JP5251976B2 - フッ化物結晶成形体の製造方法、並びに、それにより製造された光学部材、光学部材を備える光学装置及び紫外線洗浄装置 - Google Patents
フッ化物結晶成形体の製造方法、並びに、それにより製造された光学部材、光学部材を備える光学装置及び紫外線洗浄装置 Download PDFInfo
- Publication number
- JP5251976B2 JP5251976B2 JP2010513063A JP2010513063A JP5251976B2 JP 5251976 B2 JP5251976 B2 JP 5251976B2 JP 2010513063 A JP2010513063 A JP 2010513063A JP 2010513063 A JP2010513063 A JP 2010513063A JP 5251976 B2 JP5251976 B2 JP 5251976B2
- Authority
- JP
- Japan
- Prior art keywords
- fluoride crystal
- base material
- fluoride
- crystal base
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000013078 crystal Substances 0.000 title claims description 256
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 title claims description 136
- 230000003287 optical effect Effects 0.000 title claims description 67
- 238000004519 manufacturing process Methods 0.000 title claims description 30
- 238000004140 cleaning Methods 0.000 title claims description 28
- 239000000463 material Substances 0.000 claims description 129
- 239000002585 base Substances 0.000 claims description 116
- 238000002834 transmittance Methods 0.000 claims description 35
- 238000010438 heat treatment Methods 0.000 claims description 31
- WUKWITHWXAAZEY-UHFFFAOYSA-L calcium difluoride Chemical compound [F-].[F-].[Ca+2] WUKWITHWXAAZEY-UHFFFAOYSA-L 0.000 claims description 20
- 229910001634 calcium fluoride Inorganic materials 0.000 claims description 20
- 239000011159 matrix material Substances 0.000 claims description 12
- 238000002844 melting Methods 0.000 claims description 10
- 230000008018 melting Effects 0.000 claims description 10
- 238000003825 pressing Methods 0.000 claims description 7
- 229910052783 alkali metal Inorganic materials 0.000 claims description 6
- 150000001340 alkali metals Chemical class 0.000 claims description 6
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims description 6
- 150000001342 alkaline earth metals Chemical class 0.000 claims description 6
- 229910052684 Cerium Inorganic materials 0.000 claims description 3
- 229910052804 chromium Inorganic materials 0.000 claims description 3
- 229910052742 iron Inorganic materials 0.000 claims description 3
- 229910052746 lanthanum Inorganic materials 0.000 claims description 3
- 229910052745 lead Inorganic materials 0.000 claims description 3
- 229910052748 manganese Inorganic materials 0.000 claims description 3
- 229910052725 zinc Inorganic materials 0.000 claims description 3
- 238000001953 recrystallisation Methods 0.000 description 46
- 238000000465 moulding Methods 0.000 description 30
- 238000000034 method Methods 0.000 description 18
- 230000000052 comparative effect Effects 0.000 description 13
- 239000007789 gas Substances 0.000 description 9
- 238000010521 absorption reaction Methods 0.000 description 7
- 239000012298 atmosphere Substances 0.000 description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 6
- 239000011261 inert gas Substances 0.000 description 6
- 238000005259 measurement Methods 0.000 description 6
- 230000008859 change Effects 0.000 description 5
- 229910002804 graphite Inorganic materials 0.000 description 5
- 239000010439 graphite Substances 0.000 description 5
- 238000005498 polishing Methods 0.000 description 5
- 229910052799 carbon Inorganic materials 0.000 description 4
- 230000007423 decrease Effects 0.000 description 4
- 230000001678 irradiating effect Effects 0.000 description 4
- PQXKHYXIUOZZFA-UHFFFAOYSA-M lithium fluoride Chemical compound [Li+].[F-] PQXKHYXIUOZZFA-UHFFFAOYSA-M 0.000 description 4
- 230000009466 transformation Effects 0.000 description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 230000007547 defect Effects 0.000 description 3
- 230000002542 deteriorative effect Effects 0.000 description 3
- 230000014509 gene expression Effects 0.000 description 3
- 229910052698 phosphorus Inorganic materials 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 230000003746 surface roughness Effects 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- 229910004298 SiO 2 Inorganic materials 0.000 description 2
- 238000005162 X-ray Laue diffraction Methods 0.000 description 2
- 230000004913 activation Effects 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000004973 liquid crystal related substance Substances 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 238000003754 machining Methods 0.000 description 2
