KR940006901B1 - 입자상 함수겔상 중합체 및 흡수성 수지의 제조방법 - Google Patents

입자상 함수겔상 중합체 및 흡수성 수지의 제조방법 Download PDF

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Publication number
KR940006901B1
KR940006901B1 KR1019920001526A KR920001526A KR940006901B1 KR 940006901 B1 KR940006901 B1 KR 940006901B1 KR 1019920001526 A KR1019920001526 A KR 1019920001526A KR 920001526 A KR920001526 A KR 920001526A KR 940006901 B1 KR940006901 B1 KR 940006901B1
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South Korea
Prior art keywords
water
polymer
producing
gel polymer
particulate
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Expired - Lifetime
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KR1019920001526A
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English (en)
Korean (ko)
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KR920016480A (ko
Inventor
요시오 이리에
다쿠미 하쯔다
고이찌 요네무라
Original Assignee
가부시끼가이샤 니혼 쇼꾸바이
다나까 쇼소
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Publication of KR920016480A publication Critical patent/KR920016480A/ko
Application granted granted Critical
Publication of KR940006901B1 publication Critical patent/KR940006901B1/ko
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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00Processes of treating or compounding macromolecular substances
    • C08J3/12Powdering or granulating
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2300/00Characterised by the use of unspecified polymers
    • C08J2300/14Water soluble or water swellable polymers, e.g. aqueous gels
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S524/00Synthetic resins or natural rubbers -- part of the class 520 series
    • Y10S524/916Hydrogel compositions

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
  • Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
KR1019920001526A 1991-02-01 1992-01-31 입자상 함수겔상 중합체 및 흡수성 수지의 제조방법 Expired - Lifetime KR940006901B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP91-12324 1991-02-01
JP1232491 1991-02-01

Publications (2)

Publication Number Publication Date
KR920016480A KR920016480A (ko) 1992-09-24
KR940006901B1 true KR940006901B1 (ko) 1994-07-29

Family

ID=11802136

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019920001526A Expired - Lifetime KR940006901B1 (ko) 1991-02-01 1992-01-31 입자상 함수겔상 중합체 및 흡수성 수지의 제조방법

Country Status (5)

Country Link
US (1) US5275773A (enExample)
EP (1) EP0497623B1 (enExample)
KR (1) KR940006901B1 (enExample)
DE (1) DE69209104T2 (enExample)
TW (1) TW241279B (enExample)

