KR860008221A - 광중합 가능한 방향족 폴리아믹산 유도체의 제조방법 - Google Patents
광중합 가능한 방향족 폴리아믹산 유도체의 제조방법 Download PDFInfo
- Publication number
- KR860008221A KR860008221A KR1019860003215A KR860003215A KR860008221A KR 860008221 A KR860008221 A KR 860008221A KR 1019860003215 A KR1019860003215 A KR 1019860003215A KR 860003215 A KR860003215 A KR 860003215A KR 860008221 A KR860008221 A KR 860008221A
- Authority
- KR
- South Korea
- Prior art keywords
- polyamic acid
- solution
- polyisoimide
- monomer
- reaction solution
- Prior art date
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
- C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
- C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
- C08G73/12—Unsaturated polyimide precursors
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
- C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
- C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
- C08G73/1003—Preparatory processes
- C08G73/1007—Preparatory processes from tetracarboxylic acids or derivatives and diamines
- C08G73/1028—Preparatory processes from tetracarboxylic acids or derivatives and diamines characterised by the process itself, e.g. steps, continuous
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
- C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
- C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
- C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
- C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
- C08G73/1003—Preparatory processes
- C08G73/1007—Preparatory processes from tetracarboxylic acids or derivatives and diamines
- C08G73/1025—Preparatory processes from tetracarboxylic acids or derivatives and diamines polymerised by radiations
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
- C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
- C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
- C08G73/1057—Polyimides containing other atoms than carbon, hydrogen, nitrogen or oxygen in the main chain
- C08G73/1064—Polyimides containing other atoms than carbon, hydrogen, nitrogen or oxygen in the main chain containing sulfur
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
- C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
- C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
- C08G73/1067—Wholly aromatic polyimides, i.e. having both tetracarboxylic and diamino moieties aromatically bound
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
- C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
- C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
- C08G73/1067—Wholly aromatic polyimides, i.e. having both tetracarboxylic and diamino moieties aromatically bound
- C08G73/1071—Wholly aromatic polyimides containing oxygen in the form of ether bonds in the main chain
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
- C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
- C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
- C08G73/1085—Polyimides with diamino moieties or tetracarboxylic segments containing heterocyclic moieties
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
- C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
- C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
- C08G73/1089—Polyisoimides
