TW483997B - Multilayer composite pipe, fluid conduit system using multilayer composite pipe and method of making the composite pipe - Google Patents
Multilayer composite pipe, fluid conduit system using multilayer composite pipe and method of making the composite pipe Download PDFInfo
- Publication number
- TW483997B TW483997B TW088108394A TW88108394A TW483997B TW 483997 B TW483997 B TW 483997B TW 088108394 A TW088108394 A TW 088108394A TW 88108394 A TW88108394 A TW 88108394A TW 483997 B TW483997 B TW 483997B
- Authority
- TW
- Taiwan
- Prior art keywords
- layer
- composite pipe
- tube
- calendar
- adhesive
- Prior art date
Links
- 239000002131 composite material Substances 0.000 title claims abstract description 115
- 239000012530 fluid Substances 0.000 title claims abstract description 18
- 238000004519 manufacturing process Methods 0.000 title claims description 11
- 239000000853 adhesive Substances 0.000 claims abstract description 67
- 230000001070 adhesive effect Effects 0.000 claims abstract description 67
- 229920001169 thermoplastic Polymers 0.000 claims abstract description 35
- 239000004416 thermosoftening plastic Substances 0.000 claims abstract description 27
- 239000012815 thermoplastic material Substances 0.000 claims abstract description 10
- 239000010410 layer Substances 0.000 claims description 153
- 229910052751 metal Inorganic materials 0.000 claims description 72
- 239000002184 metal Substances 0.000 claims description 72
- 239000000463 material Substances 0.000 claims description 33
- 229920003023 plastic Polymers 0.000 claims description 31
- 239000004033 plastic Substances 0.000 claims description 31
- 239000004801 Chlorinated PVC Substances 0.000 claims description 28
- 229920000457 chlorinated polyvinyl chloride Polymers 0.000 claims description 28
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 23
- 229910052782 aluminium Inorganic materials 0.000 claims description 22
- 238000000034 method Methods 0.000 claims description 17
- 239000012790 adhesive layer Substances 0.000 claims description 16
- 229920000915 polyvinyl chloride Polymers 0.000 claims description 10
- 239000004800 polyvinyl chloride Substances 0.000 claims description 10
- 230000002079 cooperative effect Effects 0.000 claims description 9
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 claims description 8
- 239000010931 gold Substances 0.000 claims description 8
- 229910052737 gold Inorganic materials 0.000 claims description 8
- 239000012943 hotmelt Substances 0.000 claims description 6
- 229910000838 Al alloy Inorganic materials 0.000 claims description 3
- 238000004026 adhesive bonding Methods 0.000 claims description 2
- 239000000126 substance Substances 0.000 claims description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims 1
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 claims 1
- 229910052801 chlorine Inorganic materials 0.000 claims 1
- 239000000460 chlorine Substances 0.000 claims 1
- 239000003446 ligand Substances 0.000 claims 1
- 239000002904 solvent Substances 0.000 abstract description 16
- -1 futon Polymers 0.000 description 11
- 239000004814 polyurethane Substances 0.000 description 11
- 230000008878 coupling Effects 0.000 description 10
- 238000010168 coupling process Methods 0.000 description 10
- 238000005859 coupling reaction Methods 0.000 description 10
- 229920002635 polyurethane Polymers 0.000 description 10
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 8
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 8
- 239000010949 copper Substances 0.000 description 8
- 229910052802 copper Inorganic materials 0.000 description 8
- 239000004698 Polyethylene Substances 0.000 description 7
- 229920000573 polyethylene Polymers 0.000 description 7
- 238000001125 extrusion Methods 0.000 description 6
- 238000003466 welding Methods 0.000 description 6
- 239000011888 foil Substances 0.000 description 5
- 238000009434 installation Methods 0.000 description 5
- 230000008859 change Effects 0.000 description 4
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- 239000007769 metal material Substances 0.000 description 4
- 229920000642 polymer Polymers 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 239000004952 Polyamide Substances 0.000 description 3
- XECAHXYUAAWDEL-UHFFFAOYSA-N acrylonitrile butadiene styrene Chemical compound C=CC=C.C=CC#N.C=CC1=CC=CC=C1 XECAHXYUAAWDEL-UHFFFAOYSA-N 0.000 description 3
- 239000003292 glue Substances 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 238000005304 joining Methods 0.000 description 3
- 229920002647 polyamide Polymers 0.000 description 3
- 229920000098 polyolefin Polymers 0.000 description 3
