KR890013088A - 저흡습성, 고접착성 실리콘 함유 폴리이미드 및 이의 전구체의 제조방법 - Google Patents

저흡습성, 고접착성 실리콘 함유 폴리이미드 및 이의 전구체의 제조방법 Download PDF

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KR890013088A
KR890013088A KR1019890002241A KR890002241A KR890013088A KR 890013088 A KR890013088 A KR 890013088A KR 1019890002241 A KR1019890002241 A KR 1019890002241A KR 890002241 A KR890002241 A KR 890002241A KR 890013088 A KR890013088 A KR 890013088A
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group
independently
formula
precursor
mol
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KR1019890002241A
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KR0131457B1 (ko
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코이찌 쿠니무네
요시야 쿠쯔자와
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노기 사다오
칫소가부시끼가이샤
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
    • C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
    • C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C08G73/1003—Preparatory processes
    • C08G73/1007—Preparatory processes from tetracarboxylic acids or derivatives and diamines
    • C08G73/101—Preparatory processes from tetracarboxylic acids or derivatives and diamines containing chain terminating or branching agents
    • C08G73/1017—Preparatory processes from tetracarboxylic acids or derivatives and diamines containing chain terminating or branching agents in the form of (mono)amine
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
    • C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C08G73/1039—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors comprising halogen-containing substituents
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
    • C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C08G73/1042—Copolyimides derived from at least two different tetracarboxylic compounds or two different diamino compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
    • C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C08G73/1046—Polyimides containing oxygen in the form of ether bonds in the main chain
    • C08G73/1053—Polyimides containing oxygen in the form of ether bonds in the main chain with oxygen only in the tetracarboxylic moiety

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
  • Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)
  • Adhesives Or Adhesive Processes (AREA)

Abstract

내용 없음.

Description

저흡습성, 고접착성 실리콘 함유 폴리이미드 및 이의 전구체의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (4)

  1. 다음 일반식(I)의 불소 함유 2산 무수물 A1몰, 다음 일반식(II)의 2산 무수물 A2몰, 다음 일반식(III)의 불소 함유 디아민 B1몰, 다음 일반식(IV)의 디아민 B2몰 및 다음 일반식(V)의 아미노실란 C몰을 다음 식(VI) 내지 (VIII)의 범위의 혼합비로 반응을 수행함을 특징으로 하여, 용매중 온도 30±0.01℃및 농도 0.5g/dl에서 측정한 대수점도수가 0.05 내지 5dl/g인 실리콘 함유 폴리이미드 전구체를 제조하는 방법.
    상기식에서, R1은 각자 독립적으로 4가의 탄소환식 방향족기 또는 복소환식 기이고, R2는 각각 독립적으로 적어도 2개의 탄소원자를 갖는 지방족 기, 지환식 기, 방향지향족 기, 탄소환식 방향족 기, 복소환식 기 또는 폴리실록산 기이며, R3은(단, 여기서 s는 1 내지 4의 정수이다)이고, R4는 독립적으로 탄소수 1 내지 6의 알킬기, 페닐기 또는 탄소수 7 내지 12의 알킬치환 페닐기이며, X는 독립적으로 알콕시기, 아세톡시기 또는 할로겐이고, m은 각각 독립적으로 0 또는 1이며, n은 각각 독립적으로 Q또는 1이고, K는 1K3이다.
  2. 제1항에 있어서, B1,B2및 C가 다음 식(IX)의 범위에 존재하는 방법.
  3. 제1항 또는 제2항에 있어서, 식(V)에서 R3이 독립적으로로 표시되는 기로서, o-, m-, p-체의 적어도 1종인 방법.
  4. 제1항에 기재한 방법으로 수득한 전구체를 함유하는 용액을 50 내지 500℃에서 소성하여 용매를 증발시키는 동시에 전구체를 가교, 경화시킴을 특징으로하여 실리콘 함유 폴리이미드를 제조하는 방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019890002241A 1988-02-26 1989-02-25 저흡습성, 고접착성 실리콘 함유 폴리이미드 및 이의 전구체의 제조방법 KR0131457B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP63043387A JPH0749482B2 (ja) 1988-02-26 1988-02-26 低吸湿性かつ高接着性のシリコン含有ポリイミド及びその前駆体の製造方法
JP43387/88 1988-02-26

Publications (2)

Publication Number Publication Date
KR890013088A true KR890013088A (ko) 1989-09-21
KR0131457B1 KR0131457B1 (ko) 1998-04-13

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Country Link
US (1) US4963635A (ko)
EP (1) EP0330456B1 (ko)
JP (1) JPH0749482B2 (ko)
KR (1) KR0131457B1 (ko)
DE (1) DE68917952T2 (ko)

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Also Published As

Publication number Publication date
DE68917952T2 (de) 1995-04-20
KR0131457B1 (ko) 1998-04-13
US4963635A (en) 1990-10-16
EP0330456A1 (en) 1989-08-30
DE68917952D1 (de) 1994-10-13
JPH01217037A (ja) 1989-08-30
JPH0749482B2 (ja) 1995-05-31
EP0330456B1 (en) 1994-09-07

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