860 A AU 2014268860A AU 2014268860 A AU2014268860 A AU 2014268860A AU 2014268860 B2 AU2014268860 B2 AU 2014268860B2
Authority
AU
Australia
Prior art keywords
boiling solvent
crude product
acetic acid
acrylic acid
mixture
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
AU2014268860A
Other languages
English (en)
Other versions
AU2014268860A1 (en
Inventor
Faisal BAKSH
Mubarik BASHIR
Mustapha N. KARIME
Zeeshan NAWAZ
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Saudi Basic Industries Corp
Original Assignee
Saudi Basic Industries Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Saudi Basic Industries Corp filed Critical Saudi Basic Industries Corp
Publication of AU2014268860A1 publication Critical patent/AU2014268860A1/en
Application granted granted Critical
Publication of AU2014268860B2 publication Critical patent/AU2014268860B2/en
Ceased legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/215—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of saturated hydrocarbyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C07C51/46—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation by azeotropic distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
AU2014268860A 2013-05-20 2014-05-19 Method for the purification of acetic acid and acrylic acid Ceased AU2014268860B2 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201361825205P 2013-05-20 2013-05-20
US61/825,205 2013-05-20
PCT/US2014/038573 WO2014189829A1 (en) 2013-05-20 2014-05-19 Method for the purification of acetic acid and acrylic acid

Publications (2)

Publication Number Publication Date
AU2014268860A1 AU2014268860A1 (en) 2015-10-22
AU2014268860B2 true AU2014268860B2 (en) 2017-02-02

Family

ID=50942932

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2014268860A Ceased AU2014268860B2 (en) 2013-05-20 2014-05-19 Method for the purification of acetic acid and acrylic acid

Country Status (8)

Country Link
US (1) US9944582B2 (enExample)
EP (1) EP2999686A1 (enExample)
JP (1) JP2016520096A (enExample)
KR (1) KR20160009598A (enExample)
CN (1) CN105263895B (enExample)
AU (1) AU2014268860B2 (enExample)
CA (1) CA2908710A1 (enExample)
WO (1) WO2014189829A1 (enExample)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10239815B2 (en) 2015-02-05 2019-03-26 Nippon Shokubai Co., Ltd. Method for producing acrylic acid
WO2017114831A1 (en) * 2015-12-29 2017-07-06 Shell Internationale Research Maatschappij B.V. Process for converting alkanes and/or alkenes to alkenes and carboxylic acids
KR102079775B1 (ko) * 2016-11-25 2020-02-20 주식회사 엘지화학 (메트)아크릴산의 연속 회수 방법 및 장치
FR3060000B1 (fr) * 2016-12-08 2020-05-01 Arkema France Procede pour eviter le depot de polymeres dans un procede de purification d'acide (meth)acrylique.

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US3666632A (en) * 1968-10-08 1972-05-30 Asahi Chemical Ind Method for the separation of acrylic acid from aqueous solution containing acrylic acid and acetic acid
EP0551111A1 (en) * 1992-01-09 1993-07-14 Nippon Shokubai Co., Ltd. Process for purifying acrylic acid to high purity in the production of acrylic acid
EP0861820A2 (en) * 1997-02-28 1998-09-02 Nippon Shokubai Co., Ltd. Method for recovering acrylic acid

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US2862958A (en) 1955-10-13 1958-12-02 Hercules Powder Co Ltd Method of improving electrical properties of plasticizers by treatment with magnesium silicate
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JPS62267341A (ja) 1986-05-16 1987-11-20 Mitsubishi Kasei Vinyl Co 可塑剤の製造法
JPH0341051A (ja) 1989-07-07 1991-02-21 Idemitsu Petrochem Co Ltd アクリル酸エステル又はメタクリル酸エステルの製造方法
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JPH089567B2 (ja) 1992-01-09 1996-01-31 株式会社日本触媒 アクリル酸製造においてアクリル酸を高純度に精製する方法
JP3832868B2 (ja) 1994-07-27 2006-10-11 三菱化学株式会社 アクリル酸の精製法
JP3937462B2 (ja) 1994-08-04 2007-06-27 三菱化学株式会社 アクリル酸精製法
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JP3219682B2 (ja) * 1995-09-29 2001-10-15 昭和電工株式会社 酢酸の精製方法、及び酢酸の製造方法
JP3028925B2 (ja) 1995-12-05 2000-04-04 株式会社日本触媒 アクリル酸の製造方法
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US6114278A (en) 1998-11-16 2000-09-05 Saudi Basic Industries Corporation Catalysts for catalytic oxidation of propane to acrylic acid, methods of making and using the same
DE60005870T2 (de) 1999-03-05 2004-08-19 Rohm And Haas Co. Verfahren zur Herstellung von Acrylsäure
JP5073129B2 (ja) * 1999-03-31 2012-11-14 株式会社日本触媒 （メタ）アクリル酸の精製方法
JP4809532B2 (ja) 1999-11-15 2011-11-09 サウディ ベーシック インダストリーズ コーポレイション プロパンのアクリル酸への接触酸化用触媒、その製造法及び使用法
CN1209332C (zh) * 2000-06-14 2005-07-06 巴斯福股份公司 丙烯醛和/或丙烯酸的制备方法
JP2005232008A (ja) 2001-12-27 2005-09-02 Mitsubishi Chemicals Corp （メタ）アクリル酸の蒸留方法
WO2003064367A1 (en) * 2002-01-29 2003-08-07 Mitsubishi Chemical Corporation Process for production of (meth)acrylic acid
GB0320206D0 (en) 2003-08-29 2003-10-01 Exxonmobil Chem Patents Inc Improvements in or relating to plasticiser
FR2861724B1 (fr) 2003-11-04 2005-12-30 Arkema Procede de purification de l'acide (meth)acrylique obtenu par oxydation d'un substrat gazeux
AU2004293259A1 (en) * 2003-11-28 2005-06-09 Mitsubishi Chemical Corporation Method of purifying (meth)acrylic acid
JP2005179352A (ja) 2003-11-28 2005-07-07 Mitsubishi Chemicals Corp （メタ）アクリル酸の精製方法
JP4333471B2 (ja) 2004-05-11 2009-09-16 新日本理化株式会社 ジカルボン酸ジエステルの製造方法
JP4621174B2 (ja) 2006-06-19 2011-01-26 株式会社日本触媒 （メタ）アクリル酸および／またはそのエステルの蒸留方法
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Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3422831A (en) * 1967-02-20 1969-01-21 Gen Electric Turbine control system
US3666632A (en) * 1968-10-08 1972-05-30 Asahi Chemical Ind Method for the separation of acrylic acid from aqueous solution containing acrylic acid and acetic acid
EP0551111A1 (en) * 1992-01-09 1993-07-14 Nippon Shokubai Co., Ltd. Process for purifying acrylic acid to high purity in the production of acrylic acid
EP0861820A2 (en) * 1997-02-28 1998-09-02 Nippon Shokubai Co., Ltd. Method for recovering acrylic acid

Also Published As

Publication number Publication date
WO2014189829A1 (en) 2014-11-27
AU2014268860A1 (en) 2015-10-22
CN105263895B (zh) 2018-04-10
US9944582B2 (en) 2018-04-17
JP2016520096A (ja) 2016-07-11
KR20160009598A (ko) 2016-01-26
CN105263895A (zh) 2016-01-20
CA2908710A1 (en) 2014-11-27
US20160075630A1 (en) 2016-03-17
EP2999686A1 (en) 2016-03-30

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MK14 Patent ceased section 143(a) (annual fees not paid) or expired