JP6204346B2 - エアゾール製品とその製造方法 - Google Patents
エアゾール製品とその製造方法 Download PDFInfo
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- JP6204346B2 JP6204346B2 JP2014508047A JP2014508047A JP6204346B2 JP 6204346 B2 JP6204346 B2 JP 6204346B2 JP 2014508047 A JP2014508047 A JP 2014508047A JP 2014508047 A JP2014508047 A JP 2014508047A JP 6204346 B2 JP6204346 B2 JP 6204346B2
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- B65B7/00—Closing containers or receptacles after filling
- B65B7/16—Closing semi-rigid or rigid containers or receptacles not deformed by, or not taking-up shape of, contents, e.g. boxes or cartons
- B65B7/28—Closing semi-rigid or rigid containers or receptacles not deformed by, or not taking-up shape of, contents, e.g. boxes or cartons by applying separate preformed closures, e.g. lids, covers
- B65B7/2842—Securing closures on containers
- B65B7/285—Securing closures on containers by deformation of the closure
- B65B7/2857—Securing closures on containers by deformation of the closure and the container rim
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D83/00—Containers or packages with special means for dispensing contents
- B65D83/14—Containers or packages with special means for dispensing contents for delivery of liquid or semi-liquid contents by internal gaseous pressure, i.e. aerosol containers comprising propellant for a product delivered by a propellant
- B65D83/42—Filling or charging means
- B65D83/425—Delivery valves permitting filling or charging
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D83/00—Containers or packages with special means for dispensing contents
- B65D83/14—Containers or packages with special means for dispensing contents for delivery of liquid or semi-liquid contents by internal gaseous pressure, i.e. aerosol containers comprising propellant for a product delivered by a propellant
- B65D83/60—Contents and propellant separated
- B65D83/62—Contents and propellant separated by membrane, bag, or the like
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D83/00—Containers or packages with special means for dispensing contents
- B65D83/14—Containers or packages with special means for dispensing contents for delivery of liquid or semi-liquid contents by internal gaseous pressure, i.e. aerosol containers comprising propellant for a product delivered by a propellant
- B65D83/68—Dispensing two or more contents, e.g. sequential dispensing or simultaneous dispensing of two or more products without mixing them