- 239000005060 rubber Substances 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 description 2
- 239000002033 PVDF binder Substances 0.000 description 2
- 239000004721 Polyphenylene oxide Substances 0.000 description 2
- 239000004743 Polypropylene Substances 0.000 description 2
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical group CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 2
- 150000001252 acrylic acid derivatives Chemical class 0.000 description 2
- 239000000956 alloy Substances 0.000 description 2
- 229910045601 alloy Inorganic materials 0.000 description 2
- 238000005452 bending Methods 0.000 description 2
- YACLQRRMGMJLJV-UHFFFAOYSA-N chloroprene Chemical compound ClC(=C)C=C YACLQRRMGMJLJV-UHFFFAOYSA-N 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 229920001577 copolymer Polymers 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 238000005520 cutting process Methods 0.000 description 2
- 150000002118 epoxides Chemical class 0.000 description 2
- 229920006332 epoxy adhesive Polymers 0.000 description 2
- 239000003000 extruded plastic Substances 0.000 description 2
- NIHNNTQXNPWCJQ-UHFFFAOYSA-N fluorene Chemical compound C1=CC=C2CC3=CC=CC=C3C2=C1 NIHNNTQXNPWCJQ-UHFFFAOYSA-N 0.000 description 2
- 229920002313 fluoropolymer Polymers 0.000 description 2
- 239000000446 fuel Substances 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 229920001903 high density polyethylene Polymers 0.000 description 2
- 239000011229 interlayer Substances 0.000 description 2
- 239000012948 isocyanate Substances 0.000 description 2
- 150000002513 isocyanates Chemical class 0.000 description 2
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 229920000768 polyamine Polymers 0.000 description 2
- 239000004417 polycarbonate Substances 0.000 description 2
- 229920000515 polycarbonate Polymers 0.000 description 2
- 229920000728 polyester Polymers 0.000 description 2
- 229920000570 polyether Polymers 0.000 description 2
- 229920002981 polyvinylidene fluoride Polymers 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- UIYCHXAGWOYNNA-UHFFFAOYSA-N vinyl sulfide Chemical compound C=CSC=C UIYCHXAGWOYNNA-UHFFFAOYSA-N 0.000 description 2
- 241000208140 Acer Species 0.000 description 1
- 241001471112 Artocarpus tamaran Species 0.000 description 1
- 238000003462 Bender reaction Methods 0.000 description 1
- 229910001369 Brass Inorganic materials 0.000 description 1
- KTABEIGSPRUOMX-UHFFFAOYSA-N C[Re]CC Chemical compound C[Re]CC KTABEIGSPRUOMX-UHFFFAOYSA-N 0.000 description 1
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 description 1
- 229910000881 Cu alloy Inorganic materials 0.000 description 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
- 239000005977 Ethylene Substances 0.000 description 1
- 229920000181 Ethylene propylene rubber Polymers 0.000 description 1
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 1
- 239000004831 Hot glue Substances 0.000 description 1
- 240000002853 Nelumbo nucifera Species 0.000 description 1
- 235000006508 Nelumbo nucifera Nutrition 0.000 description 1
- 235000006510 Nelumbo pentapetala Nutrition 0.000 description 1
- 229920001328 Polyvinylidene chloride Polymers 0.000 description 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N Propene Chemical group CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 1
- 239000002174 Styrene-butadiene Substances 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- 229920006397 acrylic thermoplastic Polymers 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- 229920006125 amorphous polymer Polymers 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000010951 brass Substances 0.000 description 1
- 230000001680 brushing effect Effects 0.000 description 1
- DQXBYHZEEUGOBF-UHFFFAOYSA-N but-3-enoic acid;ethene Chemical compound C=C.OC(=O)CC=C DQXBYHZEEUGOBF-UHFFFAOYSA-N 0.000 description 1
- MTAZNLWOLGHBHU-UHFFFAOYSA-N butadiene-styrene rubber Chemical compound C=CC=C.C=CC1=CC=CC=C1 MTAZNLWOLGHBHU-UHFFFAOYSA-N 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000011365 complex material Substances 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 229920001887 crystalline plastic Polymers 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000000806 elastomer Substances 0.000 description 1
- 239000005038 ethylene vinyl acetate Substances 0.000 description 1
- 229920002457 flexible plastic Polymers 0.000 description 1
- NPEWZDADCAZMNF-UHFFFAOYSA-N gold iron Chemical compound [Fe].[Au] NPEWZDADCAZMNF-UHFFFAOYSA-N 0.000 description 1
- JVPLOXQKFGYFMN-UHFFFAOYSA-N gold tin Chemical compound [Sn].[Au] JVPLOXQKFGYFMN-UHFFFAOYSA-N 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 239000003779 heat-resistant material Substances 0.000 description 1
