MX341537B - Proceso de transesterificacion que utiliza catalizadores de sal mixta de acetilacetonatos. - Google Patents
Proceso de transesterificacion que utiliza catalizadores de sal mixta de acetilacetonatos.Info
- Publication number
- MX341537B MX341537B MX2012014722A MX2012014722A MX341537B MX 341537 B MX341537 B MX 341537B MX 2012014722 A MX2012014722 A MX 2012014722A MX 2012014722 A MX2012014722 A MX 2012014722A MX 341537 B MX341537 B MX 341537B
- Authority
- MX
- Mexico
- Prior art keywords
- catalysts
- acetylacetonates
- pref
- reaction
- mixed salt
- Prior art date
Links
- 239000003054 catalyst Substances 0.000 title abstract 4
- 238000005809 transesterification reaction Methods 0.000 title abstract 2
- 238000000034 method Methods 0.000 title 1
- 150000002148 esters Chemical class 0.000 abstract 3
- POILWHVDKZOXJZ-ARJAWSKDSA-M (z)-4-oxopent-2-en-2-olate Chemical compound C\C([O-])=C\C(C)=O POILWHVDKZOXJZ-ARJAWSKDSA-M 0.000 abstract 1
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 abstract 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- CERQOIWHTDAKMF-UHFFFAOYSA-M Methacrylate Chemical compound CC(=C)C([O-])=O CERQOIWHTDAKMF-UHFFFAOYSA-M 0.000 abstract 1
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- -1 carbon atom carboxylic acid Chemical class 0.000 abstract 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 238000011065 in-situ storage Methods 0.000 abstract 1
- 229910017053 inorganic salt Inorganic materials 0.000 abstract 1
- 238000002955 isolation Methods 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 229910052751 metal Inorganic materials 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 239000012429 reaction media Substances 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 229920006395 saturated elastomer Polymers 0.000 abstract 1
- 239000007858 starting material Substances 0.000 abstract 1
- 229910052725 zinc Inorganic materials 0.000 abstract 1
- 239000011592 zinc chloride Substances 0.000 abstract 1
- 235000005074 zinc chloride Nutrition 0.000 abstract 1
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/03—Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
- B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
- B01J31/22—Organic complexes
- B01J31/2204—Organic complexes the ligands containing oxygen or sulfur as complexing atoms
- B01J31/2208—Oxygen, e.g. acetylacetonates
- B01J31/2226—Anionic ligands, i.e. the overall ligand carries at least one formal negative charge
- B01J31/223—At least two oxygen atoms present in one at least bidentate or bridging ligand
- B01J31/2234—Beta-dicarbonyl ligands, e.g. acetylacetonates
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
- B01J31/26—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/28—Preparation of carboxylic acid esters by modifying the hydroxylic moiety of the ester, such modification not being an introduction of an ester group
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C68/00—Preparation of esters of carbonic or haloformic acids
- C07C68/06—Preparation of esters of carbonic or haloformic acids from organic carbonates
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2231/00—Catalytic reactions performed with catalysts classified in B01J31/00
- B01J2231/40—Substitution reactions at carbon centres, e.g. C-C or C-X, i.e. carbon-hetero atom, cross-coupling, C-H activation or ring-opening reactions
- B01J2231/49—Esterification or transesterification
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