Families Citing this family (74)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5610208A (en) 1994-02-17 1997-03-11 Nippon Shokubai Co., Ltd. Water-absorbent agent, method for production thereof, and water-absorbent composition
US5488104A (en) * 1994-06-30 1996-01-30 The Dow Chemical Company Process for comminuting cellulose ethers
TW387840B (en) * 1994-10-26 2000-04-21 Nippon Catalytic Chem Ind Water absorptive resin composition and method of manufacturing the same
US6432329B1 (en) * 1998-02-27 2002-08-13 Yoav Cohen Methods of manufacturing granular compositions
JP4141526B2 (ja) 1998-04-07 2008-08-27 株式会社日本触媒 吸水性樹脂の製造方法
DE19846413A1 (de) * 1998-10-08 2000-04-13 Basf Ag Verfahren zur Herstellung von hydrophilen wasserquellbaren Polymeren sowie deren Verwendung
DE19846412A1 (de) * 1998-10-08 2000-04-13 Basf Ag Hydrophile hochquellfähige Hydrogele sowie Verfahren zu ihrer Herstellung und Verwendung
DE19849499A1 (de) * 1998-10-27 2000-05-04 Basf Ag Verfahren zur vollständigen Trocknung von Hydrogelen
JP4679683B2 (ja) 1999-11-02 2011-04-27 株式会社日本触媒 吸水性重合体の製造方法、及び該重合体の製造装置
EP1130045B2 (en) 2000-02-29 2015-10-28 Nippon Shokubai Co., Ltd. Process for producing a water-absorbent resin powder
CN1262604C (zh) * 2001-01-26 2006-07-05 株式会社日本触媒 吸水剂及其制法以及吸水制品
US8426670B2 (en) * 2001-09-19 2013-04-23 Nippon Shokubai Co., Ltd. Absorbent structure, absorbent article, water-absorbent resin, and its production process and evaluation method
PL363038A1 (en) * 2002-02-04 2004-11-15 Nippon Shokubai Co, Ltd. Absorptive material, method for producing the same and absorptive article using the same
US6875511B2 (en) 2002-05-30 2005-04-05 Nippon Shokubai Co., Ltd. Production process for particulate water-absorbent resin
EP1594557B1 (en) * 2003-02-10 2019-05-01 Nippon Shokubai Co., Ltd. Water-absorbent resin composition and its production process
BRPI0401479A (pt) * 2003-04-25 2004-11-30 Nippon Catalytic Chem Ind Método para a desintegração de polìmero de hidrato e método para a produção de resina absorvente de água
BE1016025A3 (fr) * 2003-06-03 2006-01-10 Nippon Catalytic Chem Ind Procede de preparation d'un materiau absorbant l'eau.
RU2333229C2 (ru) * 2003-06-24 2008-09-10 Ниппон Шокубаи Ко., Лтд. Водопоглощающая композиция на основе смол, способ ее изготовления (варианты), поглотитель и поглощающее изделие на ее основе
JP4640923B2 (ja) * 2003-09-05 2011-03-02 株式会社日本触媒 粒子状吸水性樹脂組成物の製造方法
DE602004020159D1 (de) * 2003-09-19 2009-05-07 Nippon Catalytic Chem Ind Wasserabsorbierendes Harz mit behandelten Oberflächen und Verfahren zu seiner Herstellung
JP4866733B2 (ja) * 2004-03-31 2012-02-01 株式会社日本触媒 水性液吸収剤の製造方法
US8846823B2 (en) * 2004-05-07 2014-09-30 Nippon Shokubai Co., Ltd. Water absorbing agent and production method thereof
US20050288182A1 (en) * 2004-06-18 2005-12-29 Kazushi Torii Water absorbent resin composition and production method thereof
EP1629854B1 (en) * 2004-07-20 2010-10-13 The Procter & Gamble Company Surface cross-linked superabsorbent polymer particles and methods of making them
US8080705B2 (en) * 2004-07-28 2011-12-20 The Procter & Gamble Company Superabsorbent polymers comprising direct covalent bonds between polymer chain segments and method of making them
US20060128827A1 (en) * 2004-12-10 2006-06-15 The Procter & Gamble Company Absorbent members comprising modified water absorbent resin for use in diapers
EP1669394A1 (en) * 2004-12-10 2006-06-14 The Procter & Gamble Company Superabsorbent polymer particles with improved surface cross-linking and hydrophilicity and method of making them
JP5047616B2 (ja) * 2005-03-14 2012-10-10 株式会社日本触媒 吸水剤およびその製造方法
TWI353360B (en) 2005-04-07 2011-12-01 Nippon Catalytic Chem Ind Production process of polyacrylic acid (salt) wate
JP2007077366A (ja) * 2005-09-16 2007-03-29 Procter & Gamble Co 吸水剤の製法
JP2007099845A (ja) * 2005-09-30 2007-04-19 Procter & Gamble Co 水性液吸収剤およびその製法
DE102005055077A1 (de) 2005-11-16 2007-05-24 Basf Ag Verfahren zur Herstellung wasserabsorbierender Polymerpartikel
TWI394789B (zh) 2005-12-22 2013-05-01 Nippon Catalytic Chem Ind 吸水性樹脂組成物及其製造方法、吸收性物品