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
- A61K2800/432—Direct dyes
- A61K2800/4324—Direct dyes in preparations for permanently dyeing the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/87—Application Devices; Containers; Packaging
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B2220/00—Specific aspects of the packaging operation
- B65B2220/14—Adding more than one type of material or article to the same package
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B2230/00—Aspects of the final package
- B65B2230/02—Containers having separate compartments isolated from one another
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D83/00—Containers or packages with special means for dispensing contents
- B65D83/14—Containers or packages with special means for dispensing contents for delivery of liquid or semi-liquid contents by internal gaseous pressure, i.e. aerosol containers comprising propellant for a product delivered by a propellant
- B65D83/38—Details of the container body
Description
カバー部は、その上底にエアゾールバルブのステムを通す2つの挿通孔を有している。また、カバー部は、その上底の下面と各エアゾールバルブ71aおよび71bのカバーの上面とが当接するように下方に押し付けられた状態でカシメられており、上面に凹み部が形成されている。
試験用エアゾール製品を40℃で3箇月間正立状態で静置して保存し、このエアゾール組成物(または加圧組成物)と、酸化染料の酸化剤として過酸化水素を含む第2剤用エアゾール組成物(または加圧組成物)を、等重量混合して毛束に塗布し、染毛状態を評価した。なお評価は保存前に染めた毛束(コントロール品)との相対比較である。
◎:コントロール品とほとんど同じ色に染まった。
○:コントロール品よりも若干染まりが弱いが問題ない程度。
×:コントロール品よりも明らかに染まりが不充分。
吐出物の性能評価後、エアゾール組成物(または加圧組成物)を吐出して全量吐出できるか確認した。
○:全量吐出できた。
×:吐出途中で詰まりが発生し、吐出できなくなった。
エアゾール組成物(または加圧組成物)を全量吐出した後、各試験用エアゾール製品を解体して、ハウジング内部の状態を目視で評価した。なお、全量吐出性能評価において全量吐出できなかったものはエアゾール容器に穴をあけて、エアゾール組成物(または加圧組成物)を全量吐出させた。
◎:析出物(酸化染料の酸化物)はなかった。
○:析出物(酸化染料の酸化物)は存在したが、微量であった。
×:析出物(酸化染料の酸化物)が多数存在した。
実施例1(不活性成分として窒素ガスを使用)
下記の成分を含有する水性原液1(2液式染毛剤の第1剤)を調製し、図1cに示すエアゾール容器の内部容器に充填した。容器本体の開口部にエアゾールバルブを固着し、エアゾールバルブのステムから液化ガスとして液化石油ガスを充填した。さらに、不活性成分として窒素ガスをエアゾールバルブのステムから充填した。窒素ガスは液化石油ガス充填後のエアゾール容器内の圧力よりも0.1MPa高くなるまで充填し、エアゾールバルブの噴射通路から液化石油ガスを内部容器内に完全に排出した。なお、このエアゾール組成物は水性原液中に液化石油ガスが均一に分散し分離しないものである。
酸化染料:パラフェニレンジアミン、パラアミノフェノール
補助成分:5−アミノオルトクレゾール、レゾルシン
界面活性剤:ラウリルグルコシド、モノラウリン酸デカグリセリン、ラウリルジメチルアミンオキシド
アルカリ剤:モノエタノールアミン、アンモニア水
安定化剤:HEDTA・3Na2水塩
溶媒:精製水、グリセリン、ジプロピレングリコール
その他:セタノール、香料
不活性成分として窒素ガスの代わりにメチルポリシロキサン(10cs)を1g充填し、噴射通路全体をメチルポリシロキサンで満たしたこと以外は実施例1と同様にしてエアゾール製品を製造した。
不活性成分として窒素ガスの代わりにミリスチン酸イソプロピルを1g充填し、噴射通路全体をミリスチン酸イソプロピルで満たしたこと以外は実施例1と同様にしてエアゾール製品を製造した。
窒素ガスを充填しなかったこと以外は実施例1と同様にしてエアゾール製品を製造した。