- B01J2531/20—Complexes comprising metals of Group II (IIA or IIB) as the central metal
- B01J2531/26—Zinc
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
- B01J2531/80—Complexes comprising metals of Group VIII as the central metal
- B01J2531/84—Metals of the iron group
- B01J2531/842—Iron
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB201009969A GB201009969D0 (en) | 2010-06-15 | 2010-06-15 | Transesterification process using mixed salt acetylacetonates catalysts |
| PCT/EP2011/059672 WO2011157645A2 (en) | 2010-06-15 | 2011-06-10 | Transesterification process using mixed salt acetylacetonates catalysts |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MX2012014722A MX2012014722A (es) | 2013-04-11 |
| MX341537B true MX341537B (es) | 2016-08-24 |
Family
ID=42471652
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2012014722A MX341537B (es) | 2010-06-15 | 2011-06-10 | Proceso de transesterificacion que utiliza catalizadores de sal mixta de acetilacetonatos. |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US8865931B2 (cg-RX-API-DMAC7.html) |
| EP (1) | EP2582453B1 (cg-RX-API-DMAC7.html) |
| JP (1) | JP5916722B2 (cg-RX-API-DMAC7.html) |
| KR (1) | KR101863154B1 (cg-RX-API-DMAC7.html) |
| CN (1) | CN103140287B (cg-RX-API-DMAC7.html) |
| BR (1) | BR112012031918B1 (cg-RX-API-DMAC7.html) |
| GB (1) | GB201009969D0 (cg-RX-API-DMAC7.html) |
| MX (1) | MX341537B (cg-RX-API-DMAC7.html) |
| RS (1) | RS55808B1 (cg-RX-API-DMAC7.html) |
| WO (1) | WO2011157645A2 (cg-RX-API-DMAC7.html) |
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| US9150673B2 (en) * | 2011-07-06 | 2015-10-06 | Basf Se | Process for preparing (meth)acrylic esters |
| CN105233874B (zh) * | 2013-11-07 | 2017-07-14 | 山东科技大学 | 一步法制备卟啉功能化纳米硫化锌的工艺 |
| KR20160107181A (ko) * | 2013-12-26 | 2016-09-13 | 다우 글로벌 테크놀로지스 엘엘씨 | 리튬 염-촉매된 트랜스에스테르화 공정용 억제제 배합물 및 리튬 염의 제거방법 |
| JP6643546B2 (ja) * | 2015-03-10 | 2020-02-12 | 東亞合成株式会社 | （メタ）アクリレートの製造方法 |
| JP6633612B2 (ja) * | 2015-03-12 | 2020-01-22 | 株式会社クラレ | （メタ）アクリル酸エステル化合物の製造方法 |
| EP3072879A1 (en) | 2015-03-26 | 2016-09-28 | Nitto Europe N.V | Method for prevention of premature polymerization |
| JP6809043B2 (ja) * | 2015-09-03 | 2021-01-06 | 東亞合成株式会社 | 単官能（メタ）アクリレートの製造方法 |
| CN105330537A (zh) * | 2015-11-30 | 2016-02-17 | 抚顺东联安信化学有限公司 | 丙烯酸甲氧基乙酯的制备方法 |
| US10704262B2 (en) | 2016-09-26 | 2020-07-07 | U.S. Silica Company | Self-cleaning cool roof system |
| CN109890483B (zh) * | 2016-11-09 | 2022-03-01 | 株式会社可乐丽 | 氧吸收剂 |
| JP6828500B2 (ja) * | 2017-02-21 | 2021-02-10 | 三菱瓦斯化学株式会社 | ２−メチル−２−ヒドロキシ−１−プロピル（メタ）アクリレートおよび／または３−メチル−３−ヒドロキシ−１−ブチル（メタ）アクリレートの製造方法ならびに組成物 |
| TWI796324B (zh) * | 2017-03-09 | 2023-03-21 | 日商東亞合成股份有限公司 | (甲基)丙烯酸酯的製造方法 |
| JP6991236B2 (ja) * | 2017-10-24 | 2022-02-10 | 信越化学工業株式会社 | ラジカル重合性オルガノポリシロキサンの製造方法、放射線硬化性オルガノポリシロキサン組成物、及び剥離シート |
| EP3778554B1 (en) | 2018-04-12 | 2024-02-07 | SNF Group | Method for producing 2-dimethylaminoethyl (meth)acrylate |
| CN109748826B (zh) * | 2018-12-28 | 2021-09-21 | 京博农化科技有限公司 | 一种茚虫威中间体肼基甲酸苄酯的合成方法 |
| CN113348199B (zh) | 2018-12-31 | 2023-02-17 | 美国陶氏有机硅公司 | 支链有机硅化合物、制备支链有机硅化合物的方法以及用其形成的共聚物 |
| US12215198B2 (en) | 2018-12-31 | 2025-02-04 | Dow Silicones Corporation | Branched organosilicon compound, method of preparing same, and compositions comprising same |
| CN113330054B (zh) | 2018-12-31 | 2023-02-21 | 美国陶氏有机硅公司 | 支链有机硅化合物、其制备方法以及用其形成的共聚物 |
| JP7561738B2 (ja) | 2018-12-31 | 2024-10-04 | ダウ シリコーンズ コーポレーション | 組成物、コポリマーの調製方法、並びにその方法及び最終用途 |
