WO2005077505B1 - Counter current mixing reactor - Google Patents
Counter current mixing reactorInfo
- Publication number
- WO2005077505B1 WO2005077505B1 PCT/GB2005/000483 GB2005000483W WO2005077505B1 WO 2005077505 B1 WO2005077505 B1 WO 2005077505B1 GB 2005000483 W GB2005000483 W GB 2005000483W WO 2005077505 B1 WO2005077505 B1 WO 2005077505B1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- mixing
- fluids
- fluid
- inlet
- reactor
- Prior art date
Links
- 239000012530 fluid Substances 0.000 claims abstract 32
- 239000012266 salt solution Substances 0.000 claims abstract 6
- 229910044991 metal oxide Inorganic materials 0.000 claims abstract 5
- 150000004706 metal oxides Chemical class 0.000 claims abstract 5
- 239000002105 nanoparticle Substances 0.000 claims abstract 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract 4
- 238000004519 manufacturing process Methods 0.000 claims abstract 3
- 229910052751 metal Inorganic materials 0.000 claims 9
- 239000002184 metal Substances 0.000 claims 9
- 239000000243 solution Substances 0.000 claims 3
- NDVLTYZPCACLMA-UHFFFAOYSA-N Silver oxide Chemical compound [O-2].[Ag+].[Ag+] NDVLTYZPCACLMA-UHFFFAOYSA-N 0.000 claims 2
- 239000007864 aqueous solution Substances 0.000 claims 2
- 150000001875 compounds Chemical class 0.000 claims 2
- 229910052802 copper Inorganic materials 0.000 claims 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims 2
- 239000010949 copper Substances 0.000 claims 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims 2
- 238000000034 method Methods 0.000 claims 2
- KDLHZDBZIXYQEI-UHFFFAOYSA-N palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 claims 2
- 150000003839 salts Chemical class 0.000 claims 2
- 239000011780 sodium chloride Substances 0.000 claims 2
- 229910052684 Cerium Inorganic materials 0.000 claims 1
- OFJATJUUUCAKMK-UHFFFAOYSA-N Cerium(IV) oxide Chemical compound [O-2]=[Ce+4]=[O-2] OFJATJUUUCAKMK-UHFFFAOYSA-N 0.000 claims 1
- 239000005751 Copper oxide Substances 0.000 claims 1
- 239000005092 Ruthenium Substances 0.000 claims 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N TiO Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims 1
- MCMNRKCIXSYSNV-UHFFFAOYSA-N ZrO2 Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims 1
- 230000015572 biosynthetic process Effects 0.000 claims 1
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 claims 1
- 229910052793 cadmium Inorganic materials 0.000 claims 1
- GWXLDORMOJMVQZ-UHFFFAOYSA-N cerium Chemical compound [Ce] GWXLDORMOJMVQZ-UHFFFAOYSA-N 0.000 claims 1
- 229910000420 cerium oxide Inorganic materials 0.000 claims 1
- QPLDLSVMHZLSFG-UHFFFAOYSA-N copper oxide Chemical compound [Cu]=O QPLDLSVMHZLSFG-UHFFFAOYSA-N 0.000 claims 1
- 229910000431 copper oxide Inorganic materials 0.000 claims 1
- 229910052742 iron Inorganic materials 0.000 claims 1
- 239000002082 metal nanoparticle Substances 0.000 claims 1
- 150000002739 metals Chemical class 0.000 claims 1
- 229910003455 mixed metal oxide Inorganic materials 0.000 claims 1
- 239000011259 mixed solution Substances 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- 229910052763 palladium Inorganic materials 0.000 claims 1
- MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 claims 1
- 229910052703 rhodium Inorganic materials 0.000 claims 1
- 239000010948 rhodium Substances 0.000 claims 1
- KJTLSVCANCCWHF-UHFFFAOYSA-N ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 claims 1
- 229910052707 ruthenium Inorganic materials 0.000 claims 1
- 229910052709 silver Inorganic materials 0.000 claims 1
- BQCADISMDOOEFD-UHFFFAOYSA-N silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims 1
- 239000004332 silver Substances 0.000 claims 1
- 229910001923 silver oxide Inorganic materials 0.000 claims 1
- 238000003786 synthesis reaction Methods 0.000 claims 1
- 230000002194 synthesizing Effects 0.000 claims 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims 1
- 229910052719 titanium Inorganic materials 0.000 claims 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims 1
- 239000010936 titanium Substances 0.000 claims 1
- 229910001929 titanium oxide Inorganic materials 0.000 claims 1
- 229910052723 transition metal Inorganic materials 0.000 claims 1
- 150000003624 transition metals Chemical class 0.000 claims 1
- 235000014692 zinc oxide Nutrition 0.000 claims 1
- RNWHGQJWIACOKP-UHFFFAOYSA-N zinc;oxygen(2-) Chemical class [O-2].[Zn+2] RNWHGQJWIACOKP-UHFFFAOYSA-N 0.000 claims 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims 1
- 229910052726 zirconium Inorganic materials 0.000 claims 1
- 229910001928 zirconium oxide Inorganic materials 0.000 claims 1
- 230000000903 blocking Effects 0.000 abstract 1
- 238000010924 continuous production Methods 0.000 abstract 1
Abstract
A mixing reactor for mixing efficiently streams of fluids of differing densities. In a preferred embodiment, one of the fluids is supercritical water, and the other is an aqueous salt solution. Thus, the reactor enables the production of metal oxide nanoparticles as a continuous process, without any risk of the reactor blocking due to the inefficient mixing inherent in existing reactor designs.
