KR102179649B1 - 디에틸아미노하이드록시벤조일헥실벤조에이트의 제조 방법 - Google Patents

디에틸아미노하이드록시벤조일헥실벤조에이트의 제조 방법 Download PDF

Info

Publication number
KR102179649B1
KR102179649B1 KR1020190161828A KR20190161828A KR102179649B1 KR 102179649 B1 KR102179649 B1 KR 102179649B1 KR 1020190161828 A KR1020190161828 A KR 1020190161828A KR 20190161828 A KR20190161828 A KR 20190161828A KR 102179649 B1 KR102179649 B1 KR 102179649B1
Authority
KR
South Korea
Prior art keywords
diethylaminohydroxybenzoylhexylbenzoate
present
mol
stirred
internal temperature
Prior art date
Application number
KR1020190161828A
Other languages
English (en)
Korean (ko)
Other versions
KR20200002720A (ko
Inventor
윤종배
백현우
최은화
Original Assignee
(주)에이에스텍
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by (주)에이에스텍 filed Critical (주)에이에스텍
Publication of KR20200002720A publication Critical patent/KR20200002720A/ko
Priority to CN202080042581.9A priority Critical patent/CN113993838A/zh
Priority to PCT/KR2020/002959 priority patent/WO2021071033A1/ko
Priority to JP2020573548A priority patent/JP7195351B2/ja
Priority to DE112020004927.2T priority patent/DE112020004927T5/de
Priority to KR1020200057898A priority patent/KR102357197B1/ko
Application granted granted Critical
Publication of KR102179649B1 publication Critical patent/KR102179649B1/ko
Priority to TW109142958A priority patent/TW202122369A/zh
Priority to JP2022154975A priority patent/JP2022188148A/ja
Priority to JP2022154976A priority patent/JP2022188149A/ja

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/06Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton from hydroxy amines by reactions involving the etherification or esterification of hydroxy groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C229/00Compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C229/52Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to carbon atoms of six-membered aromatic rings of the same carbon skeleton
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/10Separation; Purification; Stabilisation; Use of additives
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C219/00Compounds containing amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C219/34Compounds containing amino and esterified hydroxy groups bound to the same carbon skeleton having amino groups and esterified hydroxy groups bound to carbon atoms of six-membered aromatic rings of the same carbon skeleton
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/14Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof
    • C07C227/18Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof by reactions involving amino or carboxyl groups, e.g. hydrolysis of esters or amides, by formation of halides, salts or esters

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
KR1020190161828A 2019-10-11 2019-12-06 디에틸아미노하이드록시벤조일헥실벤조에이트의 제조 방법 KR102179649B1 (ko)

Priority Applications (8)

Application Number Priority Date Filing Date Title
CN202080042581.9A CN113993838A (zh) 2019-10-11 2020-03-02 二乙氨基羟基苯甲酰基苯甲酸己酯的制造方法
PCT/KR2020/002959 WO2021071033A1 (ko) 2019-10-11 2020-03-02 디에틸아미노하이드록시벤조일헥실벤조에이트의 제조 방법
JP2020573548A JP7195351B2 (ja) 2019-10-11 2020-03-02 ジエチルアミノヒドロキシベンゾイル安息香酸ヘキシルの製造方法
DE112020004927.2T DE112020004927T5 (de) 2019-10-11 2020-03-02 Herstellungsverfahren für Diethylaminohydroxybenzoylhexylbenzoat
KR1020200057898A KR102357197B1 (ko) 2019-10-11 2020-05-14 디에틸아미노하이드록시벤조일헥실벤조에이트의 제조 방법
TW109142958A TW202122369A (zh) 2019-10-11 2020-12-04 二乙氨基羥苯甲醯基苯甲酸己酯的製備方法
JP2022154975A JP2022188148A (ja) 2019-10-11 2022-09-28 ジエチルアミノヒドロキシベンゾイル安息香酸ヘキシルの製造方法
JP2022154976A JP2022188149A (ja) 2019-10-11 2022-09-28 ジエチルアミノヒドロキシベンゾイル安息香酸ヘキシルの製造方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR20190126502 2019-10-11
KR1020190126502 2019-10-11

Related Child Applications (1)

Application Number Title Priority Date Filing Date
KR1020200057898A Division KR102357197B1 (ko) 2019-10-11 2020-05-14 디에틸아미노하이드록시벤조일헥실벤조에이트의 제조 방법

Publications (2)

Publication Number Publication Date
KR20200002720A KR20200002720A (ko) 2020-01-08
KR102179649B1 true KR102179649B1 (ko) 2020-11-18