- 239000004700 high-density polyethylene Substances 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 229920000831 ionic polymer Polymers 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229910001092 metal group alloy Inorganic materials 0.000 description 1
- 238000005272 metallurgy Methods 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 229920002587 poly(1,3-butadiene) polymer Polymers 0.000 description 1
- 229920001084 poly(chloroprene) Polymers 0.000 description 1
- 229920001200 poly(ethylene-vinyl acetate) Polymers 0.000 description 1
- 229920003229 poly(methyl methacrylate) Polymers 0.000 description 1
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- 239000002861 polymer material Substances 0.000 description 1
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- 229920001021 polysulfide Polymers 0.000 description 1
- 239000005077 polysulfide Substances 0.000 description 1
- 150000008117 polysulfides Polymers 0.000 description 1
- 239000005033 polyvinylidene chloride Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- XIUFWXXRTPHHDQ-UHFFFAOYSA-N prop-1-ene;1,1,2,2-tetrafluoroethene Chemical group CC=C.FC(F)=C(F)F XIUFWXXRTPHHDQ-UHFFFAOYSA-N 0.000 description 1
- 238000007348 radical reaction Methods 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 230000002787 reinforcement Effects 0.000 description 1
- 230000002940 repellent Effects 0.000 description 1
- 239000005871 repellent Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
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- 238000005096 rolling process Methods 0.000 description 1
- 238000010079 rubber tapping Methods 0.000 description 1
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- 239000007921 spray Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000011115 styrene butadiene Substances 0.000 description 1
- 229920003048 styrene butadiene rubber Polymers 0.000 description 1
- 150000003440 styrenes Chemical class 0.000 description 1
- ISXSCDLOGDJUNJ-UHFFFAOYSA-N tert-butyl prop-2-enoate Chemical compound CC(C)(C)OC(=O)C=C ISXSCDLOGDJUNJ-UHFFFAOYSA-N 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 229920002725 thermoplastic elastomer Polymers 0.000 description 1
- 229920002803 thermoplastic polyurethane Polymers 0.000 description 1
- ANRHNWWPFJCPAZ-UHFFFAOYSA-M thionine Chemical compound [Cl-].C1=CC(N)=CC2=[S+]C3=CC(N)=CC=C3N=C21 ANRHNWWPFJCPAZ-UHFFFAOYSA-M 0.000 description 1
- 229940098465 tincture Drugs 0.000 description 1
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- 238000004804 winding Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B1/00—Layered products having a non-planar shape
- B32B1/08—Tubular products
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/01—General aspects dealing with the joint area or with the area to be joined
- B29C66/341—Measures for intermixing the material of the joint interlayer
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/001—Combinations of extrusion moulding with other shaping operations
- B29C48/0013—Extrusion moulding in several steps, i.e. components merging outside the die
- B29C48/0015—Extrusion moulding in several steps, i.e. components merging outside the die producing hollow articles having components brought in contact outside the extrusion die
- B29C48/0016—Extrusion moulding in several steps, i.e. components merging outside the die producing hollow articles having components brought in contact outside the extrusion die using a plurality of extrusion dies
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/03—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor characterised by the shape of the extruded material at extrusion
- B29C48/09—Articles with cross-sections having partially or fully enclosed cavities, e.g. pipes or channels
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/16—Articles comprising two or more components, e.g. co-extruded layers
- B29C48/18—Articles comprising two or more components, e.g. co-extruded layers the components being layers
- B29C48/21—Articles comprising two or more components, e.g. co-extruded layers the components being layers the layers being joined at their surfaces
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C65/00—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor
- B29C65/48—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor using adhesives, i.e. using supplementary joining material; solvent bonding
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/01—General aspects dealing with the joint area or with the area to be joined
- B29C66/05—Particular design of joint configurations