窒素ガスの代わりに精製水を1g充填し、噴射通路全体を精製水で満たしたこと以外は実施例1と同様にしてエアゾール製品を製造した。
窒素ガスの代わりにエタノールを1g充填し、噴射通路全体をエタノールで満たしたこと以外は実施例1と同様にしてエアゾール製品を製造した。
図2aに示すエアゾール容器を使用し、窒素ガスを充填しなかったこと以外は実施例1と同様にしてエアゾール製品を製造した。
液化石油ガスの代わりに、2MPa下で液化石油ガスに窒素ガスを溶解させた溶解液化ガスを充填し、窒素ガスを充填しなかったこと以外は実施例1と同様にしてエアゾール製品を製造した。
実施例6(不活性成分として窒素ガスを使用)
下記の成分を含有する水性原液2(2液式染毛剤の第1剤)を調製し、図1aに示すエアゾール容器の内部容器に充填した。容器本体の開口部にエアゾールバルブを固着し、エアゾールバルブのステムから液化ガスとして液化石油ガスを充填した。さらに、不活性成分として窒素ガスをエアゾールバルブのステムから充填した。窒素ガスは液化石油ガス充填後のエアゾール容器内の圧力よりも0.1MPa高くなるまで充填し、エアゾールバルブの噴射通路から液化石油ガスを内部容器内に完全に排出した。なお、このエアゾール組成物は水性原液と液化石油ガスが分離するものである。
酸化染料:パラフェニレンジアミン、パラアミノフェノール
補助成分:5−アミノオルトクレゾール、レゾルシン
界面活性剤:POEラウリルエーテル、POEセチルエーテル、POEオレイルエーテル
アルカリ剤:モノエタノールアミン、アンモニア水
安定化剤:HEDTA・3Na2水塩
溶媒:精製水、プロピレングリコール
その他:セタノール、香料
不活性成分として窒素ガスの代わりにメチルポリシロキサン(10cs)を1g充填し、噴射通路全体をメチルポリシロキサンで満たしたこと以外は実施例6と同様にしてエアゾール製品を製造した。
不活性成分として窒素ガスの代わりにミリスチン酸イソプロピルを1g充填し、噴射通路全体をミリスチン酸イソプロピルで満たしたこと以外は実施例6と同様にしてエアゾール製品を製造した。
窒素ガスを充填しなかったこと以外は実施例6と同様にしてエアゾール製品を製造した。
窒素ガスの代わりに精製水を1g充填し、噴射通路全体を精製水で満たしたこと以外は実施例6と同様にしてエアゾール製品を製造した。
窒素ガスの代わりにエタノールを1g充填し、噴射通路全体をエタノールで満たしたこと以外は実施例6と同様にしてエアゾール製品を製造した。
図2aに示すエアゾール容器を使用し、窒素ガスを充填しなかったこと以外は実施例6と同様にしてエアゾール製品を製造した。
窒素ガスの代わりに精製水を0.3g充填し、ディップチューブ内で精製水と液化石油ガスが分離したこと以外は実施例6と同様にしてエアゾール製品を製造した。
液化石油ガスの代わりに、2MPa下で液化石油ガスに窒素ガスを溶解させた溶解液化ガスを充填し、窒素ガスを充填しなかったこと以外は実施例6と同様にしてエアゾール製品を製造した。
実施例12(不活性成分として窒素ガスを使用)
下記の成分を含有する水性原液3(2液式染毛剤の第1剤)および水性原液4(2液式染毛剤の第2剤)を調製し、図7に示すエアゾール容器の内部容器の下収納部15aに水性原液3を充填し、チューブが挿入された中栓をくびれ部に装着して、上収納部15bに水性原液4を充填した。次いで、エアゾールバルブのマウンティングキャップの環状壁を内部容器の開口部に嵌合して内部容器を閉じると共に、チューブをハウジングの下部に装着した。さらに、内部容器と外部容器との間に窒素ガスをアンダーカップ充填し、マウンティングキャップの環状壁を外側にクリンプして固着した。そして、エアゾールバルブのステムを押し下げて、噴射剤の圧力によりハウジング下部空間およびチューブ内の空気、ならびにハウジング上部空間の空気を排出した。この排出工程で水性原液3がハウジング下部空間とチューブ内に導入され、また、水性原液4がハウジング上部空間に導入されるが、ステムから不活性成分E(窒素ガス)を、充填することで、ハウジング下部空間およびチューブ65内の水性原液3とハウジング上部空間内の水性原液4をそれぞれ下収納部と上収納部に完全に排出した。
酸化染料:パラフェニレンジアミン、パラアミノフェノール
補助成分:5−アミノオルトクレゾール、レゾルシン
界面活性剤:POEオレイルエーテル、POEステアリルエーテル
アルカリ剤:アンモニア水
安定化剤:HEDTA・3Na2水塩
溶媒:精製水
その他:ステアリルアルコール、エチルヘキサン酸エチル、香料
酸化剤:過酸化水素水
界面活性剤:POEベヘニルエーテル
pH調整剤:クエン酸、クエン酸ナトリウム
溶媒:精製水、イソプロパノール、プロピレングリコール
その他:ベヘニルアルコール、セタノール、ラノリン
図8に示す容器本体の開口部に、パウチを2個装着したバルブアッセンブリの栓部を挿入し、容器本体と2つのパウチの間に噴射剤(窒素ガス)をアンダーカップ充填し、バルブアッセンブリを容器本体に固着した。次いで、エアゾールバルブの各ステムを押し下げて、噴射剤(窒素ガス)の圧力により噴射通路(パウチ内およびディップチューブ内)の空気を外部に排出した。その後、各ステムから各パウチへ水性原液3(2液式染毛剤の第1剤)および4(2液式染毛剤の第2剤)を充填した。さらに、不活性成分として窒素ガスをステムから充填し、噴射通路(ハウジング内およびディップチューブ内)から水性原液をパウチ内に完全に排出した。
窒素ガスを充填しなかったこと以外は実施例12と同様にしてエアゾール製品を製造した。
窒素ガスを充填しなかったこと以外は実施例13と同様にしてエアゾール製品を製造した。
101 1剤用エアゾール容器
102 2剤用エアゾール容器