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03F—PHOTOMECHANICAL PRODUCTION OF TEXTURED OR PATTERNED SURFACES, e.g. FOR PRINTING, FOR PROCESSING OF SEMICONDUCTOR DEVICES; MATERIALS THEREFOR; ORIGINALS THEREFOR; APPARATUS SPECIALLY ADAPTED THEREFOR
- G03F7/00—Photomechanical, e.g. photolithographic, production of textured or patterned surfaces, e.g. printing surfaces; Materials therefor, e.g. comprising photoresists; Apparatus specially adapted therefor
- G03F7/004—Photosensitive materials
- G03F7/038—Macromolecular compounds which are rendered insoluble or differentially wettable
- G03F7/0387—Polyamides or polyimides
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- General Physics & Mathematics (AREA)
- Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
- Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Macromonomer-Based Addition Polymer (AREA)
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (1)
- (1) 방향족 이무수물과 식 RZH에 해당하는 단량체(들)의 비양자성 용매 내 용액을 형성하고(여기서 R은 첨가중합을 할 수 있는 에틸렌적으로 불포화된 부분이고 Z는 -O-, -S- 또는 -NR'- 여기서 R'는 -H 또는 C1-4알킬이며, 단량체의 양은 이무수물기준 0-40당량%임), 그리고 이 용액을 방향족이 무수물과 실질적으로 단량체의 전부와의 부분적 반응이 일어나기에 충분한 시간 및 온도에 유지시키고 ;(2) 단계 (1)의 방향족 이무수물-함유 반응용액 내에 반응용액을 50℃이하로 유지하면서 방향족 디아민을 혼합하고 용해시켜 미반응 무수물과 아민부분의 축합중합을 일으켜 해당하는 폴리아믹산(들)을 형성하고 ;(3) 단계(2)의 폴리아믹산(들)-함유 반응용액내에, N,N'-디히드로카빌-치환된 카보디이미드, 트리플루오로아세트산 무수물 및 그 혼합물로 구성되는 군으로부터 선택되는 이소이미드화제를 혼합하고 용해시켜, 폴리아믹산(들)을 해당하는 폴리이소이미드(들)로 전환시키고 ;(4) 단계(3)의 폴리이소이미드(들)의 비양자성 용액내에 식 RZH에 해당하는 단량체 몰 초과량을 혼합하고 용해시키고, 단량체에 의한 폴리이소이미드(들)의 실질적으로 완전한 에스테르화가 일어나기에 충분한 온도 및 시간에 용액을 유지하고 폴리이소이미드(들)을 해당되는 폴리아믹산 유도체로 전환시키고 ;(5) 단계(4)의 반응용액으로부터 폴리아믹산 유도체들을 분리시키는 ;연속적 단계로 구성되는, 폴리이미드 선구체인 광감성 폴리아믹산 유도체들의 합성방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US06/727,809 US4551522A (en) | 1985-04-26 | 1985-04-26 | Process for making photopolymerizable aromatic polyamic acid derivatives |
US727,809 | 1985-04-26 |
Publications (2)
Publication Number | Publication Date |
---|---|
KR860008221A true KR860008221A (ko) | 1986-11-14 |
KR950000703B1 KR950000703B1 (ko) | 1995-01-27 |
Family
ID=24924158
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019860003215A KR950000703B1 (ko) | 1985-04-26 | 1986-04-25 | 광중합 가능한 방향족 폴리아믹산 유도체의 제조방법 |
Country Status (6)
Country | Link |
---|---|
US (1) | US4551522A (ko) |
EP (1) | EP0203372B1 (ko) |
JP (2) | JPS6218426A (ko) |
KR (1) | KR950000703B1 (ko) |
CA (1) | CA1247636A (ko) |
DE (1) | DE3661020D1 (ko) |
Families Citing this family (33)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2516897B2 (ja) * | 1983-10-21 | 1996-07-24 | 信越化学工業株式会社 | 感光性組成物 |
DE3411660A1 (de) * | 1984-03-29 | 1985-10-03 | Siemens AG, 1000 Berlin und 8000 München | Verfahren zur herstellung von polyimid- und polyisoindolochinazolindion-vorstufen |
JPS62143929A (ja) * | 1985-07-16 | 1987-06-27 | Kanegafuchi Chem Ind Co Ltd | ポリイミド前駆体薄膜 |
JPS6284123A (ja) * | 1985-10-09 | 1987-04-17 | Sumitomo Bakelite Co Ltd | 低硬化収縮樹脂材料 |
US4954608A (en) * | 1986-05-30 | 1990-09-04 | Kanegafuchi Kagaku Kogyo Kabushiki | Copolymerized polyamic acid salts and process of producing them |
DE3786628T2 (de) * | 1986-09-04 | 1994-03-24 | Kanegafuchi Chemical Ind | Hoch molekulare, amphiphile, photoempfindliche Photopolymere und Herstellungsverfahren. |
WO1993014148A1 (en) * | 1987-02-13 | 1993-07-22 | Tsuyoshi Ikeda | Polyimide resin compositions and processes for their production |
JP2626696B2 (ja) * | 1988-04-11 | 1997-07-02 | チッソ株式会社 | 感光性重合体 |
