JPS59116135A - 石英ガラスの製造方法 - Google Patents
石英ガラスの製造方法Info
- Publication number
- JPS59116135A JPS59116135A JP22819882A JP22819882A JPS59116135A JP S59116135 A JPS59116135 A JP S59116135A JP 22819882 A JP22819882 A JP 22819882A JP 22819882 A JP22819882 A JP 22819882A JP S59116135 A JPS59116135 A JP S59116135A
- Authority
- JP
- Japan
- Prior art keywords
- quartz glass
- dry gel
- gel
- sol
- added
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title claims description 98
- 238000004519 manufacturing process Methods 0.000 title claims description 18
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 23
- 150000004703 alkoxides Chemical class 0.000 claims description 16
- 239000002184 metal Substances 0.000 claims description 16
- 239000002994 raw material Substances 0.000 claims description 14
- 239000000377 silicon dioxide Substances 0.000 claims description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- 238000002360 preparation method Methods 0.000 claims description 10
- 238000003980 solgel method Methods 0.000 claims description 9
- 239000000843 powder Substances 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 4
- 239000003513 alkali Substances 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims 1
- 238000001308 synthesis method Methods 0.000 claims 1
- 239000000499 gel Substances 0.000 description 70
- 238000000034 method Methods 0.000 description 42
- 238000005245 sintering Methods 0.000 description 23
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 16
- 238000005336 cracking Methods 0.000 description 14
- 230000000704 physical effect Effects 0.000 description 13
- 239000000243 solution Substances 0.000 description 12
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 description 8
- 238000006460 hydrolysis reaction Methods 0.000 description 8
- 239000011521 glass Substances 0.000 description 7
- 238000001879 gelation Methods 0.000 description 6
- 230000003287 optical effect Effects 0.000 description 6
- -1 alkyl silicate Chemical compound 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 5
- 230000007062 hydrolysis Effects 0.000 description 5
- 238000003756 stirring Methods 0.000 description 5
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 4
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 3
- 239000004743 Polypropylene Substances 0.000 description 3
- 238000000862 absorption spectrum Methods 0.000 description 3
- 235000011114 ammonium hydroxide Nutrition 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- 238000007796 conventional method Methods 0.000 description 3
- 230000003301 hydrolyzing effect Effects 0.000 description 3
- 238000002844 melting Methods 0.000 description 3
- 230000008018 melting Effects 0.000 description 3
- 229920001155 polypropylene Polymers 0.000 description 3
- 239000003054 catalyst Substances 0.000 description 2
- 239000000919 ceramic Substances 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 239000003365 glass fiber Substances 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 229910002012 Aerosil® Inorganic materials 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 235000016496 Panda oleosa Nutrition 0.000 description 1
- 240000000220 Panda oleosa Species 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 239000004809 Teflon Substances 0.000 description 1
- 229920006362 Teflon® Polymers 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- DKAGJZJALZXOOV-UHFFFAOYSA-N hydrate;hydrochloride Chemical compound O.Cl DKAGJZJALZXOOV-UHFFFAOYSA-N 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 229920000915 polyvinyl chloride Polymers 0.000 description 1
- 239000004800 polyvinyl chloride Substances 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B19/00—Other methods of shaping glass
- C03B19/12—Other methods of shaping glass by liquid-phase reaction processes
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Manufacture, Treatment Of Glass Fibers (AREA)
- Glass Compositions (AREA)
- Silicon Compounds (AREA)
- Glass Melting And Manufacturing (AREA)
Priority Applications (10)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP22819882A JPS59116135A (ja) | 1982-12-23 | 1982-12-23 | 石英ガラスの製造方法 |
| DE19833390375 DE3390375T1 (de) | 1982-12-23 | 1983-12-22 | Verfahren zur Herstellung von Siliciumdioxidglas |
| GB08418301A GB2140408B (en) | 1982-12-23 | 1983-12-22 | Process for producing quartz glass |
| US06/642,606 US4681615A (en) | 1982-12-23 | 1983-12-22 | Silica glass formation process |
