WO2014196435A1 - Vernis, film polyimide poreux produit à l'aide dudit vernis, et procédé de production dudit film - Google Patents

Vernis, film polyimide poreux produit à l'aide dudit vernis, et procédé de production dudit film Download PDF

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Publication number
WO2014196435A1
WO2014196435A1 PCT/JP2014/064164 JP2014064164W WO2014196435A1 WO 2014196435 A1 WO2014196435 A1 WO 2014196435A1 JP 2014064164 W JP2014064164 W JP 2014064164W WO 2014196435 A1 WO2014196435 A1 WO 2014196435A1
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polyimide
film
resin fine
fine particles
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PCT/JP2014/064164
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English (en)
Japanese (ja)
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司 菅原
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東京応化工業株式会社
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Priority to JP2015521408A priority Critical patent/JP6342891B2/ja
Publication of WO2014196435A1 publication Critical patent/WO2014196435A1/fr

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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D179/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing nitrogen, with or without oxygen, or carbon only, not provided for in groups C09D161/00 - C09D177/00
    • C09D179/04—Polycondensates having nitrogen-containing heterocyclic rings in the main chain; Polyhydrazides; Polyamide acids or similar polyimide precursors
    • C09D179/08—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M50/00—Constructional details or processes of manufacture of the non-active parts of electrochemical cells other than fuel cells, e.g. hybrid cells
    • H01M50/40—Separators; Membranes; Diaphragms; Spacing elements inside cells
    • H01M50/409—Separators, membranes or diaphragms characterised by the material
    • H01M50/411—Organic material
    • H01M50/414—Synthetic resins, e.g. thermoplastics or thermosetting resins
    • H01M50/423—Polyamide resins
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D71/00—Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
    • B01D71/06—Organic material
    • B01D71/58—Other polymers having nitrogen in the main chain, with or without oxygen or carbon only
    • B01D71/62—Polycondensates having nitrogen-containing heterocyclic rings in the main chain
    • B01D71/64—Polyimides; Polyamide-imides; Polyester-imides; Polyamide acids or similar polyimide precursors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D71/00—Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
    • B01D71/06—Organic material
    • B01D71/58—Other polymers having nitrogen in the main chain, with or without oxygen or carbon only
    • B01D71/62—Polycondensates having nitrogen-containing heterocyclic rings in the main chain
    • B01D71/64—Polyimides; Polyamide-imides; Polyester-imides; Polyamide acids or similar polyimide precursors
    • B01D71/641—Polyamide-imides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
    • C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C08G73/1003—Preparatory processes
    • C08G73/1007—Preparatory processes from tetracarboxylic acids or derivatives and diamines
    • C08G73/1021—Preparatory processes from tetracarboxylic acids or derivatives and diamines characterised by the catalyst used
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
    • C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C08G73/1046—Polyimides containing oxygen in the form of ether bonds in the main chain
    • C08G73/105—Polyimides containing oxygen in the form of ether bonds in the main chain with oxygen only in the diamino moiety
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
    • C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C08G73/1067—Wholly aromatic polyimides, i.e. having both tetracarboxylic and diamino moieties aromatically bound
    • C08G73/1071—Wholly aromatic polyimides containing oxygen in the form of ether bonds in the main chain
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M50/00—Constructional details or processes of manufacture of the non-active parts of electrochemical cells other than fuel cells, e.g. hybrid cells
    • H01M50/40—Separators; Membranes; Diaphragms; Spacing elements inside cells
    • H01M50/409—Separators, membranes or diaphragms characterised by the material
    • H01M50/411—Organic material
    • H01M50/414—Synthetic resins, e.g. thermoplastics or thermosetting resins
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F220/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
    • C08F220/02—Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
    • C08F220/52—Amides or imides
    • C08F220/54—Amides, e.g. N,N-dimethylacrylamide or N-isopropylacrylamide
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
    • C09D133/24—Homopolymers or copolymers of amides or imides
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M8/00—Fuel cells; Manufacture thereof
    • H01M8/10—Fuel cells with solid electrolytes
    • H01M8/1016—Fuel cells with solid electrolytes characterised by the electrolyte material
    • H01M8/1018—Polymeric electrolyte materials
    • H01M8/102—Polymeric electrolyte materials characterised by the chemical structure of the main chain of the ion-conducting polymer
    • H01M8/1027—Polymeric electrolyte materials characterised by the chemical structure of the main chain of the ion-conducting polymer having carbon, oxygen and other atoms, e.g. sulfonated polyethersulfones [S-PES]
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M8/00—Fuel cells; Manufacture thereof
    • H01M8/10—Fuel cells with solid electrolytes
    • H01M8/1016—Fuel cells with solid electrolytes characterised by the electrolyte material
    • H01M8/1018—Polymeric electrolyte materials
    • H01M8/102—Polymeric electrolyte materials characterised by the chemical structure of the main chain of the ion-conducting polymer
    • H01M8/103—Polymeric electrolyte materials characterised by the chemical structure of the main chain of the ion-conducting polymer having nitrogen, e.g. sulfonated polybenzimidazoles [S-PBI], polybenzimidazoles with phosphoric acid, sulfonated polyamides [S-PA] or sulfonated polyphosphazenes [S-PPh]
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30—Hydrogen technology
    • Y02E60/50—Fuel cells
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/50—Manufacturing or production processes characterised by the final manufactured product