- B29C66/10—Particular design of joint configurations particular design of the joint cross-sections
- B29C66/12—Joint cross-sections combining only two joint-segments; Tongue and groove joints; Tenon and mortise joints; Stepped joint cross-sections
- B29C66/122—Joint cross-sections combining only two joint-segments, i.e. one of the parts to be joined comprising only two joint-segments in the joint cross-section
- B29C66/1222—Joint cross-sections combining only two joint-segments, i.e. one of the parts to be joined comprising only two joint-segments in the joint cross-section comprising at least a lapped joint-segment
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/01—General aspects dealing with the joint area or with the area to be joined
- B29C66/05—Particular design of joint configurations
- B29C66/10—Particular design of joint configurations particular design of the joint cross-sections
- B29C66/12—Joint cross-sections combining only two joint-segments; Tongue and groove joints; Tenon and mortise joints; Stepped joint cross-sections
- B29C66/122—Joint cross-sections combining only two joint-segments, i.e. one of the parts to be joined comprising only two joint-segments in the joint cross-section
- B29C66/1224—Joint cross-sections combining only two joint-segments, i.e. one of the parts to be joined comprising only two joint-segments in the joint cross-section comprising at least a butt joint-segment
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/01—General aspects dealing with the joint area or with the area to be joined
- B29C66/05—Particular design of joint configurations
- B29C66/10—Particular design of joint configurations particular design of the joint cross-sections
- B29C66/12—Joint cross-sections combining only two joint-segments; Tongue and groove joints; Tenon and mortise joints; Stepped joint cross-sections
- B29C66/124—Tongue and groove joints
- B29C66/1246—Tongue and groove joints characterised by the female part, i.e. the part comprising the groove
- B29C66/12469—Tongue and groove joints characterised by the female part, i.e. the part comprising the groove being asymmetric
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/50—General aspects of joining tubular articles; General aspects of joining long products, i.e. bars or profiled elements; General aspects of joining single elements to tubular articles, hollow articles or bars; General aspects of joining several hollow-preforms to form hollow or tubular articles
- B29C66/51—Joining tubular articles, profiled elements or bars; Joining single elements to tubular articles, hollow articles or bars; Joining several hollow-preforms to form hollow or tubular articles
- B29C66/52—Joining tubular articles, bars or profiled elements
- B29C66/522—Joining tubular articles
- B29C66/5221—Joining tubular articles for forming coaxial connections, i.e. the tubular articles to be joined forming a zero angle relative to each other
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/50—General aspects of joining tubular articles; General aspects of joining long products, i.e. bars or profiled elements; General aspects of joining single elements to tubular articles, hollow articles or bars; General aspects of joining several hollow-preforms to form hollow or tubular articles
- B29C66/51—Joining tubular articles, profiled elements or bars; Joining single elements to tubular articles, hollow articles or bars; Joining several hollow-preforms to form hollow or tubular articles
- B29C66/52—Joining tubular articles, bars or profiled elements
- B29C66/522—Joining tubular articles
- B29C66/5223—Joining tubular articles for forming corner connections or elbows, e.g. for making V-shaped pieces
- B29C66/52231—Joining tubular articles for forming corner connections or elbows, e.g. for making V-shaped pieces with a right angle, e.g. for making L-shaped pieces
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/50—General aspects of joining tubular articles; General aspects of joining long products, i.e. bars or profiled elements; General aspects of joining single elements to tubular articles, hollow articles or bars; General aspects of joining several hollow-preforms to form hollow or tubular articles
- B29C66/51—Joining tubular articles, profiled elements or bars; Joining single elements to tubular articles, hollow articles or bars; Joining several hollow-preforms to form hollow or tubular articles
- B29C66/52—Joining tubular articles, bars or profiled elements
- B29C66/522—Joining tubular articles
- B29C66/5229—Joining tubular articles involving the use of a socket
- B29C66/52291—Joining tubular articles involving the use of a socket said socket comprising a stop