EP1837348B9 (en) 2006-03-24 2020-01-08 Nippon Shokubai Co.,Ltd. Water-absorbing resin and method for manufacturing the same
EP2010316B1 (en) 2006-03-27 2021-10-13 Nippon Shokubai Co.,Ltd. Water absorbing agent and water absorbent core using the agent
JP2009531467A (ja) * 2006-03-27 2009-09-03 株式会社日本触媒 内部構造が改善された吸水性樹脂、およびその製造方法
CA2649299A1 (en) * 2006-04-10 2007-10-25 The Procter & Gamble Company An absorbent member comprising a modified water absorbent resin
WO2008087114A1 (en) 2007-01-16 2008-07-24 Basf Se Production of superabsorbent polymers
WO2008102322A2 (en) 2007-02-22 2008-08-28 The Procter & Gamble Company Method of surface treating particulate material using electromagnetic radiation
US8252715B2 (en) 2007-03-05 2012-08-28 Nippon Shokubai Co., Ltd. Water-absorbing agent and production method thereof
SA08290542B1 (ar) 2007-08-28 2012-11-14 نيبون شوكوباي كو. ، ليمتد طريقة لإنتاج راتنج ماص للماء
JP2009142728A (ja) * 2007-12-12 2009-07-02 Procter & Gamble Co 吸水剤及びその製法
US9518133B2 (en) 2009-02-06 2016-12-13 Nippon Shokubai Co., Ltd. Hydrophilic polyacrylic acid (salt) resin and manufacturing method thereof
JP5615801B2 (ja) 2009-03-04 2014-10-29 株式会社日本触媒 吸水性樹脂の製造方法
CN104974358B (zh) 2009-03-31 2018-11-23 株式会社日本触媒 颗粒状吸水性树脂的制造方法
JP5580812B2 (ja) 2009-05-15 2014-08-27 株式会社日本触媒 (メタ)アクリル酸の製造方法
CN102414159B (zh) 2009-05-15 2014-02-26 株式会社日本触媒 制备(甲基)丙烯酸的方法
SG175379A1 (en) 2009-05-15 2011-12-29 Nippon Catalytic Chem Ind Process for producing (meth)acrylic acid and crystallization system
EP2438096B1 (de) 2009-06-03 2016-01-27 Basf Se Verfahren zur herstellung wasserabsorbierender polymerpartikel
CN102548654A (zh) 2009-09-29 2012-07-04 株式会社日本触媒 颗粒状吸水剂及其制造方法
KR101350958B1 (ko) * 2009-11-04 2014-01-24 주식회사 엘지화학 높은 생산성을 갖는 흡수성수지의 제조방법
US8875415B2 (en) 2010-03-08 2014-11-04 Nippon Shokubai, Co., Ltd. Method for drying granular water-containing gel-like cross-linked polymer
WO2011126079A1 (ja) 2010-04-07 2011-10-13 株式会社日本触媒 ポリアクリル酸(塩)系吸水性樹脂粉末の製造方法及びポリアクリル酸(塩)系吸水性樹脂粉末
EP2581403B1 (en) 2010-06-08 2019-08-28 Nippon Shokubai Co., Ltd. Manufacturing method for granular water-absorbing resin
KR101290740B1 (ko) 2010-11-22 2013-07-29 주식회사 엘지화학 고흡수성 수지의 제조 방법
JP5635685B2 (ja) 2011-04-20 2014-12-03 株式会社日本触媒 ポリアクリル酸(塩)系吸水性樹脂の製造方法および製造装置
TWI424007B (zh) 2011-12-22 2014-01-21 Ind Tech Res Inst 使膠體交聯的方法與藉由此方法形成之經交聯的膠體
JP6226969B2 (ja) 2012-06-19 2017-11-08 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se 吸水性ポリマー粒子の製造法
US8945716B2 (en) 2012-06-19 2015-02-03 Basf Se Process for producing water-absorbing polymer particles
WO2014032909A1 (en) * 2012-08-29 2014-03-06 Basf Se Process for producing water-absorbing polymer particles
JP6312680B2 (ja) * 2012-08-29 2018-04-18 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se 吸水性ポリマー粒子の製造方法
KR20140063401A (ko) * 2012-11-15 2014-05-27 주식회사 엘지화학 고흡수성 수지의 제조방법
US9550843B2 (en) 2012-11-27 2017-01-24 Nippon Shokubai Co., Ltd. Method for producing polyacrylic acid (salt)-based water absorbent resin
JP2016506981A (ja) 2013-01-29 2016-03-07 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se 膨潤したゲル床の高い透過性と同時に、速い膨潤速度、かつ高い遠心分離保持容量を有する吸水性ポリマー粒子の製造方法
JP5989912B2 (ja) 2013-08-28 2016-09-07 株式会社日本触媒 吸水性樹脂の製造方法
KR101700907B1 (ko) * 2013-12-10 2017-01-31 주식회사 엘지화학 고흡수성 수지의 제조 방법
US9334337B2 (en) 2014-01-24 2016-05-10 Baker Hughes Incorporated Enhanced water swellable compositions
EP3140325B1 (de) * 2014-05-08 2018-07-11 Basf Se Verfahren zur herstellung wasserabsorbierender polymerpartikel
JP6548723B2 (ja) 2014-05-08 2019-07-24 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se 吸水性ポリマー粒子
US11535689B2 (en) 2015-06-19 2022-12-27 Nippon Shokubai Co., Ltd. Poly (meth) acrylic acid (salt)-based particulate water-absorbing agent and production method therefor
KR101848470B1 (ko) 2015-07-10 2018-04-12 주식회사 엘지화학 고흡수성 수지의 제조 방법 및 이로부터 제조된 고흡수성 수지
KR102555379B1 (ko) 2018-01-16 2023-07-12 주식회사 엘지화학 고흡수성 수지의 제조 방법
WO2020099154A1 (en) * 2018-11-14 2020-05-22 Basf Se Process for producing superabsorbents
WO2022163849A1 (ja) 2021-01-29 2022-08-04 株式会社日本触媒 吸水性樹脂の製造方法