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

L'objet de la présente invention est de fournir un procédé de production permettant de produire un film polyimide poreux homogène et très dense et un séparateur équipé dudit film polyimide poreux en éliminant les microparticules de résine d'un film polyimide contenant les microparticules de résine par décomposition thermique. Un procédé de production d'un film polyimide poreux selon la présente invention comprend : une étape de cuisson consistant à cuire un film composite non cuit comprenant un acide polyamique ou un polyimide, des microparticules de résine et un agent de condensation à une température qui est inférieure à la température de décomposition des microparticules de résine afin de produire un film composite polyimide-(microparticules de résine); et une étape d'élimination des microparticules consistant à éliminer les microparticules de résine dudit film composite polyimide-(microparticules de résine).
PCT/JP2014/064164 2013-06-07 2014-05-28 Vernis, film polyimide poreux produit à l'aide dudit vernis, et procédé de production dudit film WO2014196435A1 (fr)

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JP2015521408A JP6342891B2 (ja) 2013-06-07 2014-05-28 ワニス、それを用いて製造した多孔質ポリイミド膜、及びその製造方法

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JP2013120410 2013-06-07
JP2013-120410 2013-06-07

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2016104309A1 (fr) * 2014-12-24 2016-06-30 ユニチカ株式会社 Film de polyimide poreux et son procédé de production
US20160279883A1 (en) * 2015-03-26 2016-09-29 Fuji Xerox Co., Ltd. Method for producing porous polyimide film, and porous polyimide film
JP2016183333A (ja) * 2015-03-26 2016-10-20 富士ゼロックス株式会社 樹脂粒子分散ポリイミド前駆体溶液の製造方法、樹脂粒子分散ポリイミド前駆体溶液、樹脂粒子含有ポリイミドフィルム、多孔質ポリイミドフィルムの製造方法、及び多孔質ポリイミドフィルム
JP2019011383A (ja) * 2017-06-29 2019-01-24 富士ゼロックス株式会社 ポリイミド前駆体溶液、多孔質ポリイミドフィルムの製造方法、及び多孔質ポリイミドフィルム
JP2020152922A (ja) * 2020-06-24 2020-09-24 東京応化工業株式会社 微粒子含有組成物
JPWO2019182113A1 (ja) * 2018-03-23 2021-04-08 積水化成品工業株式会社 ビニル系樹脂粒子及びその製造方法
US11958922B2 (en) 2018-09-11 2024-04-16 Sekisui Plastics Co., Ltd. Vinyl-based resin particles and method for producing same

Citations (7)

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JP2002356577A (ja) * 2001-03-15 2002-12-13 Sumitomo Bakelite Co Ltd 多孔質絶縁膜用樹脂、多孔質絶縁膜およびその製造方法
JP2003165905A (ja) * 2001-11-29 2003-06-10 Du Pont Toray Co Ltd 芳香族ポリイミドフィルム、製造方法及びその用途
JP2004026954A (ja) * 2002-06-24 2004-01-29 Mitsubishi Chemicals Corp 多孔質材料の製造方法及び多孔質材料
JP2010024385A (ja) * 2008-07-22 2010-02-04 Sekisui Chem Co Ltd 多孔質樹脂フィルムの製造方法、多孔質樹脂フィルム及び電池用セパレータ
JP2010043134A (ja) * 2008-08-08 2010-02-25 Nitto Denko Corp ポリイミド管状体及びその製造方法
JP2011012207A (ja) * 2009-07-03 2011-01-20 Mitsui Chemicals Inc 樹脂組成物、樹脂組成物の製造方法、多孔質ポリマーの製造方法、多孔質ポリマー
WO2012169383A1 (fr) * 2011-06-06 2012-12-13 日東電工株式会社 Corps poreux de polyimide, et procédé de fabrication de celui-ci