| EP3906244A1 (en) | 2018-12-31 | 2021-11-10 | Dow Silicones Corporation | Method of preparing acryloxy-functional organosilicon compounds |
| EP3906274A1 (en) | 2018-12-31 | 2021-11-10 | Dow Silicones Corporation | Acrylate-functional branched organosilicon compound, method of preparing same, and copolymer formed therewith |
| US12269833B2 (en) | 2018-12-31 | 2025-04-08 | Dow Silicones Corporation | Branched organosilicon compound, method of preparing same, and compositions comprising same |
| CN113661195B (zh) * | 2019-04-11 | 2025-05-30 | 株式会社可乐丽 | 聚合物、使用了该聚合物的氧吸收剂、及固化性组合物 |
| CN110252396B (zh) * | 2019-06-27 | 2022-03-11 | 山东第一医科大学(山东省医学科学院) | 一种用于间苯二甲酸二甲酯-5-磺酸钠合成过程中的催化剂、制备方法及应用 |
| WO2022220543A1 (ko) * | 2021-04-12 | 2022-10-20 | 한국화학연구원 | 디메틸테레프탈레이트의 에스테르 교환 반응에 의한 테레프탈레이트 유도체 제조 방법 |
| KR102480102B1 (ko) * | 2021-05-14 | 2022-12-23 | 한국화학연구원 | 아크릴계 그라디언트 공중합체의 제조방법 |
| AU2022329947A1 (en) | 2021-08-16 | 2024-03-28 | Rohm And Haas Company | Preparation of ureido methacrylate |
| EP4467591A4 (en) * | 2022-01-18 | 2025-04-16 | Asahi Kasei Kabushiki Kaisha | PROCESS FOR PRODUCING POLYCARBONATE DIOL, POLYCARBONATE DIOL, AND TRANSESTERIFICATION CATALYST |
| JP2024008235A (ja) * | 2022-07-07 | 2024-01-19 | 旭化成株式会社 | エステル交換触媒 |
| CN120025247B (zh) * | 2025-04-23 | 2025-07-04 | 抚顺东联安信化学有限公司 | 一种酯交换生产甲基丙烯酸正癸酯的方法 |
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| US2845451A (en) * | 1955-06-23 | 1958-07-29 | Basf Ag | Production of acrylic acid and its functional derivatives |
| US3528946A (en) | 1967-08-30 | 1970-09-15 | Fmc Corp | Acetylacetonates as polycondensation catalysts in transesterification method of preparing polyesters |
| US3532671A (en) | 1967-08-30 | 1970-10-06 | Fmc Corp | Acetylacetonate transesterification catalysts |
| US3528945A (en) | 1967-08-30 | 1970-09-15 | Fmc Corp | Acetylacetonates as polycondensation catalysts in the direct esterification method of preparing polyesters |
| JPS491531A (cg-RX-API-DMAC7.html) * | 1972-04-28 | 1974-01-08 | ||
| GB1573071A (en) | 1977-02-10 | 1980-08-13 | Mitsubishi Rayon Co | Process for producing unsaturated carbocylic acid esters |
| JPS603292B2 (ja) | 1977-02-28 | 1985-01-26 | 三菱レイヨン株式会社 | アクリル酸エステルまたはメタクリル酸エステルの製造法 |
| US4375361A (en) | 1980-03-24 | 1983-03-01 | Suntech, Inc. | Process for making a high octane fuel component |
| JPS57183745A (en) * | 1981-05-06 | 1982-11-12 | Asahi Chem Ind Co Ltd | Production of carbonic ester |
| US4777265A (en) | 1986-03-11 | 1988-10-11 | Basf Aktiengesellschaft | Preparation of acrylates and methacrylates |
| DE3740037A1 (de) | 1987-11-26 | 1989-06-08 | Basf Ag | Neue di(meth)acrylate, verfahren zu deren herstellung und deren verwendung |
| JPH01180861A (ja) * | 1988-01-11 | 1989-07-18 | Sanyo Chem Ind Ltd | アクリル系モノマーの製造法 |
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| US5037978A (en) | 1990-03-12 | 1991-08-06 | Rohm And Haas Company | Hafnium-catalyzed transesterification |
| DE4227299C1 (de) | 1992-08-18 | 1994-01-27 | Hoechst Ag | Verfahren zur Herstellung von monomeren Terephthalsäurediestern und Diolen aus Polyestern |
| FR2707290B1 (fr) | 1993-07-06 | 1995-09-01 | Atochem Elf Sa | Procédé de préparation de l'acrylate ou du méthacrylate d'éthylthioéthyle à l'aide d'acétylacétonate de zirconium comme catalyseur. |
| FR2727112B1 (fr) * | 1994-11-18 | 1996-12-20 | Atochem Elf Sa | Procede de preparation de (meth)acrylates d'alkylimidazolidone |
| DE69714373T2 (de) | 1996-10-17 | 2003-02-13 | Rohm And Haas Co., Philadelphia | Verfahren zum Herstellen von Monomeren |
| AU743962B2 (en) | 1997-08-29 | 2002-02-14 | Rohm And Haas Company | Transesterification process |