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/50—General aspects of joining tubular articles; General aspects of joining long products, i.e. bars or profiled elements; General aspects of joining single elements to tubular articles, hollow articles or bars; General aspects of joining several hollow-preforms to form hollow or tubular articles
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Rigid Pipes And Flexible Pipes (AREA)
- Laminated Bodies (AREA)
- Pipeline Systems (AREA)
Description
483997 A7 B7 明說 明發 0 範 明 發 在 送 輸 於 用 是 者 計 設 所 管 合 複 0 多 i 種 1 係 關 明 發 本 有屬 管金 合 自 複製 層 一 多 , 〇 層)一 擐 wofl if %第 氣之 或料 體才 體熱 流晶 之结 時半 力或 壓狀 和 曰郎 度非 0 自 高製 升一 。 造包複性之 曆製明層之見 外。發多喜習 之曲本此可於 料彎 ,。多優 材被外統許而 塑以此系備力 熱 1¾ 。管具能 狀管示導而壓 晶合揭體裝耐 非複被流安和 種層已種易性 一多也一皆擊 自 ,法之況衝 製中方管狀耐 一例之合何、 和體管複任性 , 具合層 ,學 層一複多途化。 間之層種用耐管 中明多此多如合景 之發之用為諸複背 料本眈使管,層明 材在如括合質多發 固場 有現 具於 常後 體然 導 , 屬寸 金尺 ο 1 成某 製至 屬截 金切 鐵被 K前 常之 通裝 統安 系在 管而 導度 體長 流的 定 裝鐵 安比 之也 料然 管 , 種伕 此管 。 鐵 配比 匹裝 頭安 接之 件管 管銅 與。 便貴 K 昂 絲 a 攻·,而 管時 導費 鼷 、 金煩 將麻 金 鐵 比 M 可 管 •膠 塑 ο 統 系 管 導 體 流 於 用 被 已 也 〇 管 貴 _ 昂塑 管 (請先閱讀背面之注意事項再填寫本頁) 裝--------訂----------線, 經濟部智慧財產局員工消費合作社印製 而 然 ο 宜 βΓ- 0 管 之 製 銅 或 屬 撐 。 支本 的成 多料 更材 要和 需時 而 Η 因裝 ,安 性的 撓統 可系 有個 較 整 tut da J 管加 屬增 金須 鐵 撐 或支 管的 鋦外 比額 管 〇 塑 用一製 件之層 配示物 和揭合 子所聚 管 2 由 的80有 合 CO 含 混21品 屬4,產 金利此 \ 專。 膠國品 塑美產 Κ 如管 議例合 建。複 經統之 曾系狀 來管形 年導變 干體改 若流可 於種 本紙張尺度適用中國國家標準(CNS)A4規格(210 χ 297公釐) 經濟部智慧財產局員工消費合作社印製 483997 A7 B7 五、發明說明(2 ) 成含有無_內管之成型層。金屬材料較好製自銅和鋁之 合金。外層可K選自各種熱塑性而可K加工之材料,其 如橡膠、附隆、熱塑橡膠、聚氨基甲酸酯等等。較佳者 ,外_為熱塑性可加工半结晶之聚合物,如聚氯乙烯或 高密度聚乙烯複合物。聚合物材料可予交聯以改善複合 管之性質。外層較佳用擠柙方法形成於內層週圍。內外 曆被夾於兩_中間之聚醸胺基熱熔接著劑結合在一起。 外層之外徑大小,須使複合管產品能夠無須另予改變尺 寸而接合於常為耦合而具有聚合物或金屬單壁而具相當 尺寸之管子所用之配件接頭。 在歐洲專利申請案〇 084 088 A1中記述一種三曆之撓 性管子。此種管內之内暦是製自耐熱材料,如全氟乙烯 丙烯或聚偏二氟乙烯。中間層是一種金屬箔,例如鋁, 而較厚之外曆製自擠押而成之聚醯胺、聚丙烯、或聚乙 烯-丙烯混合物,或經過交聯之聚乙烯,全部都是半结 晶熱塑性聚合物。 具有積體金屬管狀補強物之一種半剛性塑膠管載於歐 洲專利申請案〇 〇 6 7 9 1 9 A 1。此種半剛性、半結晶之塑 P管可以製自聚烯烴、聚醻胺或聚醯胺樹脂。此管被包 Μ —層鋁金屬或合金而用雷射焊接。外層為擠押所成之 層0 歐洲專利申請案〇 2 3 0 4 5 7 A 1揭示一種複合的燃料和 蒸汽管。此複合管是一種可彎曲的管狀物,用於輸送燃 料,含有一可彎曲金屬帶,形成袖狀,延伸於整個物件 一4 一 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) -----------I — · I I I I I I I 訂·! ----I-- (請先閱讀背面之注意事項再填寫本頁) 483997 A7 B7 五、發明說明(3 ) (請先閱讀背面之注意事項再填寫本頁) 之長度,在金屬袖管之其他表面上具有接著劑,一撓性 塑膠套包裹於金屬袖管上。此外,金屬袖管具有撓性而 可彎曲之管狀内襯,而耐石油材料製成。用於此發明之 金鼷袖管Μ鋁為佳。金屬袖管在被彎成所需形狀時提供 足夠之強度Μ使塑膠層具有彈性。 相似者,歐洲專利申請案0 639 411 Α1揭示一種具有 二或多種不同材料層之複合管之製法,此管較佳之處在 於含有三層,金屬間夾於各塑膠曆之中,其如聚乙烯或 已交聯之聚乙烯;兩者均為半結晶物質。 歐洲專利〇 154 931 Α1記述一種複合管,製自延性金 屬片_捲於一擠押成之塑膠管而成為延縝管狀。在另再 被擠柙所成塑膠外鞘或管子包複之前,金屬片先被對縫 焊合。接著劑可被置於金屬片和塑膠外鞘之間。内曆之 擠柙所成塑膠管是一種經過交聯之聚乙烯、氟化聚合物 、聚醸胺或一種彈性體。在複合管中所用之金屬片是鋁 或鋁合金;而接著劑是一種離子性聚合物、乙烯-乙酸 乙烯酯或經過改質之聚乙烯。再者,此管可被用於最高 為300巴爾之壓力。 經濟部智慧財產局員工消費合作社印製 歐洲專利〇 237 234 Α1,授予Yasuo者,揭示一種方 法,產製一種複合管,用金屬製成而在金屬之內表面複 K塑膠層。根據此一專利,旋捲之金屬片形成一圓筒。 熔融之樹脂被擠柙成為阆筒形而複蓋於由金屬製成之圓 筒内之表面上。通常,内襯製自氟樹脂或芳香族聚酯樹 B旨。在一較佳具體例中,内襯製自一種聚烯烴化合物, 一 5 - 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) 經濟部智慧財產局員工消費合作社印製 483997 A7 B7 五、發明說明(4 ) 在其中聚烯烴被水解和自由基反應兩者所交聯。金屬片 是製自一種鋁合金。 、 美國專利4,559,973揭示一種不透水而可熱收縮之管 。此管是由内、外兩塑膠層所成之管,和一間夾於內、 外兩層之中之#積金屬箔膜構成。此金屬箔層厚度為〇 . 1 毫米。被脣積於金屬箔膜兩側之塑膠材料是選自包括聚 乙烯、聚氯乙烯、飽和聚酯、交聯聚乙烯、乙烯-丙烯 橡膠、δ夕橡膠、氯丁二烯橡膠和氟塑膠等之組合。 相似者,國際專利申請案W0/96/18840揭示一種多曆 材料製成之導管,專用於輸送機動車輛之流體。導管含 有一內層、一中間層和一外層。中間層含有一薄片材料 ,其如為鋁而具有大約10-70毫微米之厚度。在一實施 例中,內層是一聚_胺管而外層是經過交聯之聚氯乙烯。 各種混合的結構也曾被提出而用作配件。例如美國專 利5, 143, 407 ,授予Cokeh ,揭示一種管的耦合裝置, 含有由塑膠形成之圓筒形外層,具有中央向内延伸之凸 肋,同軸支持一延伸於其間之銅管,並具有多個凹陷圍 繞於銅管,鄰接於外曆之各端,使待耦合之管得K被插 入該等凹陷之中,圍繞銅管,並使管之接合與外層耦合 。如若需要,K圓形橡膠墊片插入於與凸肋各端相鄰之 凹陷中使有較奸的封合。 美國專利4,27 7,09 1揭示之一種耦合接頭,用於連接 具有塑膠内襯之金屬導管段落之各端,使形成一連續而 有内襯之導管,並揭示製造此種接頭之方法。一裸面套 -6 — 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) -------------裝--------訂---------線 (請先閱讀背面之注意事項再填寫本頁) 483997 A7 B7_ 五、發明說明(5 ) (請先閱讀背面之注意事項再填寫本頁) 筒被用於連接各管段之各端,使形成連續而有内襯之導 管。裸面套筒含有一裸端之圓筒體,其外尺寸實質上吻 合管中內襯之内尺寸。裸面套筒包括一徑向延伸之凸緣 ,從筒體端部向外輻射K匹配管之露出面。裸面套筒是 用諸如甲基乙基嗣之溶劑或任何適用之習知環氧黏膠结 合於管上。一相同之裸面套筒被置於第二個管段之露裸 端之內。如有需要,溶劑或膠合劑可在耦合組成之前立 即加於各凸緣上,Μ提供密封之結合。待連接之各管段 之各端被用耦合袖管作同軸之安排。耦合袖管是一比較 短之金屬管段,内徑稍小於管段各端之外徑。耦合袖管 是各開口端較佳為向外張開Μ便管段插入。在一較佳具 體例中,耦合袖管具備一位於中央之圓形凹陷或溝狀, 附有一密封帶。密封帶最好與内襯和裸面套筒為同一材 質,而Η被用環氧膠黏劑等結合而安置於凹陷之內。 經濟部智慧財產局員工消費合作社印製 雖然複合管和配件有種種混合的變化,各種管子依然 缺乏在金屬管和塑膠管兩者性質之間取得平衡,仍然需 要一種剛性、耐壓、耐衝擊,而且易於安裝之多層熱塑 複合管。能夠平衡金屬和塑膠管兩者性質之多曆複合管 有極大之需求。再者,可以使用此種多曆複合管之流體 導管系統也有需求存在。 發明槪沭 本發明專注於一種多層複合管。此多層複合管含有一 空心內導管,由硬質之熱塑材料製成;附有一金屬中間 脣,園繞於空心内導管上。一種非晶熱塑材料包圍於中 一7 — 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) 經濟部智慧財產局員工消費合作社印製 483997 A7 B7 五、發明說明(6 ) 間之金鼷層上。此多層複合管為耐衝擊,而且具有附溫 度和壓力兩者之能力,未見於習知之熱塑性管子和配件 。此外,多層複合管可被製成各種大小,包括若干習知 複合管系統前所未有之大口徑管子。多層複合管可在現 場易予裁切,而月易於安裝。 在本發明之一具體例中,多層複合管為可被彎曲。在 另一具髎例中,多餍複合管可被形成為大口徑複合管結 構。在再另一具體例中,比由相同塑膠構成之習知塑膠 管,在安裝之時,此多層複合管需要較少的懸吊管架。 又再在另一具體例中,此多層複合管可耐若干化學品, 其如氧和液氯、酸和鹼。 在流體導管系統中也可能採用此種獨特之多層複合 管。複合的多層管可用機械接頭、推入契合接頭、習用 配件或特別設計之配件,厄Μ溶劑黏膠,或其他接合手 段,例如熱熔法,予Κ接合而形成一種流體導管糸統。 