- 230000035699 permeability Effects 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 239000004065 semiconductor Substances 0.000 description 2
- 238000007493 shaping process Methods 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 239000000758 substrate Substances 0.000 description 2
- 241000501754 Astronotus ocellatus Species 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 1
- 239000006061 abrasive grain Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- OYLGJCQECKOTOL-UHFFFAOYSA-L barium fluoride Chemical compound [F-].[F-].[Ba+2] OYLGJCQECKOTOL-UHFFFAOYSA-L 0.000 description 1
- 229910001632 barium fluoride Inorganic materials 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 229910000420 cerium oxide Inorganic materials 0.000 description 1
- QCCDYNYSHILRDG-UHFFFAOYSA-K cerium(3+);trifluoride Chemical compound [F-].[F-].[F-].[Ce+3] QCCDYNYSHILRDG-UHFFFAOYSA-K 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 150000002222 fluorine compounds Chemical class 0.000 description 1
- 238000005242 forging Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- 229910052734 helium Inorganic materials 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 239000011810 insulating material Substances 0.000 description 1
- 238000005304 joining Methods 0.000 description 1
- ORUIBWPALBXDOA-UHFFFAOYSA-L magnesium fluoride Chemical compound [F-].[F-].[Mg+2] ORUIBWPALBXDOA-UHFFFAOYSA-L 0.000 description 1
- 229910001635 magnesium fluoride Inorganic materials 0.000 description 1
- 238000010338 mechanical breakdown Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
- BMMGVYCKOGBVEV-UHFFFAOYSA-N oxo(oxoceriooxy)cerium Chemical compound [Ce]=O.O=[Ce]=O BMMGVYCKOGBVEV-UHFFFAOYSA-N 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
- BYMUNNMMXKDFEZ-UHFFFAOYSA-K trifluorolanthanum Chemical compound F[La](F)F BYMUNNMMXKDFEZ-UHFFFAOYSA-K 0.000 description 1
- 229940105963 yttrium fluoride Drugs 0.000 description 1
- RBORBHYCVONNJH-UHFFFAOYSA-K yttrium(iii) fluoride Chemical compound F[Y](F)F RBORBHYCVONNJH-UHFFFAOYSA-K 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F11/00—Compounds of calcium, strontium, or barium
- C01F11/20—Halides
- C01F11/22—Fluorides
-
- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B1/00—Optical elements characterised by the material of which they are made; Optical coatings for optical elements
- G02B1/02—Optical elements characterised by the material of which they are made; Optical coatings for optical elements made of crystals, e.g. rock-salt, semi-conductors
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
- C30B29/10—Inorganic compounds or compositions
- C30B29/12—Halides
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B33/00—After-treatment of single crystals or homogeneous polycrystalline material with defined structure
- C30B33/02—Heat treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Metallurgy (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Physics & Mathematics (AREA)
- Inorganic Chemistry (AREA)
- Thermal Sciences (AREA)
- General Physics & Mathematics (AREA)
- Optics & Photonics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2010513063A JP5251976B2 (ja) | 2008-05-23 | 2009-05-22 | フッ化物結晶成形体の製造方法、並びに、それにより製造された光学部材、光学部材を備える光学装置及び紫外線洗浄装置 |
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2008135239 | 2008-05-23 | ||
JP2008135239 | 2008-05-23 | ||
PCT/JP2009/059405 WO2009142284A1 (fr) | 2008-05-23 | 2009-05-22 | Procédé de production d’un article en cristal de fluorure moulé, élément optique produit selon le procédé, et dispositif optique et dispositif de lavage par rayonnement ultraviolet comprenant chacun l’élément optique |
JP2010513063A JP5251976B2 (ja) | 2008-05-23 | 2009-05-22 | フッ化物結晶成形体の製造方法、並びに、それにより製造された光学部材、光学部材を備える光学装置及び紫外線洗浄装置 |
Related Child Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2012283977A Division JP5648675B2 (ja) | 2008-05-23 | 2012-12-27 | フッ化物結晶成形体からなる光学部材、光学部材を備える光学装置及び紫外線洗浄装置 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPWO2009142284A1 JPWO2009142284A1 (ja) | 2011-09-29 |
JP5251976B2 true JP5251976B2 (ja) | 2013-07-31 |
Family
ID=41340211
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2010513063A Active JP5251976B2 (ja) | 2008-05-23 | 2009-05-22 | フッ化物結晶成形体の製造方法、並びに、それにより製造された光学部材、光学部材を備える光学装置及び紫外線洗浄装置 |
JP2012283977A Active JP5648675B2 (ja) | 2008-05-23 | 2012-12-27 | フッ化物結晶成形体からなる光学部材、光学部材を備える光学装置及び紫外線洗浄装置 |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2012283977A Active JP5648675B2 (ja) | 2008-05-23 | 2012-12-27 | フッ化物結晶成形体からなる光学部材、光学部材を備える光学装置及び紫外線洗浄装置 |