KR910000832A (ko) * | 1988-06-28 | 1991-01-30 | 랄프 챨스 메더스트 | 인터레벨 유전체 및 기질 피복물용의 저유전상수 및 저수분흡수율을 갖는 폴리이미드 및 코폴리이미드 |
US4876329A (en) * | 1988-06-28 | 1989-10-24 | Amoco Corporation | Polyimide polymers and copolymers using 3,5-diaminobenzotrifluoride |
DE3833437A1 (de) * | 1988-10-01 | 1990-04-05 | Basf Ag | Strahlungsempfindliche gemische und deren verwendung |
DE3833438A1 (de) * | 1988-10-01 | 1990-04-05 | Basf Ag | Strahlungsempfindliche gemische und deren verwendung |
JP2880523B2 (ja) * | 1989-05-26 | 1999-04-12 | 日立化成工業株式会社 | 感光性樹脂組成物及びこれを用いた感光性エレメント |
DE68921052T2 (de) * | 1988-12-16 | 1995-06-01 | Hitachi Chemical Co Ltd | Lichtempfindliche Kunststoffzusammensetzung und lichtempfindliches Element unter Verwendung dieser Zusammensetzung. |
US5055549A (en) * | 1989-01-18 | 1991-10-08 | Chisso Corporation | Process for preparing photosensitive heat-resistant polymer |
US5104944A (en) * | 1989-07-18 | 1992-04-14 | International Business Machines Corporation | Process for nucleophilic derivatization of materials having an imide group conjugated to an aromatic moiety |
DE3927498C2 (de) * | 1989-08-21 | 2002-01-17 | Merck Patent Gmbh | Polyamidester, Verfahren zu ihrer Herstellung und ihre Verwendung zur Herstellung von Polyimiden |
JPH0415226A (ja) * | 1990-05-10 | 1992-01-20 | Chisso Corp | ヒドロキシフェニル基を有する感光性耐熱重合体 |
US5187241A (en) * | 1990-05-15 | 1993-02-16 | International Business Machines Corporation | Isoimide modifications of a polyimide and reaction thereof with nucleophiles |
US5242551A (en) * | 1991-03-28 | 1993-09-07 | International Business Machines Corporation | Electron induced transformation of an isoimide to an n-imide and uses thereof |
JPH0641305A (ja) * | 1991-10-25 | 1994-02-15 | Internatl Business Mach Corp <Ibm> | フッ素化された反応体からのポリアミド酸およびポリイミド |
US5420232A (en) * | 1992-04-29 | 1995-05-30 | International Business Machines Corporation | Process for making polyamic esters |
DE4217688A1 (de) * | 1992-05-29 | 1993-12-02 | Basf Lacke & Farben | Durch Einwirkung von Strahlung vernetzendes Gemisch und dessen Verwendung zur Herstellung hochtemperaturbeständiger Reliefstrukturen |
DE4218718A1 (de) * | 1992-06-06 | 1993-12-09 | Basf Lacke & Farben | Verfahren zur Herstellung strukturierter Schichten wärmebeständiger Polykondensate |
US5446074A (en) * | 1993-12-17 | 1995-08-29 | International Business Machines Corporation | Photosensitive polyimide precursors |
EP1219662B1 (en) | 1999-01-21 | 2004-08-04 | Asahi Kasei Kabushiki Kaisha | Polyamic acid ester |
US6410677B1 (en) * | 1999-09-28 | 2002-06-25 | Sumitomo Bakelite Company Limited | Resin composition for insulating material, and insulating material produced from said resin composition |
TWI311142B (en) * | 2006-10-18 | 2009-06-21 | Eternal Chemical Co Ltd | Amic acid ester oligomer, precursor composition for polyimide resin containing the same, and uses |
TWI658067B (zh) * | 2017-11-24 | 2019-05-01 | 台虹科技股份有限公司 | 聚醯亞胺前驅物及其所製得之微影圖案 |
JPWO2019193647A1 (ja) * | 2018-04-03 | 2021-04-30 | Hdマイクロシステムズ株式会社 | ポリイミド前駆体の製造方法、感光性樹脂組成物の製造方法、パターン硬化物の製造方法、層間絶縁膜、カバーコート層又は表面保護膜の製造方法、及び電子部品の製造方法 |
RU2680492C1 (ru) * | 2018-05-11 | 2019-02-21 | Общество с ограниченной ответственностью "Белфармамед" | Способ получения диметакрилата пиромеллитовой кислоты |
CN114634620B (zh) * | 2022-03-16 | 2024-09-20 | 广州广钢气体能源股份有限公司 | 一种水溶性光固化聚酰亚胺及其制备方法和应用 |