可選優採用者,在配件和多層複合管之間可Μ含入一插 入物以提供比較安全而更可靠的附壓接頭。 在再另一觀點中,本發明是一種製造多層複合管流體導 管之方法,在其中一空心內導管是用熱塑聚合物以擠押 法形成。一接著劑層被胞於空心内導管之外表面。一金 屬中間層形成於空心內導管週圍。一第二接著劑層被置 於金屬中間層外表面上,而一非晶熱塑聚合物層被擠押 於如此之複合结構之外面。 為便於更為瞭解本發明此等及其他觀點與目標,各項 一 8 — 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) -------------裝--------訂---------線 (請先閱讀背面之注意事項再填寫本頁) 483997 A7 B7 五、發明說明(9 ) 料 S 資簡 考式 參圖 第 0 Μ是 配明 複 後 如。 明面 說剖 之 之 细例 詳體 作具 , 佳 園較 附管 合 -合 面 剖 之 時 曲 彎 被和 管管 合合 複複 明 1? 發多 本一 是 是 圖 圖 A 1 2 第第 第 用 M- 可 為 _ 接 。 用 明習 說和 統管 系合 之複 頭層 接多 結結 連連 所於 之 。 例 面體 截具 横能 之 可 筒種 套一 入之 插管 時合 合複 接層 。被多 _ 管明 意合發 示複本 之層造 筒多製 套為為 入圖圖 横 之 頭 接 良 改 f 1 種 1 之 明 發 本 於 用K 可 為 B 6 。 和 圖:6A 意第 示 明 說0 詳 之 例 體 〇 具 圖佳 而較 第 如 ο 管 合 複 層 多 種 一 是 明 發 本 各 看 請 示 所 圖 2 (請先閱讀背面之注意事項再填寫本頁) 曆 間 中 層屬 一 金 第繞 之圍 管 一 導和 心 ; 空上 成層 形一 一 第 有於 含繞 , 圍 il , 管 3 合 0 複間 0 中 多屬 ,金 經濟部智慧財產局員工消費合作社印製 被第表 5 一 内 曆及之 劑 K 曆 著,,外 接間三 一 之第 ❶ 面和 4 表面 層內表 三層外 第間層 之中間 成屬中 所金屬 物和金 合面於 聚表置 rhf 邕 夕 6 熱層層 晶一劑 非第菁 由於接 而置二 合 封 全 完 有 具 成 形 條 長 心 空 的 管K 是 2 管 導 。 内 間心 之空 面 管膠 導塑 内性 心塑 空熱 。 晶 面非 表性 內剛 狀或 管膠 的塑 合性 封塑 而熱 對的 相晶 和結 面半 表件 ?r^^一 夕 岡 狀用。 管 K 成 之可製 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) 經濟部智慧財產局員工消費合作社印製 483997 A7 B7 五、發明說明(8 ) 剛件非晶熱塑性材料是一種可被拉伸至越過其降伏點 之熱塑件材料。在此所用之剛性熱塑材料,根據AS TM試 驗方法D790、D638、或D882所試驗,在231C和5(U相對 濕度時,具有大於3 0 0 , 0 0 0 p s i (磅每平方时)之彈性模 數,不論是撓曲或伸張。一般上,非晶聚合物具有少於 十五百分比之结晶度。對於非晶熱塑聚合物之進一步資 料可獲自Alfrey,Jr.,高聚合物的機槭行為,JOhn Wiley & Sons, Inc·,(紐約,1965),第 510-515頁。 若干可Μ用於形成第一曆之適當非晶熱塑料,如在此 所界定之實例,包括氯化聚氯乙烯(” C Ρ V C ”)、聚氯乙烯 (” Ρ V C ”)聚偏二氯乙烯(” Ρ V D F ”)、聚醚賊和聚硫化苯基 、聚碳酸酯、懕克力類如甲基丙烯酸甲酯、和苯乙烯類 如丙烯腈苯乙烯丁二烯聚合物(” A B S ”)等。最佳之非晶 熱塑料為C P V C。 一般上,空心內導管之厚度隨熱塑複合管所需之最後 厚度而定。較佳者,空心內導管之外徑至少應大於管之 內孔0 . 1毫米。用於形成空心内導管之非晶熱塑料,最 佳為CPVC。在一具體例中,CPVC為金屬中間層之一至二 倍厚。在最佳的具體例中,CPVC層是金屬中間層厚度的 1 . 5倍。在最佳具體例中,形成空心内導管的C P V C具有 大約為0 . 6毫米之厚度。空心内導管較佳是K擠押法形 成,雖然其他方法也可用於形成空心導管。 在第一層之外表面和金屬中間層内表面之間所用之第 一接著劑脣,為適於永久使形成空心内導管之熱塑聚 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) -------------裝--------訂---------線 (請先閱讀背面之注意事項再填寫本頁) 483997 A7 B7 五、發明說明(9 ) (請先閱讀背面之注意事項再填寫本頁) 合物結合至金屬中間層上之任何膠合劑。接著劑之所以 需要,是因為空心内導管本身的熱塑材料不能_合至金 屬内層上。較佳者,由於兩層間之材料不同而旦熱膨脹 傜數有異,故膠合劑須予兼顧而採用。接著劑可以用噴 塗、擠押、刷塗或任何施用方式加至空心内導管之外表 面上。如用噴塗施用接著劑,可依製造廠商之建議予以 稀釋。第一接箸劑最好施加於内層的整個外表面。或者 ,可將第一接著劑形成為一条列圓環,均勻間隔璟繞於 各内層之外表面上。一般,第一接箸劑之施用産生一層 之厚度約為0.01毫米至約0.5毫米。第一接著劑層之較 佳厚度為0.1毫米。 經濟部智慧財產局員工消費合作社印製 第一接著劑可以是業者所用之任何接著劑材料。適當 接著劑之實例包括聚氯乙烯和聚氯乙烯共聚物、聚氨基 甲酸酯或其他異氣酸酯基之聚合物、氯丁二烯與其共聚 物、環氧化物、丙烯酸酯類、聚乙烯共聚物等。如用聚 乙烯共聚物,其共單體最好是乙酸乙烯酯或馬來酐。用 於與CPVC空心内導管連結之較佳接著劑層為聚氨基甲酸 酯。最佳者為Estane 5 8 2 7 1聚氨基甲酸酯,為B.F. Goodrich公司供應。Estane是B.F Goodrich公司之登錄 商標。 多層複合管之第二層可用任何金屬材料形成,只要其 抗拉強度大於塑膠所具有者。適合之金鼷中間層之實例 包括鐵質材料、銅、不銹銷、黃銅、和銅等材料。此夕卜 ,各種合金也可使用,只要能支持形成複合管結構第一 -11- 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) 483997 經濟部智慧財產局員工消費合作社印製 A7 _B7_ 五、發明說明(10 ) 和第三兩層之熱塑材料而符恰本發明之標的者即可。 金屬中間層最奸用平滑之金屬材料製成。通常,金屬 中間曆之厚度應在0 . 0 1 - 4 0毫米範圍內。較佳者,厚度 應存〇 .]牵4 . 0毫米範園内。金屬中間層可Μ是導管形狀 而有開口端,_繞於空心內導管上。或者改為,如後之 所詳述,金屬中間層可Κ用金屬條片包纏於空心內導管 而形成。所用之最佳材料為鋁。如果金屬層未被焊接, 則在繞於第一脣時必須重曼。金屬中間曆可以藉由Κ 一 角度將金屬娜繞而重疊,或是使金屬Κ材料毗鄰之對邊 互相平#。較佳者,如果用鋁,厚度為多曆複合管外徑 之0.5至5. 5 %範圍内。在最佳具體例中,鋁層為0.2毫米 厚。 用於多層複合管之第二接著劑層置於第二層之外表面 上。此種用於第二層之接著劑可為任何適當之膠合劑, 其為可Μ將金屬中間層外表面永久結合至熱塑曆之內表 面h。較佳者,膠合劑能夠適應兩層間因材料不同而生 之熱膨脹係數之差異。接著劑可以用噴塗、刷塗、擠押 、或其他任何方式施加於表面上。接著劑可以施於第二 _外表面全面。或改而為,可將接著劑層K 一系列圓環 均勻間隔園繞施於第二材料外表面。通常施用之接著劑 厚度約為〇.〇1至約0.5毫米,較佳為0.1毫米。 此第二接著劑層可K與第一曆接著劑相同,用於空心 內導管外表面和第二層之内表面之間。或改為,接著劑 也可以是不同的,只要在金屬中間層外表面和第三層内 -12- 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) ---------------------訂--------- (請先閱讀背面之注意事項再填寫本頁) 483997 A7 B7 五、發明說明(11) (請先閱讀背面之注意事項再填寫本頁) 表而之間建立膠合即可。適當接著劑之實例包括聚氯乙 烯和聚氯乙烯共聚物、聚氨基甲酸酯或其他異氰酸酯基 聚合物、氯丁二烯與其共聚物、環氧化物、丙烯酸酯類 、聚乙烯共聚物。如用聚乙烯共聚物,其共單體最好是 乙酸乙烯酯或馬來酐。若第三層是氯化聚氯乙烯,則較 佳之接著劑膺為Estane 58271聚氨基甲酸酯,由B.F. Goodr丨cli公司供應。此第二接著劑層之施用方法和所用 厚度與第一接著劑曆相關前述者相同。 多層複合管之外層是由剛性塑膠形成,如上所述。較 佳者,外層製自剛性塑膠,為非晶熱塑聚合物。可K用 於形成多曆複合管外曆之適當非晶熱塑料,在此界定為 包括氯化聚氯乙烯(” C P V C ”)、聚氯乙烯(” P V C ”)、聚偏 二氟乙烯("P VD R”)、聚醚賊和聚硫化亞乙烯、聚碳酸酯 、如甲基丙烯酸甲酯之懕克力類,笨乙烯類如丙烯_苯 乙烯丁二烯("ABS”)。在一具體例中,多層複合管之外 ( 經濟部智慧財產局員工消費合作社印製 層可以製自與空心内導管相同之材料。或改變之,如果 空心内導管製自非晶熱塑料,則外層可以製自與製成空 心內導管所用者不同之非晶熱塑料。然而,必須小心選 擇材料K確保多曆複合管能夠連接形成一複合糸統。通 常,外覉厚度隨多層複合管所需之最後厚度而定。較佳 者,外層厚度與金屬中間曆比較,將在1 : 5至5 : 1範圍内 。較佳者,外層厚度與金屬中間層比較,在1 : 3至3 : 1之 比率之中。在多層複合管之最佳具體例中,外層以C P V C 形成。在最佳具體例中,CPVC所形成之外曆厚度大約為 一13- 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) 483997 經濟部智慧財產局員工消費合作社印製 A7 B7_ 五、發明說明(12 ) 0 . 6毫米。 較佳者,外層流體導管所備有之外徑符合標稱管子外 尺寸,其如例如在ASTM F438所界定之40及/或80號, 或存ASTM 1)2846或其他ASTM標準,或DIN 8063和8079標 準,及/或BS 7291標準等所界定之SDR11 。其較佳者為 使習用配件能夠用於本發明之多層流體導管系統。管子 通常W特定之外徑為尺寸大小。所用配件為使管子承接 於管子配件之中而選定與標準外徑相關之内部尺寸。本 發明多層複合管尺寸僅有之限制為營在須彎曲時之彎曲 能力。此意謂複合管之直徑若太大則複合管結構不能被 彎曲。本發明彎曲管子之一示意實例見於第1Α圖。然而 ,所有各層須有足夠厚度Μ提供安全上所需之強度和剛 性,和在流體導管系統中複合管所專用之防漏系統,無 論流體為氣體或液體。 本發明之最佳具體例包含一多層複合管,其中之空心 內導管製自CPVC,金屬中間層為鋁箔,外層也是CPVC。 鋁層厚度約等於多層複合管外徑之1至5百分比。