JP5084266B2 - 向流混合反応装置 - Google Patents
向流混合反応装置 Download PDFInfo
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- JP5084266B2 JP5084266B2 JP2006552685A JP2006552685A JP5084266B2 JP 5084266 B2 JP5084266 B2 JP 5084266B2 JP 2006552685 A JP2006552685 A JP 2006552685A JP 2006552685 A JP2006552685 A JP 2006552685A JP 5084266 B2 JP5084266 B2 JP 5084266B2
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- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims description 4
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- ZMIGMASIKSOYAM-UHFFFAOYSA-N cerium Chemical compound [Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce] ZMIGMASIKSOYAM-UHFFFAOYSA-N 0.000 claims description 2
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- HSJPMRKMPBAUAU-UHFFFAOYSA-N cerium(3+);trinitrate Chemical compound [Ce+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O HSJPMRKMPBAUAU-UHFFFAOYSA-N 0.000 description 2
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Description
したがって、本発明の第1の態様によれば、第1の入口と、出口とを備える、異なる密度の2つ以上の流体を連続的に混合する向流混合反応装置であって、1つ以上のさらなる入口が上記第1の入口に対して直径方向に対向するとともに上記出口内に配置されることを特徴とする、向流混合反応装置が提供される。
まず図2を参照すると、水性流は反応装置の底部に導入され、ここで冷却が、好ましくはヒートシンクによって行われる。この溶液は上向き方向に加圧される。超臨界水は逆方向すなわち下向きに反応装置に導入される。scH2Oは、水性流よりも低密であるため、反応室内で上方に浮き上がり、それにつれて塩水溶液と密に混合することになる。この混合は効率性が高く、その結果、金属酸化物ナノ粒子が生成され、この金属酸化物ナノ粒子は下流で水性流出物と分離され得る。
反応スキーム:
以下の反応を、図4に示すリグ構成に組み込んだ本発明の混合反応装置を用いて行った。
加水分解:Ce(NO3)4+4H2O→Ce(OH)4(s)+4HNO3
脱水:Ce(OH)4→CeO2+2H2O
図5は、反応装置中の硝酸セリウムの流量の増大がもたらす影響を示す。8ml/分までは金属塩の流れが増大するにつれて表面積が増大し(65m2/g〜100m2/gまで)、8ml/分を越えると粒径が小さくなり始める、という興味深い傾向が明らかに見られる。この増大は流速と反応速度論の関係によって生じ、小さくなるのは「過剰な」金属塩が原因で、この結果、より大きな粒子が生成されると考えられる。
反応装置内における動作温度がもたらす影響、及び表面積へのその影響も、関心事の1つである。反応装置を外部から、任意の所与の臨界未満温度、亜臨界温度、又は超臨界温度に加熱することができ、表面積(及び間接的には粒径)と動作温度の関係を確立できる。反応装置内の加熱水用の入口が臨界未満で作動している場合であっても、金属塩と加熱水には温度差が依然としてあり、このため、図2に示すように、入口流の向きが管の下流出口へ上向きに変ることになる。
Claims (21)
- 高密度の流体を導入する第1の入口と、低密度の流体を導入する少なくとも1の第2の入口と、前記高密度の流体と前記低密度の流体との混合液を排出する出口と、前記出口付近に設けられ、前記低密度の流体を高温に保つことで前記高密度の流体と前記低密度の流体との温度差を維持するヒータとを備える対流混合反応装置であって、前記第2の入口が、前記第1の入口に対して反対向きに配置されるとともに前記出口内に配置されることを特徴とする、対流混合反応装置。
- 前記高密度の流体を冷却するヒートシンクを更に備えることを特徴とする、請求項1に記載の混合反応装置。
- 前記第2の入口は、成形ノズルを備えることを特徴とする、請求項1又は2に記載の混合反応装置。
- 前記成形ノズルは円錐型漏斗であることを特徴とする、請求項3に記載の混合反応装置。
- 直列に配置される、請求項1ないし4のいずれか一項に記載の複数の混合反応装置を備えることを特徴とする、混合室。
- 金属塩溶液の温度と、前記金属塩溶液とは異なる密度を有する流体の温度とを異ならせ、第1の入口を介して前記金属塩溶液を反応装置内へ導入し、前記第1の入口に対して反対向きに配置された第2の入口を介して前記流体を前記反応装置内へ導入することを備え、前記第2の入口は、前記金属塩溶液と前記流体との混合液を排出するための出口内に配置されることを特徴とする、金属ナノ粒子又は金属酸化物ナノ粒子を調製するプロセス。
- 前記反応装置は、請求項1乃至4の何れか一項に記載の反応装置であることを特徴とする、請求項6記載のプロセス。
- 前記流体は、加熱水、加圧水、又は超臨界水であることを特徴とする、請求項6又は7に記載のプロセス。
- 前記流体は、前記金属塩溶液よりも低密度であり、前記出口周辺でヒータにより高温に保たれることを特徴とする、請求項6乃至8の何れか一項に記載のプロセス。
- 前記金属塩溶液は、金属塩又は化合物の水溶液であることを特徴とする、請求項6乃至9の何れか一項に記載のプロセス。
- 前記水溶液は、ルテニウム、カドミウム、ロジウム、パラジウム、鉄、セリウム、チタン、ジルコニウム、銅、及び銀を含む遷移金属から選択される少なくとも1の金属の金属塩水溶液であることを特徴とする、請求項10に記載のプロセス。
- 前記金属塩溶液は、前記流体よりも、高密度であり低温であることを特徴とする、請求項6乃至11の何れか一項に記載のプロセス。
- 前記金属塩溶液と前記流体とを混合することを更に備え、前記金属塩溶液は金属塩水溶液であって、前記流体は超臨界水であって、前記金属塩溶液は、混合前に冷却されることを特徴とする、請求項6乃至12の何れか一項に記載のプロセス。
