UA79242C2 - Spirocyclic 3-phenyl-3-substituted 4-ketolactams and 4-ketolactones, process for preparation thereof (variants) - Google Patents

Info

Publication number

UA79242C2

UA79242C2 UA20040403052A UA20040403052A UA79242C2 UA 79242 C2 UA79242 C2 UA 79242C2 UA 20040403052 A UA20040403052 A UA 20040403052A UA 20040403052 A UA20040403052 A UA 20040403052A UA 79242 C2 UA79242 C2 UA 79242C2

Authority

UA

Ukraine

Prior art keywords

chlorine

methyl

hydrogen

alkyl

bromine

Prior art date

2001-09-24

Links

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• 238000000034 method Methods 0.000 title claims abstract description 33
• 238000002360 preparation method Methods 0.000 title description 18
• 230000008569 process Effects 0.000 title description 3
• -1 methoxy, ethoxy Chemical group 0.000 claims description 197
• 229910052739 hydrogen Inorganic materials 0.000 claims description 123
• 239000001257 hydrogen Substances 0.000 claims description 123
• ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 121
• 239000000460 chlorine Substances 0.000 claims description 121
• 229910052801 chlorine Inorganic materials 0.000 claims description 121
• 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 100
• 150000001875 compounds Chemical class 0.000 claims description 91
• 150000002431 hydrogen Chemical class 0.000 claims description 90
• WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 claims description 67
• GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 claims description 67
• 229910052794 bromium Inorganic materials 0.000 claims description 67
• 239000002904 solvent Substances 0.000 claims description 63
• 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims description 54
• 229910052736 halogen Inorganic materials 0.000 claims description 52
• 150000002367 halogens Chemical class 0.000 claims description 52
• UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 33
• 125000004093 cyano group Chemical group *C#N 0.000 claims description 30
• 125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 claims description 29
• 229910052760 oxygen Inorganic materials 0.000 claims description 29
• 229910052731 fluorine Inorganic materials 0.000 claims description 28
• 239000011737 fluorine Substances 0.000 claims description 27
• PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 claims description 26
• QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 23
• 239000003795 chemical substances by application Substances 0.000 claims description 23
• 239000001301 oxygen Substances 0.000 claims description 23
• 125000002023 trifluoromethyl group Chemical group FC(F)(F)* 0.000 claims description 19
• 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 18
• 125000000217 alkyl group Chemical group 0.000 claims description 15
• 125000000956 methoxy group Chemical group [H]C([H])([H])O* 0.000 claims description 11
• 229910052796 boron Inorganic materials 0.000 claims description 10
• 125000000876 trifluoromethoxy group Chemical group FC(F)(F)O* 0.000 claims description 8
• GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 6
• 230000003993 interaction Effects 0.000 claims description 6
• 125000004786 difluoromethoxy group Chemical group [H]C(F)(F)O* 0.000 claims description 4
• 239000003999 initiator Substances 0.000 claims description 4
• 230000002140 halogenating effect Effects 0.000 claims description 3
• 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 claims description 3
• 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 2
• 125000000959 isobutyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])* 0.000 claims description 2
• 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 claims description 2
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