Family

ID=69154356

Family Applications (3)

Application Number Title Priority Date Filing Date
KR1020190161828A KR102179649B1 (ko) 2019-10-11 2019-12-06 디에틸아미노하이드록시벤조일헥실벤조에이트의 제조 방법
KR1020200057898A KR102357197B1 (ko) 2019-10-11 2020-05-14 디에틸아미노하이드록시벤조일헥실벤조에이트의 제조 방법
KR1020210156960A KR102439837B1 (ko) 2019-10-11 2021-11-15 디에틸아미노하이드록시벤조일헥실벤조에이트의 제조 방법

Family Applications After (2)

Application Number Title Priority Date Filing Date
KR1020200057898A KR102357197B1 (ko) 2019-10-11 2020-05-14 디에틸아미노하이드록시벤조일헥실벤조에이트의 제조 방법
KR1020210156960A KR102439837B1 (ko) 2019-10-11 2021-11-15 디에틸아미노하이드록시벤조일헥실벤조에이트의 제조 방법

Country Status (6)

Country Link
JP (3) JP7195351B2 (ja)
KR (3) KR102179649B1 (ja)
CN (1) CN113993838A (ja)
DE (1) DE112020004927T5 (ja)
TW (1) TW202122369A (ja)
WO (1) WO2021071033A1 (ja)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102179649B1 (ko) * 2019-10-11 2020-11-18 (주)에이에스텍 디에틸아미노하이드록시벤조일헥실벤조에이트의 제조 방법
KR20220147622A (ko) * 2020-02-27 2022-11-03 바스프 에스이 2-(4'-디에틸아미노-2'-히드록시벤조일)벤조산 헥실 에스테르를 단리시키는 방법
CN112479890B (zh) * 2020-11-27 2023-09-26 苏州亚科科技股份有限公司 一种硝基化合物的制备方法
CN116096701A (zh) * 2020-12-18 2023-05-09 巴斯夫欧洲公司 用于获得结晶二乙氨基羟基苯甲酰苯甲酸己酯的方法
CN112679393A (zh) * 2020-12-31 2021-04-20 江苏科本药业有限公司 索非布韦杂质的制备方法
CN114149339B (zh) * 2021-12-28 2023-01-31 黄冈美丰化工科技有限公司 一种紫外线吸收剂、组合物、化妆品及配制化妆品的工艺
CN115010615B (zh) * 2022-07-14 2023-12-08 四川沃肯精细化工有限公司 一种二乙氨基羟苯甲酰基苯甲酸正己酯的制备方法

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2005533764A (ja) * 2002-05-15 2005-11-10 ビーエーエスエフ アクチェンゲゼルシャフト 2−(4−n,n−ジアルキルアミノ−2−ヒドロキシベンゾイル)ベンゾエートの製造方法

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0342665A3 (en) * 1988-05-20 1990-08-16 Takeda Chemical Industries, Ltd. Physiologically active substance tan-931, its derivatives, their production and use
JPH0733709A (ja) * 1993-07-27 1995-02-03 Tanabe Seiyaku Co Ltd シュウ酸モノエステル化合物の製法
KR100236388B1 (ko) * 1995-11-28 1999-12-15 성재갑 신규한 고분자 자외선 차단제 및 그 제조방법
DE19917906A1 (de) 1999-04-20 2000-10-26 Basf Ag Verwendung von aminosubstituierten Hydroxybenzophenonen als photostabile UV-Filter in kosmetischen und pharmazeutischen Zubereitungen
DE10011317A1 (de) 2000-03-10 2001-09-13 Basf Ag Verwendung von aminosubstituierten Hydroxybenzophenonen als Lichtschutzmittel und Stabilisatoren für nicht lenbendes organisches Material
DE10342861A1 (de) 2003-09-15 2005-04-21 Basf Ag Pulverförmiger Zubereitungen, enthaltend eine Mischung von 2,4,6-Trianilino-p-(carbo-2'-ethylhexyl-1'-oxi)-1,3,5-triazin und Diethylamino-hydroxybenzoyl-hexyl-benzoat
AU2008248760A1 (en) * 2007-05-02 2008-11-13 Basf Se Method for the crystallization of 2-(4-N,N-diethyl amino-2-hydroxy benzoyl)-benzoic acid-n-hexyl ester
CA2725199A1 (en) * 2008-05-21 2009-11-26 The Regents Of The University Of Colorado Ionic liquids and methods for using the same
JP4299878B1 (ja) 2008-10-06 2009-07-22 株式会社パラエルモサ 化粧料
CN102665652B (zh) 2009-12-24 2014-07-16 花王株式会社 水凝胶颗粒
JP2014210715A (ja) 2013-04-17 2014-11-13 ロート製薬株式会社 アミノヒドロキシベンゾフェノン誘導体およびその製造方法、ならびに、それを用いた紫外線吸収剤および皮膚外用剤
TWI724049B (zh) * 2015-11-04 2021-04-11 日商大塚製藥股份有限公司 碘美醇的創新製備法及結晶化法
KR102179649B1 (ko) * 2019-10-11 2020-11-18 (주)에이에스텍 디에틸아미노하이드록시벤조일헥실벤조에이트의 제조 방법