下列 所示圖表說明本發明較佳具體例之各種管子尺寸。各層 之最度以及合計量度Κ毫米(mm)列計。管子尺寸是基於 DIN 8078 標準。 一 14一 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) -------------裝--------訂---------線 (請先閱讀背面之注意事項再填寫本頁) 經濟部智慧財產局員工消費合作社印製 483997 A7 B7 五、發明說明(13) 管之尺寸 CP VC 鋁 CP VC 合計 16 0.6 0 . 4 0,6 1 . 6 20 0 . 9 0 . 6 0 . 9 2.4 25 1.0 0 . 7 1,0 2.7 32 1.3 0,9 1.3 3 . 5 40 1,6 1,2 1,6 4,3 50 2 . 1 1.4 2 . 1 5 . 6 63 2.6 1.7 2 . 6 6 . 9 最佳者,鋁曆為管之外徑之1.5%。在管中CPVC層厚度 對鋁之厚度之比率為1 : 5至3 : 1。最佳者,在較佳之多層 複合管中CPVC厚度對鋁之厚度為3:2 。在此較佳具體例 中,用於金屬中間曆兩面之接著劑為Estane 58 27 1聚氨 基甲酸_,可由B.P. Goodrich公司提供,如上所已詳 述0 第2圖Μ _解說明本發明配用多曆複合管之流體導管 系統之一部份。多個本發明之多曆複合管被用多個接頭 或/及配件7 Κ终端對終端連接。此等接頭及/或配件 包括接頭、直管耦合接頭、肘管、襯管、十字頭、蓋帽 、杵塞、凸緣、及/或連接管節。 在本發明之一具體例中,習用之配件或機械接頭可被 用Μ連接多層複合管。可用機械接頭之實例包括推入契 一 15 - 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) ------------农--------訂··---—-----線丨 (請先閱讀背面之注意事項再填寫本頁) 483997
五、發明說明(1 ) (請先閱讀背面之注意事項再填寫本頁) 合之配件,供作防漏接頭或供作防漏組件。合用之推入 楔合接頭包括獲自Genova Plastics之兼用接頭,自 J〇hn Guest,之 PI件,以及自 IMI Yorkshire Fittings 之 盲管·合接頭ΤΙ件。 對於接合配件之為非機械形成者,溶劑黏膠可以用於 接合配件。任何習見之溶劑黏膠均可應用於形成多層複 合管和配件之特別材料。另或,一種熔融膠合条統也可 以用於接合配件與多層複合管。此種条統載於AST M F4 12 ,以熱熔接頭為定義。任何習用之熱熔結合方法均可採 用。在3 —具體例中,如第6 Α和6 Β圖所示,各配件可以 被修改成為含有唇部8以軸向自配件内部延伸而匹配接 合形成内層之空心導管之内表面。一種溶劑黏膠或熱熔 可以被用於接合此型配件至多層複合管上。 第3A、3B和3C圖說明插入物或襯件9 ,適當用於接合本 經濟部智慧財產局員工消費合作社印製 發明之多層複合管與習用配件(為圓錐形或圓筒形 >。插 入物含有一開口端,空心圖筒體有一徑向外伸凸緣,從本 體端部外伸。插入物内之空心體之外徑應小於多層複合 管之内徑,然而須假定管外徑與管内徑之差不超過AST Μ D2846之建議者。凸緣部之造形須與多層複合管之外徑 相同。接著劑可以用以永久膠合多層複合管外表面至插 入物空心圓筒體之外表面上。較佳者,此插入物用與空 心内導管相同之材料製成。 用於膠合空心内導管與插入物空心圓筒體之溶劑黏膠 可以是任何能夠永久膠合兩層之適當膠合劑。溶劑黏膠 -1 6 - 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) 經濟部智慧財產局員工消費合作社印製 483997 A7 B7 五、發明說明(15) 可以用噴塗、刷塗或任何其他方式施於插入物外表面。 或變更為,溶劑黏膠可以施於空心内導管之内表面。任 何溶劑黏膠如若能夠在所需各表面建立膠合者均可被採 用。較佯之接著劑層,如果多曆複合管之第一和第三層 為CPVC,則應符合AST M F 49 3之要求。適用之溶劑黏膠, 其實例如IPS ,Oatey,Verhager及或Henkel所可供應 之CP VC溶劑黏膠。然後將附有插入物之多層複合管與習 用配件用膠合劑接合,如第4圖橫截面所示。 仟何形式的膠合劑,如若能夠永久膠合多層複合管表 面牵配件之表面上而成無漏接頭者,即可適合用於含有 選用插入物之多曆複合管與配件之接合。對於C P V C管, 這些膠合劑包栝一步之溶劑黏膠和二步之溶劑黏膠。用 於含有CPVC之多層複合管,適合之膠合劑實例包括合於 A S TM F 49 3之要求而保持防漏者。膠合劑是直接被施用, 月Μ在週圍溫度在(0 °F ( - 1 8 1C )至2 1 0 T (9 9 10 ))為宜。 在本發明之一具體例中,本發明多曆複合管可在任何 位置被彎1 0牵1 8 0 ° 。多曆複合管可用任何能夠形成小 半徑之手段予K彎曲,只要此種手段不致造成管子的扭 變即可。較佳者,用彎管器彎屈多層複合管結構。任何 被業者用於彎屈金屬管之彎管器均可被使用。通常,任 何產業上所用之彎管器皆可使用。例如,Lakeland製 造公司之彎管器H824, M & Greenlee公司之Greenlee 181導管彎管器皆可使用。根據本發明之複合管經過彎 曲後如第1 A圖所示。 一 17- 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) -------------裳--------訂---------線 (請先閱讀背面之注意事項再填寫本頁) 483997 經濟部智慧財產局員工消費合作社印製 A7 _B7_ 五、發明說明(16) 在本發明之另一具體例中,多層複合管以及所選用插 入物被熱熔至配件上。這是將熱塑層加熱至高於其材料 之軟化溫度以上。然後複合管各層(以及所選插入物)接 合於配件。任何已知之熱熔技術均可使用。 第5圖以方塊圖說明本發明製作多層複合管所用一種 方法所建議之步驟。進行各步驟所用機具為Kuhne Uffliaantelungstechnik GmbHin Swiss CAB 業 JL 所供 應。 在製造多層複合管之方法中,首先製備金颶條H。小 心使金屬條片上無任何油脂。然後擠押出空心内導管。 如果空心内導管是用CPVC粉製成,較佳用雙螺桿擠押機 ,擠押物溫度約在400至450 °F範圍内,較佳約自415至 430 °F。一經形成,空心内導管可以經過一第二擠押機 之擠柙頭而移動。此可藉由各種方式完成,包括推、拉 或兩者兼用。其次,以適當接著劑施加於空心内導管之 外表面,在施加接箸劑之步驟中用業者習知之適當方式 為之 在空心内導管整個外表面上擠押接箸劑為較好, 然也可以刷塗、噴塗或棍塗接著劑於管上。 然後將在第一步所製成之金屬條Η在空心内導管之外 表面之圍繞成形而為一導管。金屬條Η可用習知方法焊 合成為圍繞於空心内導管上之一導管。焊接之實例包括 雷射桿和電弧焊。較佳者,焊接時以避免使金颶層重叠 之狀況為宜。金屬中間層和其下之接著劑間之間隙以小 於2·0毫米為佳。對於在其中有一定間隙而金颶中間層 ~ 1 8 - 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) -------------裝--------訂---------線 (請先閱讀背面之注意事項再填寫本頁) 483997 A7 B7_ 五、發明說明(17) (請先閱讀背面之注意事項再填寫本頁) 被焊接之具體例中,金屬在經焊接之後即須被減薄(軋 平),目若需要,加熱活化接著劑而形成三層導管。軋 平稃序之细節依金屬厚度和種類而定,且為業者所已知 。其次,κ第二接著劑層皰於己成導管之金屬中間層外 表面。然後,一種熱塑料外層被擠押於具有接著劑塗層 之金屬中間層外表面。或改為,將第二接著劑和中間層 兩者形成為導管,然後將熱塑料外曆擠押於具有接著劑 塗覉之金屬中間曆之外表。或改為,使第二接著劑曆和 非晶熱塑外層被共同擠押。 或改之為,Μ接著劑塗於預成形之剛性熱塑管上。然 後Κ第二接著劑層施至金屬中間層之外側。然後一外曆 可被擠柙於金屬中間層頂上。可選擇者,第二接著劑層 Μ及熱塑料層可用共同擠押模頭在單一步驟中被共同擠 出0 經濟部智慧財產局員工消費合作社印製 本發明之多靨複合管具有比較好之可塑性和其他性質 之塑料管之優點。例如,多層複合管可用普通輪盤切割 機於現場切成任何長度。切割端最好去除毛頭,而且熱 塑料層可Κ倒角使易組裝,無須攻絲或起溝或對管之各 端破壞。膠合劑可以簡易皰於導管端部週圍而在露出之 熱塑料脣之上及/或在以露出熱塑料層而形成之配件之 最内面。各工件Μ將多層複合管插入而接合,用適當選 擇之插入物固定開口端,並予扭轉Μ分佈膠合劑。所成 _合接口將被施懕支撐,於數分鐘之内對所用膠合劑熟 ih 〇 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) 經濟部智慧財產局員工消費合作社印製 483997 A7 B7 五、發明說明(18) 本發明之多層複合管和導管系統在比較其他習知金屬 、塑膠或複管系統,在易於使用上,提供充裕之優點。 多層複合管對可相比較之材料所製成之塑膠管,在減小 厚度下,提供較大的強度和剛性。此外,多層複合管之 一具_例可以用習用彎管機繞一緊迫半徑而輕易彎曲, 減少在流體導管系統中所需接頭之數量。再者,多曆複 合管可以極易被耦連成為流體導管系統,少用技巧勞力 ,無需攻絲、擴口等裝置、吹管、或鉗夾系統,或其他 昂貴機械配裝耦聯糸統等耗費。 多層複合管有許多用途。例如,多曆複合管可Μ用於 仟何流Ρ導管系統,包括而非予限制,熱水器、消防麗 水系統、冷熱水用之板下裝置,中央加熱系統、壓縮空 氣系統、液壓系統、氣體傳輸、地板下加熱、工業流體 等系統、和接板下加熱系統。 管_例 内導管用 TempRite 88709 TAN 309 CPVC(Terap Rite 為B.F. Goodrich公司之一種註冊商標)形成,由B.F. Goodr丨ch公司供應。CPVC在由 Cincinrati Μ丨 lacron之 CM-5 5 HP擠押機上被擠成壁厚0.6毫米而外徑為24毫米 之管。擠柙機之1- 5區訂定在360°F(1821C),如同螺稈 油之馮度。模頭溫度訂為3 6 5 °F ί 1 8 5 t )。螺桿速率為 9”《1(每分轉數)。進料馬進以100「9111蓮轉,管子以45磅 /小時(20公斤./小時)被擠出。