Country Status (3)
Country | Link |
---|---|
JP (2) | JP5251976B2 (fr) |
KR (2) | KR101394781B1 (fr) |
WO (1) | WO2009142284A1 (fr) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2009142284A1 (fr) * | 2008-05-23 | 2009-11-26 | 株式会社ニコン | Procédé de production d’un article en cristal de fluorure moulé, élément optique produit selon le procédé, et dispositif optique et dispositif de lavage par rayonnement ultraviolet comprenant chacun l’élément optique |
JP6233017B2 (ja) * | 2013-12-27 | 2017-11-22 | 株式会社ニコン | フッ化カルシウム光学部材、フッ化カルシウム部材の製造方法、及びフッ化カルシウム単結晶の加工方法 |
JP7042471B2 (ja) * | 2017-04-13 | 2022-03-28 | 国立大学法人東海国立大学機構 | 無機結晶材料の加工方法 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS59141500A (ja) * | 1983-02-01 | 1984-08-14 | Sumitomo Electric Ind Ltd | 光学部品の製造法 |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS59184533A (ja) * | 1983-04-04 | 1984-10-19 | Agency Of Ind Science & Technol | 3−5族化合物半導体結晶の処理方法 |
JPH0797277A (ja) * | 1993-08-02 | 1995-04-11 | Kyocera Corp | 酸化物超電導体の接合方法 |
JP3650872B2 (ja) * | 1998-07-15 | 2005-05-25 | 株式会社豊田中央研究所 | 結晶配向ビスマス層状ペロブスカイト型化合物及びその製造方法 |
JP2003034194A (ja) | 2001-07-23 | 2003-02-04 | Hiroshima Kasei Ltd | ウェザーストリップ |
WO2009142284A1 (fr) * | 2008-05-23 | 2009-11-26 | 株式会社ニコン | Procédé de production d’un article en cristal de fluorure moulé, élément optique produit selon le procédé, et dispositif optique et dispositif de lavage par rayonnement ultraviolet comprenant chacun l’élément optique |
-
2009
- 2009-05-22 WO PCT/JP2009/059405 patent/WO2009142284A1/fr active Application Filing
- 2009-05-22 JP JP2010513063A patent/JP5251976B2/ja active Active
- 2009-05-22 KR KR1020137007827A patent/KR101394781B1/ko active IP Right Grant
- 2009-05-22 KR KR1020107027598A patent/KR101330974B1/ko active IP Right Grant
-
2012
- 2012-12-27 JP JP2012283977A patent/JP5648675B2/ja active Active
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS59141500A (ja) * | 1983-02-01 | 1984-08-14 | Sumitomo Electric Ind Ltd | 光学部品の製造法 |
Also Published As
Publication number | Publication date |
---|---|
JP2013082620A (ja) | 2013-05-09 |
KR20110015621A (ko) | 2011-02-16 |
KR101330974B1 (ko) | 2013-11-18 |
KR20130041369A (ko) | 2013-04-24 |
WO2009142284A1 (fr) | 2009-11-26 |
KR101394781B1 (ko) | 2014-05-15 |
JP5648675B2 (ja) | 2015-01-07 |
JPWO2009142284A1 (ja) | 2011-09-29 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
US5908503A (en) | Low defect density diamond single crystal and a process for the production of the same | |
US20060174826A1 (en) | Tantalum based crucible | |
JP5648675B2 (ja) | フッ化物結晶成形体からなる光学部材、光学部材を備える光学装置及び紫外線洗浄装置 | |
CN114303232A (zh) | SiC衬底的制造方法 | |
TW201629281A (zh) | 碳化矽基板之表面處理方法 | |
JPH07331441A (ja) | 強化された化学蒸着ダイヤモンド | |
US20210047749A1 (en) | Diameter expansion of aluminum nitride crystals during growth by physical vapor transport | |
JP5260797B2 (ja) | 蛍石の製造方法 | |
JP5489614B2 (ja) | 光学部材の製造方法 | |
JP4839205B2 (ja) | 蛍石の製造方法 | |
JP2016175780A (ja) | フッ化物結晶及び光学部品 | |
JP4839204B2 (ja) | 蛍石 | |
JP4500531B2 (ja) | フッ化アルカリ土類金属のアズグロウン単結晶体 | |
JP2018035029A (ja) | 石英ガラスルツボの製造方法、及び石英ガラスルツボ | |
JP5876798B2 (ja) | ZnSe多結晶体およびその製造方法 | |
JP2012096955A (ja) | フッ化金属単結晶の熱処理方法 | |
JP2007051013A (ja) | フッ化カルシウム結晶の製造方法 | |
JP5682894B2 (ja) | 蛍石 | |
EP3438332A1 (fr) | Oxyde d'aluminium, procédé de production d'oxyde d'aluminium et élément optique | |
JP2005330123A (ja) | CaF2結晶の製造方法 | |
JP2005330122A (ja) | フッ化物結晶の熱処理装置および熱処理方法 | |
JP2005330145A (ja) | フッ化物結晶の製造方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20121106 |
|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20121227 |
|
A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20130205 |
|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20130215 |
|
TRDD | Decision of grant or rejection written | ||
A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 20130319 |
|
A61 | First payment of annual fees (during grant procedure) |
Free format text: JAPANESE INTERMEDIATE CODE: A61 Effective date: 20130401 |
|
R150 | Certificate of patent or registration of utility model |
Free format text: JAPANESE INTERMEDIATE CODE: R150 Ref document number: 5251976 Country of ref document: JP Free format text: JAPANESE INTERMEDIATE CODE: R150 |
|
FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20160426 Year of fee payment: 3 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |