KR20010079763A - 무수당 알콜의 연속 제조 방법 - Google Patents

무수당 알콜의 연속 제조 방법 Download PDF

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Publication number
KR20010079763A
KR20010079763A KR1020017002972A KR20017002972A KR20010079763A KR 20010079763 A KR20010079763 A KR 20010079763A KR 1020017002972 A KR1020017002972 A KR 1020017002972A KR 20017002972 A KR20017002972 A KR 20017002972A KR 20010079763 A KR20010079763 A KR 20010079763A
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KR
South Korea
Prior art keywords
reaction product
solvent
reaction
organic solvent
recrystallization
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KR1020017002972A
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English (en)
Korean (ko)
Inventor
윌라드 씨. 브라인거
미하엘 볼러스
마이클 에이. 허바드
에드워드 지. 지
조지 크바코프스즈키
토마스 에이치 쇼클리
라이너 뢰스키
우베 딩게르디쎈
베르너 킨트
노르베르트 콜
요헨 리트
만프레트 톰칙크
Original Assignee
메리 이. 보울러
이 아이 듀폰 디 네모아 앤드 캄파니
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Application filed by 메리 이. 보울러, 이 아이 듀폰 디 네모아 앤드 캄파니 filed Critical 메리 이. 보울러
Publication of KR20010079763A publication Critical patent/KR20010079763A/ko

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D493/00—Heterocyclic compounds containing oxygen atoms as the only ring hetero atoms in the condensed system
    • C07D493/02—Heterocyclic compounds containing oxygen atoms as the only ring hetero atoms in the condensed system in which the condensed system contains two hetero rings
    • C07D493/04—Ortho-condensed systems
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/04—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having no double bonds between ring members or between ring members and non-ring members
    • C07D307/18—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having no double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D307/20—Oxygen atoms
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/66—Polyesters containing oxygen in the form of ether groups
    • C08G63/668—Polyesters containing oxygen in the form of ether groups derived from polycarboxylic acids and polyhydroxy compounds
    • C08G63/672—Dicarboxylic acids and dihydroxy compounds

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polyethers (AREA)
  • Saccharide Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
KR1020017002972A 1998-09-09 1999-01-11 무수당 알콜의 연속 제조 방법 KR20010079763A (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE19841032A DE19841032A1 (de) 1998-09-09 1998-09-09 Verfahren zur Herstellung von Anhydrozuckeralkoholen
DE19841032.8 1998-09-09
PCT/US1999/000537 WO2000014081A1 (en) 1998-09-09 1999-01-11 Continuous process for the production of anhydrosugar alcohols

Publications (1)

Publication Number Publication Date
KR20010079763A true KR20010079763A (ko) 2001-08-22

Family

ID=7880252

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020017002972A KR20010079763A (ko) 1998-09-09 1999-01-11 무수당 알콜의 연속 제조 방법

Country Status (11)

Country Link
EP (1) EP1119558A4 (tr)
JP (1) JP2002524455A (tr)
KR (1) KR20010079763A (tr)
CN (1) CN1317001A (tr)
AU (1) AU2111299A (tr)
BR (1) BR9913612A (tr)
CA (1) CA2340348A1 (tr)
DE (1) DE19841032A1 (tr)
ID (1) ID28701A (tr)
TR (1) TR200100701T2 (tr)
WO (1) WO2000014081A1 (tr)

Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2012081785A1 (en) * 2010-12-15 2012-06-21 Samyang Genex Corporation Methods for distilling and manufacturing anhydrosugar alcohols
WO2014061962A1 (ko) * 2012-10-15 2014-04-24 주식회사 삼양제넥스 무수당 알코올의 제조방법
WO2014073848A1 (ko) * 2012-11-08 2014-05-15 주식회사 삼양제넥스 결정화 공정 폐기물을 사용하여 수율을 향상시킨 고순도 무수당 알코올의 제조방법
WO2014129834A1 (ko) * 2013-02-22 2014-08-28 주식회사 삼양제넥스 박막증류에 이은 컬럼증류를 채택한 단일 증류단계를 포함하는 고순도 무수당 알코올의 제조방법
WO2014129833A1 (ko) * 2013-02-22 2014-08-28 주식회사 삼양제넥스 수소화 당의 연속 탈수반응을 통한 무수당 알코올의 제조방법
KR101452903B1 (ko) * 2012-11-08 2014-10-23 주식회사 삼양제넥스 결정화 공정 폐기물의 재결정물을 사용하여 수율을 항상시킨 고순도 무수당 알코올의 제조방법
KR20160044776A (ko) * 2014-10-16 2016-04-26 에스케이이노베이션 주식회사 공비증류를 이용한 무수당 알코올의 제조방법
WO2016060398A3 (ko) * 2014-10-16 2016-08-11 에스케이이노베이션 주식회사 고압 반응에 의한 무수당 알코올의 제조방법
WO2016105106A3 (ko) * 2014-12-23 2016-09-15 에스케이이노베이션 주식회사 무수당 알코올의 연속적인 생산방법
WO2016105107A3 (ko) * 2014-12-23 2016-09-15 에스케이이노베이션 주식회사 무수당 알코올의 효과적인 생산 및 정제 방법
US10752638B2 (en) 2014-10-16 2020-08-25 Sk Innovation Co., Ltd. Method for producing anhydrosugar alcohol by high-pressure reaction
WO2021172940A1 (ko) * 2020-02-28 2021-09-02 주식회사 삼양사 수율이 개선된 무수당 알코올의 디에테르 제조 방법
WO2021172929A1 (ko) * 2020-02-27 2021-09-02 주식회사 삼양사 무수당 알코올의 디에테르를 고순도로 정제하는 방법