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002356577A (ja) * 2001-03-15 2002-12-13 Sumitomo Bakelite Co Ltd 多孔質絶縁膜用樹脂、多孔質絶縁膜およびその製造方法
JP2003165905A (ja) * 2001-11-29 2003-06-10 Du Pont Toray Co Ltd 芳香族ポリイミドフィルム、製造方法及びその用途
JP2004026954A (ja) * 2002-06-24 2004-01-29 Mitsubishi Chemicals Corp 多孔質材料の製造方法及び多孔質材料
JP2010024385A (ja) * 2008-07-22 2010-02-04 Sekisui Chem Co Ltd 多孔質樹脂フィルムの製造方法、多孔質樹脂フィルム及び電池用セパレータ
JP2010043134A (ja) * 2008-08-08 2010-02-25 Nitto Denko Corp ポリイミド管状体及びその製造方法
JP2011012207A (ja) * 2009-07-03 2011-01-20 Mitsui Chemicals Inc 樹脂組成物、樹脂組成物の製造方法、多孔質ポリマーの製造方法、多孔質ポリマー
WO2012169383A1 (fr) * 2011-06-06 2012-12-13 日東電工株式会社 Corps poreux de polyimide, et procédé de fabrication de celui-ci

Cited By (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5944613B1 (ja) * 2014-12-24 2016-07-05 ユニチカ株式会社 多孔質ポリイミドフィルムおよびその製造方法
CN107001681A (zh) * 2014-12-24 2017-08-01 尤尼吉可株式会社 多孔聚酰亚胺膜及其制造方法
CN107001681B (zh) * 2014-12-24 2018-10-12 尤尼吉可株式会社 多孔聚酰亚胺膜及其制造方法
WO2016104309A1 (fr) * 2014-12-24 2016-06-30 ユニチカ株式会社 Film de polyimide poreux et son procédé de production
CN106009007B (zh) * 2015-03-26 2020-09-11 富士施乐株式会社 多孔聚酰亚胺膜的制造方法和多孔聚酰亚胺膜
US20160279883A1 (en) * 2015-03-26 2016-09-29 Fuji Xerox Co., Ltd. Method for producing porous polyimide film, and porous polyimide film
CN106009007A (zh) * 2015-03-26 2016-10-12 富士施乐株式会社 多孔聚酰亚胺膜的制造方法和多孔聚酰亚胺膜
JP2016183333A (ja) * 2015-03-26 2016-10-20 富士ゼロックス株式会社 樹脂粒子分散ポリイミド前駆体溶液の製造方法、樹脂粒子分散ポリイミド前駆体溶液、樹脂粒子含有ポリイミドフィルム、多孔質ポリイミドフィルムの製造方法、及び多孔質ポリイミドフィルム
US9707722B2 (en) * 2015-03-26 2017-07-18 Fuji Xerox Co., Ltd. Method for producing porous polyimide film, and porous polyimide film
US10195794B2 (en) 2015-03-26 2019-02-05 Fuji Xerox Co., Ltd. Method for producing porous polyimide film, and porous polyimide film
JP2020109189A (ja) * 2015-03-26 2020-07-16 富士ゼロックス株式会社 樹脂粒子分散ポリイミド前駆体溶液の製造方法、樹脂粒子分散ポリイミド前駆体溶液、樹脂粒子含有ポリイミドフィルム、多孔質ポリイミドフィルムの製造方法、及び多孔質ポリイミドフィルム
JP2019011383A (ja) * 2017-06-29 2019-01-24 富士ゼロックス株式会社 ポリイミド前駆体溶液、多孔質ポリイミドフィルムの製造方法、及び多孔質ポリイミドフィルム
JPWO2019182113A1 (ja) * 2018-03-23 2021-04-08 積水化成品工業株式会社 ビニル系樹脂粒子及びその製造方法
JP7263318B2 (ja) 2018-03-23 2023-04-24 積水化成品工業株式会社 ビニル系樹脂粒子及びその製造方法
US11958922B2 (en) 2018-09-11 2024-04-16 Sekisui Plastics Co., Ltd. Vinyl-based resin particles and method for producing same
JP2020152922A (ja) * 2020-06-24 2020-09-24 東京応化工業株式会社 微粒子含有組成物

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TWI636076B (zh) 2018-09-21
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TW201509999A (zh) 2015-03-16

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