- 前記流体は前記金属塩溶液よりも低密度であって、前記流体は前記反応装置内へ下向きに導入されるのに対し、前記金属塩溶液は上向きに導入されることを特徴とする、請求項6乃至13の何れか一項に記載のプロセス。
- 前記第2の入口は、前記金属塩溶液と前記流体との混合を助ける円錐型ノズルを備えることを特徴とする、請求項14に記載のプロセス。
- ナノ粒子酸化セリウムを生成するのに用いられることを特徴とする、請求項6乃至15のいずれか一項に記載のプロセス。
- ナノ粒子酸化チタンを生成するのに用いられることを特徴とする、請求項6乃至15のいずれか一項に記載のプロセス。
- ナノ粒子酸化ジルコニウムを生成するのに用いられることを特徴とする、請求項6乃至15のいずれか一項に記載のプロセス。
- ナノ粒子酸化銅を生成するのに用いられることを特徴とする、請求項6乃至15のいずれか一項に記載のプロセス。
- ナノ粒子酸化銀を生成するのに用いられることを特徴とする、請求項6乃至15のいずれか一項に記載のプロセス。
- 混合された金属酸化物を生成するのに用いられることを特徴とする、請求項6乃至15のいずれか一項に記載のプロセス。
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GB0402963.3 | 2004-02-11 | ||
GBGB0402963.3A GB0402963D0 (en) | 2004-02-11 | 2004-02-11 | Counter current mixing device for two different fluids |
PCT/GB2005/000483 WO2005077505A2 (en) | 2004-02-11 | 2005-02-11 | Counter current mixing reactor |
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Families Citing this family (53)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP4461900B2 (ja) | 2004-05-10 | 2010-05-12 | 富士ゼロックス株式会社 | 微粒子分散液の送液方法、及び微粒子分散液の送液装置 |
JP4461941B2 (ja) * | 2004-07-21 | 2010-05-12 | 富士ゼロックス株式会社 | 微粒子分散液の送液方法、及び微粒子分散液の送液装置 |
EA013089B1 (ru) | 2005-12-11 | 2010-02-26 | Скф Технолоджис А/С | Получение наноразмерных материалов |
ATE538888T1 (de) | 2006-02-16 | 2012-01-15 | Univ Brigham Young | Herstellung gleichförmiger nanopartikel aus ultrahochreinen metalloxiden, mischmetalloxiden, metallen und metalllegierungen |
JP5223065B2 (ja) * | 2007-03-16 | 2013-06-26 | 国立大学法人 岡山大学 | マイクロミキサー |
EP2140930A1 (en) * | 2007-03-16 | 2010-01-06 | National University Corporation Okayama University | Micromixer |
JP5232983B2 (ja) * | 2007-03-16 | 2013-07-10 | 国立大学法人 岡山大学 | マイクロミキサー |
FR2915405B1 (fr) * | 2007-04-30 | 2011-09-09 | Areva Np | Preparation de particules minerales en milieu co2 supercritique |
US8715378B2 (en) | 2008-09-05 | 2014-05-06 | Turbulent Energy, Llc | Fluid composite, device for producing thereof and system of use |
US9708185B2 (en) * | 2007-09-07 | 2017-07-18 | Turbulent Energy, Llc | Device for producing a gaseous fuel composite and system of production thereof |
US9144774B2 (en) * | 2009-09-22 | 2015-09-29 | Turbulent Energy, Llc | Fluid mixer with internal vortex |
US20100281766A1 (en) * | 2007-09-07 | 2010-11-11 | David Livshits | Dynamic Mixing of Fluids |
US9310076B2 (en) | 2007-09-07 | 2016-04-12 | Turbulent Energy Llc | Emulsion, apparatus, system and method for dynamic preparation |
US8871090B2 (en) | 2007-09-25 | 2014-10-28 | Turbulent Energy, Llc | Foaming of liquids |
JP2009081301A (ja) * | 2007-09-26 | 2009-04-16 | Toyo Tanso Kk | 太陽電池ユニット |
FR2948034B1 (fr) | 2009-07-20 | 2011-08-19 | Centre Nat Rech Scient | Synthese de particules par thermohydrolyse de precurseurs mineraux |
US8844495B2 (en) | 2009-08-21 | 2014-09-30 | Tubulent Energy, LLC | Engine with integrated mixing technology |
US9192901B2 (en) | 2010-05-25 | 2015-11-24 | Ucl Business Plc | Co-current mixer, apparatus, reactor and method for precipitating nanoparticles |