其次,用一 Davis標準1.5时單螺稈擠押機於380 °F -20 - 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) -------------裝--------訂---------線 (請先閱讀背面之注意事項再填寫本頁) 483997 經濟部智慧財產局員工消費合作社印製 Α7 Β7 五、發明說明(19) 之溻度將E s t a n e 5 8 2 7 1聚氨基甲酸酯接著劑擠押於內導 管上。擠出之聚氨基甲酸酯厚度為0 . 1毫米,螺桿速率 訂於2 0 r p m ϋ 一種鋁脣,用鋁3 Ο Ο 3 ( Ο . 2毫米厚)形成於管之聚氨基 甲酸酯和C P V C等層之上,用裝有雷射焊接功能而由 A 1 e a t e丨供給之11 n U e in a機器。所成鋁層在其内表面與其 下之接著劑間有0 . 8毫米之間隙,被焊合並軋平至外徑 為2 4 . 3毫米。
Estane 58271聚氨基甲酸酯接著劑被用Davis標準1.5 吋單螺稈擠柙機於設定3 8 0 °F Π 9 3 °C )之潙度被擠出於鋁 層之h。此接著劑被擠出成0 . 1毫米厚度。螺桿速率為 2 0 r p m ° CPVC外層,為0.6 毫米之 TempRite 3205 TAN309,用 1.5时Davis標準單螺桿擠押機設定於400 °F(204 1C)之 溫度擠出於4層之管上,產生一種五層2 5毫米複合管。 螺稈速率為20rpm。 對本發明相關事項,熟悉此技術者將能夠蓮用本發明 之原理,於不離其實質特徵之精神,特別基於上述各項 教示,予K修改並造成其他事例。K上記述之各項具體 例存仟何方面均只作說明之用而非予限制。因此,發明 之範圍是Μ所附申請專利範圍各項之所指,而非前文之 說明。所Κ ,雖然發明已參照特定具體例予以敘逑,在 結構、次序、材料等等之變更,為對熟悉此技藝者為顯 而易知者,依然屬於本發明之範圍。 一21- 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) ϋ ϋ ί ϋ ϋ ϋ —.1 ϋ ϋ 1__— r · I ϋ Βϋ .^1 I ^-r^J .1 ϋ —r- ϋ ϋ ϋ ϋ I (請先閱讀背面之注意事項再填寫本頁) 483997 A7 B7 經濟部智慧財產局員工消費合作社印製 五、發明說明(2()) 符號之說明 1 2 6 7 8 多層複合管 空心内導管 金屬中間層 非晶熱塑聚合物 接著劑曆 接著劑層 接頭或配件 唇部 插入物或襯墊 一 22- 本紙張尺度適用中國國家標準(CNS)A4規格(210 x 297公釐) -------------裝--------訂---------線 (請先閱讀背面之注意事項再填寫本頁)
Claims (1)
- 483997 A8 B8 C8 D8 六、申請專利範圍 1 . 一種多層複合管,包栝一内層,為非晶或半结晶之熱 (請先閱讀背面之注意事項再填寫本頁) 塑件材料,有完全封合之管狀外表面;一金屬中間層 ;和一非晶熱塑料之外曆,實質上圍繞金屬中間曆。 2 .如申請專利範圍第1項之多層複合管,其在内層和金 屬中間曆之間另含一接著劑層。 3 .如申請專利範圍第2項之多層複合管,其在金屬中間 腾和外餍之間另含一接著劑層。 4,如申請專利範圍第1項之多層複合管,其中該内層包 栝氯化聚氯乙烯。 5 .如申請專利範圍第1項之多曆複合管,其中該金屬中 間層包括鋁。 6 .如申請專利範圍第1項之多層複合管,其中該外曆包 栝氯化聚氯乙烯。 7.如申請專利範圚第1項之多層複合管,其中該內管為 〇 . 6毫米厚,該金屬中間層為0 . 2毫米厚,而該外層 為〇 . 6毫米厚。 8 . —種製造多曆複合管之方法,包括: 經濟部智慧財產局員工消費合作社印製 (a)用熱塑材料擠柙出該多曆複合管之内層,成為 一導管,該導管具有一外表面; (b )在該導管之外表面上施加一接著劑層; (c )用一金屬條片形成金屬中間曆; (d )在該金屬中間層之外表面上施加一第二接著劑 層;及 (e )用一種非晶熱塑材料擠押出多曆複合管之外曆 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) 483997 A8 B8 C8 D8 六、申請專利範圍 於該金 9 .如申請 材料為 I 0 ·如申 中該熱 II , 如申 中該熱 1 2 ·如申 中該金 1 3 ·如申 中該非 屬中間層上。 專利範園第8 一種非晶熱塑 請專利 塑材料 請專利 塑材料 請專利 屬中間 請專利 晶熱塑 範圍第 為一種 範圍第 包栝氯 範圍第 材料包 範圍第 材料包 1 4 . 一個用於結合一多 開一端 包栝: 緣,從 一個啟 啟開一 項製造多 材料。 8項製造 半结晶熱 8項製造 化聚氯乙 8項製造 栝鋁。 8項製造 栝氯化聚 層複合管 之空心圓 心圓筒體 合管之内 層複合管之方法,熱塑 多層複合管之方法,其 塑材料。 多層複合管之方法,其 烯。 多層複合管之方法,其 多曆複合管之方法,其 (請先閱讀背面之注意事項再填寫本頁) 端之空 有之外徑小於多層複 .一種流體導管条統,包括: 氯乙烯。 至一配件上之插 筒體,具有一延 之端部向外伸出 徑。 入物, 伸之凸 ,所具 (a ) —多層複合管,由一非晶熱塑性之内層 屬之中間曆和一非晶熱塑料之外曆構成;和 (b) —裝於 經濟部智慧財產局員工消費合作社印製 一個防漏的密 多曆管和配件 1 β .如申 統另含 1 7 .如申 多層複合管之一開口端之配件, 封接頭於多曆複合管之一端,直 之間。 請專利範圍第1 5項之流 有一插入物,位於該多 請專利範圍第1 5項之流 一 24 - 體導管系統,其 層複合管與該配 體導管系統,其 ,一金 使形成 接在於 中該系 件之間 中該配 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐) 483997 A8 B8 C8 D8 六、申請專利範圍 件與該多(f複合管被用溶劑黏膠结合形成該防漏密封。 1 8 .如申請專利範圍第1 5項之流體導管系統,其中該配 件與該多層複合管K熱熔結合。 1 9 .如申請專利範圍第1 5項之流體導管系統,其中該配 件是一種推入契合之配件。 2 0 . —種由氯化聚氯乙烯之内層、鋁之金屬中間層和氯 化聚氯乙烯之外層所構成之多層複合管,其中該多層 複合管具有約自16毫米至約110毫米之整體直徑,且 其中該鋁餍約成為該管外層之1至5L外曆對金屬中 間層之厚度比率在1 : 5至5 : 1之範圍内,且其中内曆對 鋁之厚度比率在1 : 5至5 : 1之間。 -------------裝--------訂----------線 (請先閱讀背面之注意事項再填寫本頁) 經濟部智慧財產局員工消費合作社印製 本紙張尺度適用中國國家標準(CNS)A4規格(210 X 297公釐)
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EP (1) | EP1078189B1 (zh) |
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AT (1) | ATE254737T1 (zh) |
DE (1) | DE69912943T2 (zh) |
HK (1) | HK1035570A1 (zh) |
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-
1998
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-
1999
- 1999-05-18 WO PCT/US1999/011086 patent/WO1999061833A1/en active IP Right Grant
- 1999-05-18 AT AT99924364T patent/ATE254737T1/de not_active IP Right Cessation
- 1999-05-18 DE DE69912943T patent/DE69912943T2/de not_active Expired - Lifetime
- 1999-05-18 EP EP99924364A patent/EP1078189B1/en not_active Expired - Lifetime
- 1999-05-18 PL PL99344261A patent/PL194169B1/pl not_active IP Right Cessation
- 1999-05-18 JP JP2000551190A patent/JP2002516973A/ja active Pending
- 1999-08-02 TW TW088108394A patent/TW483997B/zh not_active IP Right Cessation
-
2001
- 2001-08-27 HK HK01106027A patent/HK1035570A1/xx not_active IP Right Cessation
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
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TWI472421B (zh) * | 2007-11-30 | 2015-02-11 | Lubrizol Advanced Mat Inc | 具有金屬夾層的pvc/cpvc複合管及其製造方法 |
CN103108739A (zh) * | 2010-08-02 | 2013-05-15 | 路博润高级材料公司 | 具有坚固耐用插入件的流体输送组件 |
TWI621800B (zh) * | 2010-08-02 | 2018-04-21 | 盧伯利索先進材料有限公司 | 具堅固嵌件之流體處理總成 |
US8615878B2 (en) | 2011-08-19 | 2013-12-31 | Wistron Corp. | Method for fabricating a heat pipe, and instrument of the method |
Also Published As
Publication number | Publication date |
---|---|
EP1078189A1 (en) | 2001-02-28 |
HK1035570A1 (en) | 2001-11-30 |
US6293311B1 (en) | 2001-09-25 |
PL194169B1 (pl) | 2007-05-31 |
JP2002516973A (ja) | 2002-06-11 |
DE69912943T2 (de) | 2004-09-02 |
EP1078189B1 (en) | 2003-11-19 |
WO1999061833A1 (en) | 1999-12-02 |
ATE254737T1 (de) | 2003-12-15 |
PL344261A1 (en) | 2001-10-22 |
DE69912943D1 (de) | 2003-12-24 |
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