103 吐出部材
11 外部容器
12 内部容器
13 外部容器
14 内部容器
15 内部容器
15a 下収納部
15b 上収納部
16 外部容器
17 内部容器
17a 第1パウチ
17b 第2パウチ
20 エアゾールバルブ
21 マウンティングキャップ
22 カバーキャップ
23 ガスケット
24 ハウジング
240 ハウジング内部
241 導入孔
25 ステム
250 ステム内通路
251 ステム孔
26 ステムラバー
27 スプリング
28 ディップチューブ
29 横溝
30 エアゾールバルブ
40 エアゾールバルブ
41 ハウジング
410 ハウジング内部
42 カバーキャップ
43 ガスケット
44 ステム
440 ステム孔
45 ステムラバー
46 スプリング
47 ディップチューブ
48 環状ラバー
49 連通孔
50 エアゾールバルブ
60 エアゾールバルブ
61 マウンティングキャップ
62 ハウジング
620 ハウジング内部
621a、b 導入孔
63 ステム
630a、b ステム内通路
631a、b ステム孔
64a、b ステムラバー
65 チューブ
66 中栓
70 バルブアッセンブリ
71a 第1エアゾールバルブ
71b 第2エアゾールバルブ
72a 第1ディップチューブ
72b 第2ディップチューブ
73 バルブホルダー
731 栓部
732 蓋部
733 フランジ部
734 凹部
74 マウンテンカバー
75 O−リング
76a 第1ハウジング
76b 第2ハウジング
77a、b O−リング
A 水性原液
Aa、b 内容物
B 液化ガスの液層
C 液化ガスの気層
D 水性原液に液化ガスの液層が均一に分散した液層
E 不活性成分
Ea、b 不活性成分
F 不活性成分
G 噴射剤
X 液相
Y 気相
Claims (6)
- 容器本体の開口部にエアゾールバルブが固着されたエアゾール容器に、
水性原液および噴射剤が充填されたエアゾール製品であって、
前記エアゾール容器は、外部容器と、第1パウチおよび第2パウチを含む内部容器と、バルブアッセンブリとを備え、
前記バルブアッセンブリは、
前記外部容器を閉じるバルブホルダーと、
前記バルブホルダーに保持され、前記第1パウチを閉じる第1エアゾールバルブおよび前記第2パウチを閉じる第2エアゾールバルブと、を備え、
前記第1パウチおよび前記第2パウチに充填された前記水性原液のうち、少なくともいずれか一方の水性原液は、酸素反応性の有効成分を含有しており、
前記酸素反応性の有効成分を含有する水性原液が充填されている方のエアゾールバルブの噴射通路の少なくとも一部に不活性成分を有するエアゾール製品。 - 前記酸素反応性の有効成分は、酸化染料であり、
前記水性原液は、前記酸化染料を含む第1剤と、第2剤とからなる2液式染毛剤であり、
前記第1剤は、前記第1パウチおよび前記第2パウチのいずれか一方に充填されており、
前記第2剤は、前記第1パウチおよび前記第2パウチのうち、他のいずれか一方に充填されている、請求項1記載のエアゾール製品。 - 前記不活性成分が気体である請求項1または2記載のエアゾール製品。
- 容器本体の開口部にエアゾールバルブが固着されたエアゾール容器に、水性原液および噴射剤が充填されたエアゾール製品であり、前記水性原液が酸素反応性の有効成分を含み、前記エアゾールバルブの噴射通路の少なくとも一部に不活性成分を有し、
前記噴射剤が液化ガスであり、
前記エアゾール容器に水性原液と液化ガスとからなるエアゾール組成物が充填されており、
前記不活性成分が気体であるエアゾール製品の製造方法であり、
容器本体に水性原液を充填し、エアゾールバルブを固着する工程、
気体の不活性成分を液化ガスに溶解させた溶解液化ガスをエアゾールバルブから充填する工程、
エアゾールバルブの噴射通路内で気体の不活性成分の一部を溶解液化ガスから気化させる工程を有するエアゾール製品の製造方法。 - 容器本体の開口部にエアゾールバルブが固着されたエアゾール容器に、水性原液および噴射剤が充填されたエアゾール製品であり、前記水性原液が酸素反応性の有効成分を含み、前記エアゾールバルブの噴射通路の少なくとも一部に不活性成分を有し、
前記容器本体は、外部容器と内部容器とからなり、
内部容器に水性原液が充填され、外部容器と内部容器の間に噴射剤が充填され、内部容器を介して水性原液が加圧されエアゾール製品の製造方法であり、
内部容器に水性原液を充填する工程、
外部容器と内部容器の間に噴射剤を充填し、エアゾールバルブを固着する工程、
エアゾールバルブの噴射通路内の空気を排出する工程、
エアゾールバルブから不活性成分を充填し、噴射通路内の水性原液を内部容器内に排出する工程を有するエアゾール製品の製造方法。 - 請求項1に記載のエアゾール製品の製造方法であって、
外部容器と内部容器の間に噴射剤を充填し、前記バルブアッセンブリを固着する工程、
内部容器、前記第1エアゾールバルブおよび前記第2エアゾールバルブのそれぞれの噴射通路内の空気を排出する工程、
前記第1エアゾールバルブおよび前記第2エアゾールバルブからそれぞれの内部容器に水性原液を充填する工程において、前記第1パウチおよび前記第2パウチのうち、少なくともいずれか一方のパウチに酸素反応性の有効成分を含有する水性原液を充填する工程、
前記第1パウチおよび前記第2パウチのうち、酸素反応性の有効成分を含有する水性原液が充填されている方のエアゾールバルブから不活性成分を充填し、噴射通路内の水性原液を内部容器内に排出する工程を有するエアゾール製品の製造方法。
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