Family Cites Families (32)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5432176B2 (enExample) * 1973-05-02 1979-10-12
US3996411A (en) * 1973-07-07 1976-12-07 Nitto Kagaku Kogyo Kabushiki Kaisha Production of water-soluble polymers
JPS50136348A (enExample) * 1974-04-18 1975-10-29
US3966679A (en) * 1974-05-09 1976-06-29 The Dow Chemical Company Absorbent articles and methods for their preparation
JPS51125468A (en) * 1975-03-27 1976-11-01 Sanyo Chem Ind Ltd Method of preparing resins of high water absorbency
JPS5432176A (en) * 1977-08-15 1979-03-09 Sanyo Kokusaku Pulp Co Ltd Granulating and drying method by fluidization
US4113688A (en) * 1977-12-14 1978-09-12 Hercules Incorporated Process for rapidly dissolving gels of water-soluble polymers by extrusion, cutting and then slurrying under high shearing forces
JPS5951567B2 (ja) * 1978-02-08 1984-12-14 三井東圧化学株式会社 水溶性ビニル系重合体含水ゲルの破砕方法
US4286082A (en) * 1979-04-06 1981-08-25 Nippon Shokubai Kagaku Kogyo & Co., Ltd. Absorbent resin composition and process for producing same
JPS56161408A (en) * 1980-05-19 1981-12-11 Kao Corp Production of water-absorbing resin
JPS5734101A (en) * 1980-08-11 1982-02-24 Nippon Shokubai Kagaku Kogyo Co Ltd Novel polymerization process
JPS5794011A (en) * 1980-12-03 1982-06-11 Sumitomo Chem Co Ltd Productin of high-molecular material having excellent water absorbability
GB2088392B (en) * 1980-12-03 1984-05-02 Sumitomo Chemical Co Production of hydrogels
JPS57158209A (en) * 1981-03-25 1982-09-30 Kao Corp Production of bead-form highly water-absorbing polymer
JPS57198714A (en) * 1981-05-29 1982-12-06 Sumitomo Chem Co Ltd Production of hydrogel
US4358550A (en) * 1981-07-14 1982-11-09 Hercules Incorporated Process for preparation of aqueous solutions of water-soluble polymers
JPS5849714A (ja) * 1981-09-18 1983-03-24 Arakawa Chem Ind Co Ltd ポリアクリル酸塩乾燥固体の製造方法
DE3221947A1 (de) * 1982-06-11 1983-12-22 Cassella Ag, 6000 Frankfurt Verfahren zur herstellung klebfreier oder klebarmer partikel von hydrogelpolymerisaten
JPS5937003A (ja) * 1982-08-18 1984-02-29 Daisho Seiki Kosakusho:Kk ピ−リングマシンの案内装置
JPS59119172A (ja) * 1982-12-27 1984-07-10 日本化薬株式会社 含水ゲル状重合体の乾燥方法
JPS59184203A (ja) * 1983-04-04 1984-10-19 Nitto Chem Ind Co Ltd 部分加水分解されたアクリルアミド重合体の製造法
US4904715A (en) * 1983-12-16 1990-02-27 Calgon Corporation Method for producing free-flowing, water-soluble polymer gels
JPS6136763A (ja) * 1984-07-30 1986-02-21 Ricoh Co Ltd 多色画像形成方法
US4625001A (en) * 1984-09-25 1986-11-25 Nippon Shokubai Kagaku Kogyo Co., Ltd. Method for continuous production of cross-linked polymer
CA1253833A (en) * 1984-11-06 1989-05-09 Akira Yada Process for preparing water-soluble polymer gel particles
JPS61110511A (ja) * 1984-11-06 1986-05-28 Dai Ichi Kogyo Seiyaku Co Ltd 水溶性重合体ゲルの細粒化方法
US4654039A (en) * 1985-06-18 1987-03-31 The Proctor & Gamble Company Hydrogel-forming polymer compositions for use in absorbent structures
GB8910788D0 (en) * 1989-05-10 1989-06-28 Allied Colloids Ltd Absorbent products and their manufacture
US4920202A (en) * 1987-04-30 1990-04-24 Nippon Shokubai Kagaku Kogyo Co., Ltd. Method for production of hydrophilic polymer from hydrated gel polymer
SU1797612A1 (ru) * 1987-08-10 1993-02-23 Nippon Catalytic Chem Ind Cпocoб пoлучehия boдoпoглoщaющeй cmoлы
JP2555159B2 (ja) * 1987-08-10 1996-11-20 株式会社日本触媒 吸水性樹脂の製造方法
JP2639970B2 (ja) * 1988-07-07 1997-08-13 三洋電機株式会社 床用吸込具

Also Published As

Publication number Publication date
EP0497623B1 (en) 1996-03-20
DE69209104T2 (de) 1996-08-29
DE69209104D1 (de) 1996-04-25
KR920016480A (ko) 1992-09-24
EP0497623A3 (en) 1992-09-09
EP0497623A2 (en) 1992-08-05
US5275773A (en) 1994-01-04
TW241279B (enExample) 1995-02-21

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