WO2012020986A2 (ko) * | 2010-08-11 | 2012-02-16 | 주식회사 엘지화학 | 무기화합물의 제조장치 및 이를 사용한 무기화합물의 제조방법 |
FR2979842B1 (fr) * | 2011-09-09 | 2013-10-04 | Commissariat Energie Atomique | Procede de synthese en continu de nanoparticules en oxyde metallique par reaction hydrothermale en milieu supercritique |
KR101643428B1 (ko) * | 2011-11-07 | 2016-07-28 | 주식회사 엘지화학 | 양극 활물질의 제조장치 및 이에 구비되는 교반장치 |
KR101655921B1 (ko) * | 2011-11-07 | 2016-09-09 | 주식회사 엘지화학 | 양극 활물질의 제조장치 및 이에 구비되는 교반장치 |
WO2013103762A1 (en) * | 2012-01-04 | 2013-07-11 | Virginia Commonwealth University | Non-rare earth magnetic nanoparticles |
US9079164B2 (en) | 2012-03-26 | 2015-07-14 | Brigham Young University | Single reaction synthesis of texturized catalysts |
US9114378B2 (en) | 2012-03-26 | 2015-08-25 | Brigham Young University | Iron and cobalt based fischer-tropsch pre-catalysts and catalysts |
KR101471433B1 (ko) * | 2012-05-31 | 2014-12-10 | 주식회사 엘지화학 | 무기 입자의 제조방법 |
CN102897823B (zh) * | 2012-07-26 | 2014-01-15 | 北京科技大学 | 一种超临界水体系氧化制备纳米CeO2粉末装置及工艺 |
RU2538585C2 (ru) * | 2012-08-31 | 2015-01-10 | Общество с ограниченной ответственностью "Инновационные Технологии Синтеза" | Способ получения нанодисперсных оксидов металлов |
JP5884708B2 (ja) * | 2012-10-23 | 2016-03-15 | 住友金属鉱山株式会社 | 銀粉の製造方法及びその製造装置 |
KR101565303B1 (ko) | 2012-11-27 | 2015-11-03 | 주식회사 엘지화학 | 수열 합성 장치 및 이를 사용한 양극 활물질의 제조방법 |
KR101565298B1 (ko) | 2012-11-27 | 2015-11-03 | 주식회사 엘지화학 | 무기화합물의 제조장치 및 이를 사용한 무기화합물의 제조방법 |
KR102255664B1 (ko) | 2013-01-15 | 2021-05-24 | 더 유니버시티 오브 노팅햄 | 혼합 반응기 및 관련된 공정 |
US9289750B2 (en) | 2013-03-09 | 2016-03-22 | Brigham Young University | Method of making highly porous, stable aluminum oxides doped with silicon |
CN103331455B (zh) * | 2013-07-19 | 2016-04-13 | 四川大学 | 一种放电微等离子体辅助的金属纳米材料连续制备方法 |
GB201320417D0 (en) | 2013-11-19 | 2014-01-01 | Univ Nottingham | Mixing reactors |
FR3027822A1 (fr) * | 2014-11-03 | 2016-05-06 | Guy Baret | Preparation de nanoparticules par traitement d'une solution en milieu hydrothermal |
JP6080317B2 (ja) * | 2015-01-30 | 2017-02-15 | 関東電化工業株式会社 | 無機微粒子の製造方法 |
JP6488152B2 (ja) * | 2015-02-27 | 2019-03-20 | 富士フイルム株式会社 | 酸化第二銅微粒子の製造方法及び酸化第二銅微粒子 |
US9802176B2 (en) | 2015-03-24 | 2017-10-31 | Saudi Arabian Oil Company | Method for mixing in a hydrocarbon conversion process |
EP3302423B1 (en) | 2015-06-04 | 2022-05-25 | Crititech, Inc. | Particle production system and particle collection device |
GB201602552D0 (en) | 2016-02-12 | 2016-03-30 | Univ Nottingham | Enhanced fabric |
KR102490665B1 (ko) | 2016-04-04 | 2023-01-27 | 크리티테크, 인크. | 고형 종양의 치료 방법 |
JP6726745B2 (ja) * | 2016-07-22 | 2020-07-22 | 富士フイルム株式会社 | 酸化銅微粒子の製造方法及び分散液 |
US10626021B2 (en) | 2017-03-31 | 2020-04-21 | Honda Motor Co., Ltd. | Method of making metal and metal oxide nanoparticles |
WO2018227037A1 (en) | 2017-06-09 | 2018-12-13 | Crititech, Inc. | Treatment of epithelial cysts by intracystic injection of antineoplastic particles |
CN115919815A (zh) | 2017-06-14 | 2023-04-07 | 克里蒂泰克公司 | 治疗肺部疾病的方法 |