WO2024111129A1 (ja) * | 2022-11-25 | 2024-05-30 | Hdマイクロシステムズ株式会社 | ポリイミド前駆体の製造方法、ポリイミド前駆体、感光性樹脂組成物、硬化物、パターン硬化物の製造方法、及び電子部品 |
Family Cites Families (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US30186A (en) * | 1860-09-25 | John j | ||
US3822202A (en) * | 1972-07-20 | 1974-07-02 | Du Pont | Heat treatment of membranes of selected polyimides,polyesters and polyamides |
JPS49106599A (ko) * | 1973-02-08 | 1974-10-09 | ||
NL177718C (nl) * | 1973-02-22 | 1985-11-01 | Siemens Ag | Werkwijze ter vervaardiging van reliefstructuren uit warmte-bestendige polymeren. |
USRE30186E (en) * | 1974-08-02 | 1980-01-08 | Siemens Aktiengesellschaft | Method for the preparation of relief structures |
JPS52108435A (en) * | 1976-03-09 | 1977-09-10 | Showa Electric Wire & Cable Co Ltd | Method of manufacturing electrical insulating paint based on aromatic polyimide soluble in phenolic solvents |
JPS5512131A (en) * | 1978-07-11 | 1980-01-28 | Hitachi Chem Co Ltd | Preparation of polyamic acid for semiconductor treatment |
DE2933826A1 (de) * | 1979-08-21 | 1981-03-19 | Siemens AG, 1000 Berlin und 8000 München | Polyimid-, polyisoindolochinazolindion-, polyoxazindion- und polychinazolindion-vorstufen sowie deren herstellung |
US4320217A (en) * | 1980-01-25 | 1982-03-16 | Plastics Engineering Company | Polymerization products of polyimide derivatives having acetylenic terminal amide groups |
US4316845A (en) * | 1980-01-25 | 1982-02-23 | Plastics Engineering Company | Polyimide derivatives having terminal acetylenic groups |
DE3021748A1 (de) * | 1980-06-10 | 1981-12-17 | Siemens AG, 1000 Berlin und 8000 München | Strahlungsreaktive vorstufen hochwaermebestaendiger polymerer |
JPS592794B2 (ja) * | 1980-09-05 | 1984-01-20 | 株式会社デンソー | 点火時期制御方法 |
US4336175A (en) * | 1980-10-01 | 1982-06-22 | E. I. Du Pont De Nemours And Company | Polyimide precursor solutions |
US4496711A (en) * | 1981-07-24 | 1985-01-29 | Hughes Aircraft Company | Process for preparing isoimide containing oligomers |
US4438273A (en) * | 1981-07-24 | 1984-03-20 | Hughes Aircraft Company | Isoimide containing oligomers |
US4495342A (en) * | 1981-07-24 | 1985-01-22 | Hughes Aircraft Company | Isoimide containing oligomers |
US4485231A (en) * | 1981-07-24 | 1984-11-27 | Hughes Aircraft Company | Isoimide containing oligomers |
US4416973A (en) * | 1982-01-04 | 1983-11-22 | E. I. Du Pont De Nemours & Co. | Radiation-sensitive polyimide precursor composition derived from a diaryl fluoro compound |
-
1985
- 1985-04-26 US US06/727,809 patent/US4551522A/en not_active Expired - Lifetime
- 1985-07-16 JP JP60156852A patent/JPS6218426A/ja active Pending
-
1986
- 1986-04-23 EP EP86105608A patent/EP0203372B1/en not_active Expired
- 1986-04-23 DE DE8686105608T patent/DE3661020D1/de not_active Expired
- 1986-04-24 CA CA000507474A patent/CA1247636A/en not_active Expired
- 1986-04-25 JP JP61094977A patent/JPS61254547A/ja active Granted
- 1986-04-25 KR KR1019860003215A patent/KR950000703B1/ko not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
CA1247636A (en) | 1988-12-28 |
EP0203372A3 (en) | 1987-10-14 |
KR950000703B1 (ko) | 1995-01-27 |
EP0203372A2 (en) | 1986-12-03 |
US4551522A (en) | 1985-11-05 |
JPH0462306B2 (ko) | 1992-10-05 |
DE3661020D1 (en) | 1988-12-01 |
EP0203372B1 (en) | 1988-10-26 |
JPS6218426A (ja) | 1987-01-27 |
JPS61254547A (ja) | 1986-11-12 |
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