| JPH11158261A (ja) * | 1997-12-01 | 1999-06-15 | Mitsubishi Chemical Corp | 芳香族ポリカーボネート樹脂の製造方法 |
| US5840957A (en) | 1998-03-16 | 1998-11-24 | E. I. Du Pont De Nemours And Company | Transesterification process using lanthanum compound catalyst |
| AT408882B (de) | 1998-08-07 | 2002-03-25 | Dsm Fine Chem Austria Gmbh | Verfahren zur umesterung von alpha-ketocarbonsäureestern |
| US6350895B1 (en) | 1999-03-26 | 2002-02-26 | E. I. Du Pont De Nemours And Company | Transesterification process using yttrium and samarium compound catalystis |
| DE10008901B4 (de) | 2000-02-25 | 2009-01-29 | Evonik Degussa Gmbh | Verfahren zur Herstellung von Malonsäurediestern durch kontinuierliche Umesterung |
| DE10145228A1 (de) | 2001-09-13 | 2003-04-24 | Roehm Gmbh | Synthese von t-Butylaminoethylmethacrylat durch Umesterung des Alkohols mit MMA |
| JP2004010551A (ja) | 2002-06-07 | 2004-01-15 | Nippon Shokubai Co Ltd | ビニルエーテル基含有（メタ）アクリル酸エステル類の製造方法 |
| DE10321149A1 (de) | 2003-05-12 | 2004-12-02 | Bayer Materialscience Ag | Ytterbium(III)acetylacetonat als Katalysator zur Herstellung von aliphatischen Oligocarbonatpolyolen |
| US6971614B2 (en) | 2003-07-11 | 2005-12-06 | Jifram Extrusions, Inc. | Slatwall hanger stabilizing chip |
| GB0324964D0 (en) * | 2003-10-27 | 2003-11-26 | Great Lakes Chemical Europ | Preparation of hydroxyphenyl carboxylic acid esters |
| JP4336961B2 (ja) | 2003-10-31 | 2009-09-30 | 三菱瓦斯化学株式会社 | ２−メチル−２−ヒドロキシ−１−プロピル（メタ）アクリレートの製造方法 |
| DE102004042843A1 (de) * | 2004-09-04 | 2006-03-09 | Bayer Materialscience Ag | Metallacetylacetonate als Umesterungskatalysatoren |
| DE102007031468A1 (de) | 2007-07-05 | 2009-01-08 | Evonik Röhm Gmbh | Verfahren zur Herstellung von Allylmethacrylat |
| DE102008043810A1 (de) | 2007-11-20 | 2009-05-28 | Basf Se | Verfahren zur Herstellung von (Meth)acrylsäureestern von Prenol und Isoprenol |
| FR2949779B1 (fr) | 2009-09-07 | 2011-09-09 | Arkema France | Procede de preparation de (meth)acrylates d'alkylimidazolidone |
-
2010
- 2010-06-15 GB GB201009969A patent/GB201009969D0/en not_active Ceased
-
2011
- 2011-06-10 US US13/704,057 patent/US8865931B2/en not_active Expired - Fee Related
- 2011-06-10 RS RS20170282A patent/RS55808B1/sr unknown
- 2011-06-10 WO PCT/EP2011/059672 patent/WO2011157645A2/en not_active Ceased
- 2011-06-10 EP EP11736298.8A patent/EP2582453B1/en not_active Not-in-force
- 2011-06-10 BR BR112012031918-3A patent/BR112012031918B1/pt not_active IP Right Cessation
- 2011-06-10 JP JP2013514655A patent/JP5916722B2/ja not_active Expired - Fee Related
- 2011-06-10 MX MX2012014722A patent/MX341537B/es active IP Right Grant
- 2011-06-10 CN CN201180037399.5A patent/CN103140287B/zh not_active Expired - Fee Related
- 2011-06-10 KR KR1020137000243A patent/KR101863154B1/ko not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| RS55808B1 (sr) | 2017-08-31 |
| GB201009969D0 (en) | 2010-07-21 |
| CN103140287A (zh) | 2013-06-05 |
| US8865931B2 (en) | 2014-10-21 |
| EP2582453B1 (en) | 2016-12-28 |
| JP2013533861A (ja) | 2013-08-29 |
| CN103140287B (zh) | 2016-08-03 |
| JP5916722B2 (ja) | 2016-05-11 |
| BR112012031918B1 (pt) | 2019-07-02 |
| US20130090492A1 (en) | 2013-04-11 |
| KR101863154B1 (ko) | 2018-07-04 |
| WO2011157645A2 (en) | 2011-12-22 |
| MX2012014722A (es) | 2013-04-11 |
| KR20140002591A (ko) | 2014-01-08 |
| EP2582453A2 (en) | 2013-04-24 |
| WO2011157645A3 (en) | 2012-10-18 |
| BR112012031918A2 (pt) | 2016-11-08 |
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