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2005533764A (ja) * 2002-05-15 2005-11-10 ビーエーエスエフ アクチェンゲゼルシャフト 2−(4−n,n−ジアルキルアミノ−2−ヒドロキシベンゾイル)ベンゾエートの製造方法

Also Published As

Publication number Publication date
JP2022188148A (ja) 2022-12-20
WO2021071033A1 (ko) 2021-04-15
JP2022188149A (ja) 2022-12-20
WO2021071033A9 (ko) 2021-10-14
CN113993838A (zh) 2022-01-28
KR20200002720A (ko) 2020-01-08
KR102439837B1 (ko) 2022-09-05
JP2021533088A (ja) 2021-12-02
KR20210071804A (ko) 2021-06-16
TW202122369A (zh) 2021-06-16
KR102357197B1 (ko) 2022-02-03
KR20210142575A (ko) 2021-11-25
JP7195351B2 (ja) 2022-12-23
DE112020004927T5 (de) 2022-06-23

Similar Documents

Publication Publication Date Title
KR102179649B1 (ko) 디에틸아미노하이드록시벤조일헥실벤조에이트의 제조 방법
CN101600716A (zh) 用于制备9-羟基-3-(2-氯乙基)-2-甲基-4H-吡啶并[1,2-a]嘧啶-4-酮盐酸盐的改进方法
EP1025107A1 (en) Photochromic compounds
JP2008266172A (ja) 3−o−アルキル−5,6−o−(1−メチルエチリデン)−l−アスコルビン酸の製造方法および5,6−o−(1−メチルエチリデン)−l−アスコルビン酸の製造方法
KR100674522B1 (ko) 스피로플루오레놀의 제조 방법
KR20040041605A (ko) 시로스타졸의 제조 방법
RU2315042C2 (ru) Фотохромные оксазиновые соединения и способы их производства
EP0206789B1 (en) Crystalline hydroxyphenylpropionic acid ester and its production
JPH0739419B2 (ja) 新規な結晶構造を有するヒドロキシフエニルプロピオン酸エステル及びその製造法
KR102633630B1 (ko) n-헥실-2-(4-N,N-디에틸아미노-2-하이드록시벤조일)벤조에이트의 제조 방법
DE4329727C2 (de) Verfahren zur Herstellung von Hydroxyalkylaminonitrobenzol-Derivaten
KR102109210B1 (ko) 인계 (메타)아크릴레이트 화합물 및 그 제조 방법
CA1059518A (en) Process for preparing 2-hydroxymethyl-3-hydroxy-6-(1-hydroxy-2-t-butylaminoethyl) pyridine
TW201808904A (zh) 製備白克列之方法
JPH07179774A (ja) キナクリドン合成及びその中間体の製造方法
CH640226A5 (it) Procedimento in due stadi per preparare un composto di addizione mole a mole tra l'acido 2-6-piridin-bicarbossilico e l'anidride cromica.
JPS6395269A (ja) ナフタロシアニン系化合物
JPS58152855A (ja) 低級アルコキシベンゾニトリルの製法
JPS6032756A (ja) Ν−(cis−3,4−ジメトキシシンナモイル)アントラニル酸の製造方法
JPH04208252A (ja) ビス(2,3―ジヒドロキシプロピル)アミンの精製方法
JPH0368571A (ja) N―置換2、4、6―トリイミノトリアジン誘導体の製造方法
JPH0333150B2 (ja)
JPH06287176A (ja) 2−アミノ−3−ニトロピリジン類の製造方法
JP2002220390A (ja) 無水ミルタザピンおよびその製法
JPH04260607A (ja) トリチオ炭酸塩類の製造法

Legal Events

Date Code Title Description
A201 Request for examination
A302 Request for accelerated examination
E902 Notification of reason for refusal
E701 Decision to grant or registration of patent right
GRNT Written decision to grant