| EP84900294A EP0131057B1 (en) | 1982-12-23 | 1983-12-22 | Process for producing quartz glass |
| NLAANVRAGE8320410,A NL188795C (nl) | 1982-12-23 | 1983-12-22 | Werkwijze voor het vervaardigen van een kwartsglas. |
| PCT/JP1983/000450 WO1984002519A1 (en) | 1982-12-23 | 1983-12-22 | Process for producing quartz glass |
| US07/008,226 US4801318A (en) | 1982-12-23 | 1987-01-29 | Silica glass formation process |
| SG395/88A SG39588G (en) | 1982-12-23 | 1988-06-20 | A process of forming silica glass |
| HK695/89A HK69589A (en) | 1982-12-23 | 1989-08-31 | A process of forming silica glass |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP22819882A JPS59116135A (ja) | 1982-12-23 | 1982-12-23 | 石英ガラスの製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS59116135A true JPS59116135A (ja) | 1984-07-04 |
| JPS64331B2 JPS64331B2 (enrdf_load_stackoverflow) | 1989-01-06 |
Family
ID=16872732
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP22819882A Granted JPS59116135A (ja) | 1982-12-23 | 1982-12-23 | 石英ガラスの製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS59116135A (enrdf_load_stackoverflow) |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6027611A (ja) * | 1983-07-22 | 1985-02-12 | Hitachi Ltd | 添加形シリカゲルの製造方法 |
| JPS6126521A (ja) * | 1984-07-12 | 1986-02-05 | Seiko Epson Corp | 石英ガラスの製造方法 |
| JPS6140825A (ja) * | 1984-07-31 | 1986-02-27 | Seiko Epson Corp | 石英ガラスの製造方法 |
| JPS6144720A (ja) * | 1984-08-07 | 1986-03-04 | Seiko Epson Corp | 石英ガラスの製造方法 |
| JPS6191033A (ja) * | 1984-10-05 | 1986-05-09 | Seiko Epson Corp | 光フアイバ用母材の製造方法 |
| JPS6191022A (ja) * | 1984-09-20 | 1986-05-09 | Seiko Epson Corp | 石英ガラスの製造方法 |
| JPS6191021A (ja) * | 1984-09-20 | 1986-05-09 | Seiko Epson Corp | 石英ガラスの製造方法 |
| DE3623843A1 (de) * | 1985-07-16 | 1987-01-22 | Seiko Epson Corp | Verfahren zur herstellung von quarzglas |
| US4937208A (en) * | 1988-02-19 | 1990-06-26 | Tohru Yamamoto | Catalyst for sol-gel method using metal alkoxide and sol-gel method using the same |
| EP1661866A1 (en) * | 2004-11-27 | 2006-05-31 | Degussa AG | Method for the production of shaped silica aquagels |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS4893636A (enrdf_load_stackoverflow) * | 1972-03-15 | 1973-12-04 | ||
| JPS56125240A (en) * | 1980-03-07 | 1981-10-01 | Natl Inst For Res In Inorg Mater | Preparation of silica glass |
| JPS5711845A (en) * | 1980-06-20 | 1982-01-21 | Natl Inst For Res In Inorg Mater | Production of colored silica glass |
| JPS64330A (en) * | 1987-06-23 | 1989-01-05 | Atsugi Motor Parts Co Ltd | Compression ratio variable device for internal combustion engine |
-
1982
- 1982-12-23 JP JP22819882A patent/JPS59116135A/ja active Granted
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS4893636A (enrdf_load_stackoverflow) * | 1972-03-15 | 1973-12-04 | ||
| JPS56125240A (en) * | 1980-03-07 | 1981-10-01 | Natl Inst For Res In Inorg Mater | Preparation of silica glass |
| JPS5711845A (en) * | 1980-06-20 | 1982-01-21 | Natl Inst For Res In Inorg Mater | Production of colored silica glass |
| JPS64330A (en) * | 1987-06-23 | 1989-01-05 | Atsugi Motor Parts Co Ltd | Compression ratio variable device for internal combustion engine |
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6027611A (ja) * | 1983-07-22 | 1985-02-12 | Hitachi Ltd | 添加形シリカゲルの製造方法 |
| JPS6126521A (ja) * | 1984-07-12 | 1986-02-05 | Seiko Epson Corp | 石英ガラスの製造方法 |
| JPS6140825A (ja) * | 1984-07-31 | 1986-02-27 | Seiko Epson Corp | 石英ガラスの製造方法 |
| JPS6144720A (ja) * | 1984-08-07 | 1986-03-04 | Seiko Epson Corp | 石英ガラスの製造方法 |
| JPS6191022A (ja) * | 1984-09-20 | 1986-05-09 | Seiko Epson Corp | 石英ガラスの製造方法 |
| JPS6191021A (ja) * | 1984-09-20 | 1986-05-09 | Seiko Epson Corp | 石英ガラスの製造方法 |
| JPS6191033A (ja) * | 1984-10-05 | 1986-05-09 | Seiko Epson Corp | 光フアイバ用母材の製造方法 |
| DE3623843A1 (de) * | 1985-07-16 | 1987-01-22 | Seiko Epson Corp | Verfahren zur herstellung von quarzglas |
| US4937208A (en) * | 1988-02-19 | 1990-06-26 | Tohru Yamamoto | Catalyst for sol-gel method using metal alkoxide and sol-gel method using the same |
| EP1661866A1 (en) * | 2004-11-27 | 2006-05-31 | Degussa AG | Method for the production of shaped silica aquagels |
| WO2006056291A1 (en) * | 2004-11-27 | 2006-06-01 | Degussa Gmbh | Method for the production of shaped silica aquagels |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS64331B2 (enrdf_load_stackoverflow) | 1989-01-06 |
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