SG11202001802YA (en) | 2017-10-03 | 2020-03-30 | Crititech Inc | Local delivery of antineoplastic particles in combination with systemic delivery of immunotherapeutic agents for the treatment of cancer |
GB201721808D0 (en) | 2017-12-22 | 2018-02-07 | Sensient Colors Uk Ltd | Nanaoparticle dispersions |
GB201811076D0 (en) | 2018-07-05 | 2018-08-22 | Sensient Colors Uk Ltd | Nanoparticle dispersions |
CN109928417B (zh) * | 2019-02-28 | 2022-03-22 | 昆明理工大学 | 一种白色纯氧化铈的制备方法 |
DE102019120020A1 (de) * | 2019-07-24 | 2021-01-28 | Analytik Jena Ag | Herstellung von Nanopartikeln |
CN113750926B (zh) * | 2021-09-18 | 2023-01-10 | 浙江工业大学 | 一种适用于强放热体系的反应装置 |
GB2625824A (en) | 2022-12-30 | 2024-07-03 | Promethean Particles Ltd | Mixing reactors |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2692764A (en) * | 1951-01-19 | 1954-10-26 | Howe Baker Corp | Mixing apparatus |
US2768123A (en) * | 1953-04-01 | 1956-10-23 | Exxon Research Engineering Co | Process and apparatus for treating hydrocarbon oils with immiscible reagents |
US3726297A (en) | 1971-04-14 | 1973-04-10 | Technicon Instr | Method and device for introducing for mixing a first liquid into a second liquid |
JPS61238330A (ja) * | 1985-04-12 | 1986-10-23 | Mitsui Petrochem Ind Ltd | 乳化装置 |
US4963329A (en) * | 1987-03-02 | 1990-10-16 | Turbotak Inc. | Gas reacting apparatus and method |
JP3051945B2 (ja) * | 1991-07-22 | 2000-06-12 | 大阪瓦斯株式会社 | 無機質均一微小球体、及びその製造方法 |
GB9703673D0 (en) * | 1997-02-21 | 1997-04-09 | Bradford Particle Design Ltd | Method and apparatus for the formation of particles |
JPH11128707A (ja) * | 1997-10-29 | 1999-05-18 | Shimizu Corp | 大量の液体に少量の液体を混合する装置 |
GB0117696D0 (en) | 2001-07-20 | 2001-09-12 | Bradford Particle Design Plc | Particle information |
US7718099B2 (en) | 2002-04-25 | 2010-05-18 | Tosoh Corporation | Fine channel device, fine particle producing method and solvent extraction method |
DE20306915U1 (de) * | 2003-05-05 | 2003-08-07 | HAAGEN & RINAU Mischtechnik GmbH, 28307 Bremen | Dispergiervorrichtung |
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2004
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Also Published As
Publication number | Publication date |
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DK1713569T3 (da) | 2009-10-12 |
CN103831074A (zh) | 2014-06-04 |
CN1917936A (zh) | 2007-02-21 |
CA2597480C (en) | 2012-08-07 |
JP2007526113A (ja) | 2007-09-13 |
EP1713569A2 (en) | 2006-10-25 |
GB0402963D0 (en) | 2004-03-17 |
WO2005077505A2 (en) | 2005-08-25 |
ES2327755T3 (es) | 2009-11-03 |
CN103831074B (zh) | 2019-10-25 |
EP1713569B1 (en) | 2009-06-03 |
ATE432761T1 (de) | 2009-06-15 |
KR101153043B1 (ko) | 2012-06-04 |
AU2005211990B2 (en) | 2010-07-29 |
US20070206435A1 (en) | 2007-09-06 |
KR20070001999A (ko) | 2007-01-04 |
AU2005211990A1 (en) | 2005-08-25 |
DE602005014740D1 (de) | 2009-07-16 |
WO2005077505A3 (en) | 2005-11-10 |
CA2597480A1 (en) | 2005-08-25 |
US7566436B2 (en) | 2009-07-28 |
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