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JP2003535085A (ja) * 2000-05-26 2003-11-25 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー アンヒドロ糖アルコールの連続的製造方法およびそれに有用な反応器
JP2004501117A (ja) * 2000-05-26 2004-01-15 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー ガスパージ支援によるアンヒドロ糖アルコールの製造方法
FR2810040B1 (fr) * 2000-06-09 2004-04-09 Roquette Freres Procede de purification d'une composition contenant au moins un produit de deshydratation interne d'un sucre hydrogene
JP4729238B2 (ja) * 2000-06-09 2011-07-20 ロケット・フルーレ 少なくとも１つの水素添加糖の内部脱水生成物を含む組成物の精製方法
US7439352B2 (en) 2000-11-01 2008-10-21 Archer-Daniels-Midland Company Process for the production of anhydrosugar alcohols
US6849748B2 (en) 2000-11-01 2005-02-01 Archer-Daniels-Midland Company Process for the production of anhydrosugar alcohols
FR2832407B1 (fr) * 2001-11-20 2005-07-01 Roquette Freres Procede de preparation d'une composition contenant au moins un produit de deshydratation interne d'un sucre hydrogene
US6818781B2 (en) * 2002-04-17 2004-11-16 E. I. Du Pont De Nemours And Company Simultaneous reaction and separation process for the manufacture of dianhydro sugar alcohols
US6831181B2 (en) * 2002-04-17 2004-12-14 E. I. Dupont De Nemours And Co. High yield byproduct recycle process for anhydro sugar alcohols
US6867296B2 (en) * 2002-04-17 2005-03-15 E. I. Du Pont De Nemours And Company Recovery and purification of anhydro sugar alcohols from a vapor stream
US6864378B2 (en) * 2002-04-17 2005-03-08 E. I. Du Pont De Nemours And Company Integrated continuous process for anhydro sugar alcohol manufacture
US7615652B2 (en) 2006-01-26 2009-11-10 Battelle Memorial Institute Two-stage dehydration of sugars
US7649099B2 (en) 2006-01-26 2010-01-19 Battelle Memorial Institute Method of forming a dianhydrosugar alcohol
US7772412B2 (en) * 2006-01-26 2010-08-10 Battelle Memorial Institute Methods for dehydration of sugars and sugar alcohols
US7728156B2 (en) 2006-01-26 2010-06-01 Battelle Memorial Institute Method of performing sugar dehydration and catalyst treatment
ES2561837T3 (es) * 2006-03-09 2016-03-01 Archer-Daniels-Midland Company Procedimiento para la producción de polialcoholes anhidros
GB0713598D0 (en) * 2007-07-13 2007-08-22 Ici Ltd Cyclic ethers
JP5635227B2 (ja) * 2008-02-18 2014-12-03 帝人株式会社 光拡散性ポリカーボネート樹脂組成物
JP5635228B2 (ja) * 2008-02-18 2014-12-03 帝人株式会社 ポリカーボネート樹脂組成物
EP2100972A1 (en) 2008-03-13 2009-09-16 BIOeCON International Holding N.V. Process for converting polysaccharides in a molten salt hydrate
US9765084B2 (en) 2008-04-10 2017-09-19 Iowa Corn Promotion Board Recovery and refining of dianhydrosugars
US9120806B2 (en) 2008-04-10 2015-09-01 Iowa Corn Promotion Board Dianhydrosugar production process
WO2010106055A1 (en) 2009-03-17 2010-09-23 Bioecon International Holding N.V. Process for converting polysaccharides in an inorganic molten salt hydrate
WO2010106057A1 (en) 2009-03-17 2010-09-23 Bioecon International Holding N.V. Process for converting polysaccharides in an inorganic molten salt hydrate
ES2438180T3 (es) 2009-03-17 2014-01-16 Bioecon International Holding N.V. Procedimiento para convertir polisacáridos en una sal fundida inorgánica hidratada
WO2010106052A1 (en) 2009-03-17 2010-09-23 Bioecon International Holding N.V. Process for converting polysaccharides in an inorganic molten salt hydrate
WO2012015616A1 (en) 2010-07-30 2012-02-02 Archer Daniels Midland Company Microwave assisted synthesis of dehydrated sugar derivatives hydroxymethylfurfural, levulinic acid, anhydrosugar alcohols, and ethers thereof
WO2012165676A1 (en) * 2011-06-02 2012-12-06 Samyang Genex Corporation A method for preparation of anhydrosugar alcohols
EP2615093A1 (en) 2012-01-16 2013-07-17 BIOeCON International Holding N.V. Isolation of anhydro sugar hexitols by selective adsorbents
KR101388676B1 (ko) 2012-05-11 2014-04-25 주식회사 삼양제넥스 박막증류를 통한 고순도 무수당 알코올의 제조방법
MX356806B (es) 2012-10-31 2018-06-12 Archer Daniels Midland Co Metodo mejorado de fabricacion de productos de deshidratacion interna de alcoholes de azucar.
KR101475388B1 (ko) 2012-12-14 2014-12-23 주식회사 삼양제넥스 하이드롤을 이용한 무수당 알코올의 제조방법
JP6347545B2 (ja) * 2014-07-16 2018-06-27 国立大学法人北海道大学 糖アルコールの脱水用固体触媒、およびその触媒を使用する二無水糖アルコールの製造方法。
CN104788465B (zh) * 2015-02-10 2017-04-19 沈阳化工大学 一种由山梨醇制异山梨醇的连续化制备方法
ES2827527T3 (es) 2015-02-24 2021-05-21 Archer Daniels Midland Co Fabricación y purificación de isoididas
KR102330592B1 (ko) * 2015-08-26 2021-11-24 에스케이이노베이션 주식회사 수증기를 이용한 무수당 알코올의 제조방법
KR102420908B1 (ko) * 2015-08-26 2022-07-15 에스케이이노베이션 주식회사 2단계 반응에 따른 무수당 알코올의 제조방법
JP6852263B2 (ja) * 2016-02-08 2021-03-31 三菱ケミカル株式会社 アンヒドロ糖アルコールの製造方法
FR3048970B1 (fr) 2016-03-16 2019-07-19 Roquette Freres Procede de fabrication de dianhydrohexitol avec une etape de distillation sur un evaporateur a couche mince
FR3050456B1 (fr) 2016-04-25 2018-04-27 Roquette Freres Procede de fabrication de cristaux de dianhydrohexitol avec une etape d'evapocristallisation des eaux meres de premiere cristallisation
CN109134485B (zh) * 2017-06-16 2021-02-09 中国科学院大连化学物理研究所 一种制备异山梨醇的方法

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DE3229412A1 (de) * 1982-08-06 1984-02-09 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von dianhydrohexitol-gemischen aus hexitolen, dianhydro-idit enthaltende dianhydro-hexitol-gemischen und ihre verwendung zur herstellung von polymeren
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Cited By (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2012081785A1 (en) * 2010-12-15 2012-06-21 Samyang Genex Corporation Methods for distilling and manufacturing anhydrosugar alcohols
WO2014061962A1 (ko) * 2012-10-15 2014-04-24 주식회사 삼양제넥스 무수당 알코올의 제조방법
KR101480849B1 (ko) * 2012-10-15 2015-01-13 주식회사 삼양제넥스 무수당 알코올의 제조방법
US9505777B2 (en) 2012-10-15 2016-11-29 Samyang Corporation Method for preparing anhydrous sugar alcohol
WO2014073848A1 (ko) * 2012-11-08 2014-05-15 주식회사 삼양제넥스 결정화 공정 폐기물을 사용하여 수율을 향상시킨 고순도 무수당 알코올의 제조방법
KR101452903B1 (ko) * 2012-11-08 2014-10-23 주식회사 삼양제넥스 결정화 공정 폐기물의 재결정물을 사용하여 수율을 항상시킨 고순도 무수당 알코올의 제조방법
US9260447B2 (en) 2012-11-08 2016-02-16 Samyang Genex Corporation Method for preparing high-purity anhydrosugar alcohol having improved yield by using waste from crystallization step
WO2014129834A1 (ko) * 2013-02-22 2014-08-28 주식회사 삼양제넥스 박막증류에 이은 컬럼증류를 채택한 단일 증류단계를 포함하는 고순도 무수당 알코올의 제조방법
WO2014129833A1 (ko) * 2013-02-22 2014-08-28 주식회사 삼양제넥스 수소화 당의 연속 탈수반응을 통한 무수당 알코올의 제조방법
US9399212B2 (en) 2013-02-22 2016-07-26 Samyang Corporation Method for producing anhydrosugar alcohol through continuous dehydration reaction of hydrogenated sugar
WO2016060398A3 (ko) * 2014-10-16 2016-08-11 에스케이이노베이션 주식회사 고압 반응에 의한 무수당 알코올의 제조방법
WO2016060399A3 (ko) * 2014-10-16 2016-08-18 에스케이이노베이션 주식회사 공비증류를 이용한 무수당 알코올의 제조방법
KR20160044776A (ko) * 2014-10-16 2016-04-26 에스케이이노베이션 주식회사 공비증류를 이용한 무수당 알코올의 제조방법
US10335710B2 (en) 2014-10-16 2019-07-02 Sk Innovation Co., Ltd. Method for producing anhydrous sugar alcohol using azeotropic distillation
US10752638B2 (en) 2014-10-16 2020-08-25 Sk Innovation Co., Ltd. Method for producing anhydrosugar alcohol by high-pressure reaction
WO2016105106A3 (ko) * 2014-12-23 2016-09-15 에스케이이노베이션 주식회사 무수당 알코올의 연속적인 생산방법
WO2016105107A3 (ko) * 2014-12-23 2016-09-15 에스케이이노베이션 주식회사 무수당 알코올의 효과적인 생산 및 정제 방법
US10414776B2 (en) 2014-12-23 2019-09-17 Sk Innovation Co., Ltd. Efficient method for producing and purifying anhydrous sugar alcohol
WO2021172929A1 (ko) * 2020-02-27 2021-09-02 주식회사 삼양사 무수당 알코올의 디에테르를 고순도로 정제하는 방법
WO2021172940A1 (ko) * 2020-02-28 2021-09-02 주식회사 삼양사 수율이 개선된 무수당 알코올의 디에테르 제조 방법

Also Published As

Publication number Publication date
ID28701A (id) 2001-06-28
BR9913612A (pt) 2001-10-30
TR200100701T2 (tr) 2001-07-23
WO2000014081A1 (en) 2000-03-16
CN1317001A (zh) 2001-10-10
CA2340348A1 (en) 2000-03-16
DE19841032A1 (de) 2000-03-16
EP1119558A4 (en) 2002-01-09
AU2111299A (en) 2000-03-27
JP2002524455A (ja) 2002-08-06
EP1119558A1 (en) 2001-08-01

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