Claims
1. A counter current mixing reactor for continuously mixing two or more fluids of differing densities comprising a first inlet and an outlet characterised in that one or more further inlets are diametrically opposed to the first inlet and are disposed within the outlet, wherein at least one of the fluids is in the sub critical, near critical or supercritical state.
2. A mixing reactor as defined in claim 1 comprising a first inlet and an outlet characterised in that a further inlet is diametrically opposed to the first inlet and is disposed within the outlet.
3. A mixing reactor as defined in claim 1 or claim 2 arranged in a vertical configuration.
4. A mixing reactor as defined in any preceding claim wherein at least one of the fluids is heated, pressurised or supercritical water.
5. A mixing reactor as defined in claim 4 wherein the fluid of lower density is kept hot using a heater around the outlet.
6. A mixing reactor as defined in any of claims 1 to 5 wherein at least one of the fluids is a solution of a metal salt or compound.
7. A mixing reactor as defined in claim 6 wherein at least one of the fluids is an aqueous solution of a metal salt or compound.
8. A mixing reactor as defined in claim 7 wherein the aqueous solution is an aqueous metal salt solution of the metals selected from transition metals including ruthenium, cadmium, rhodium, palladium, iron, cerium, titanium, zirconium, copper and silver.
9. A mixing reactor as defined in any of claims 1 to 8 wherein the fluid of higher density is cooler than the fluid of lower density.
10. A mixing reactor as defined in claim 9 wherein the fluid of higher density is cooled using a heat sink.
11. A mixing reactor as defined in any of claims 1 to 10 wherein the one or more further inlets comprise a shaped nozzle, for example, a conical funnel.
12. A mixing chamber comprising one or more mixing reactors as defined in any of claims 1 to 11 arranged in series .
13. A process for preparing metal or metal oxide nanoparticles which comprises delivery of a metal salt solution through a first inlet of a mixing reactor as defined in any of claims 1 to 11 and delivery of a fluid in the sub critical, near critical or supercritical state through a further inlet diametrically opposed to the first inlet wherein said further inlet is disposed within an outlet such that the mixed solutions exit the reactor once mixed.
14. A process for preparing metal or metal oxide nanoparticles which comprises mixing a solution of supercritical water with an aqueous metal salt solution, characterised in that the aqueous metal salt solution is cooled prior to mixing.
15. Metal or metal oxide nanoparticles obtainable by a process as defined in claim 13 or claim 14. 21
16. A device capable of mixing two fluids of differing densities having a downwardly facing outlet for less dense fluid and inlet for more dense fluid adapted to cause an upwards flow of the more dense fluid in use, the arrangement being such that the less dense fluid is introduceable into the device in a downwards orientation relative to the upwards flow of the denser fluid.
17. A device as specified in claim 16, characterised by the inlet of the less dense fluid having a conical nozzle to aid mixing of the fluids.
18. A device as specified in claim 16 or claim 17 in which the denser of the two solutions is cooled prior to entry into the reactor.
19. Fluid mixing apparatus in which two or more devices specified in any of claims 16 to 18 are used in series.
20. Use of the device of any one of claims 1 to 19 to mix two fluids of differing densities such that the mixing occurs within the device.
21. Use as claimed in claim 20 in which one or both fluids is/are in the near critical or supercritical state.
22. Use as claimed in claim 20 or claim 21, in which one of the fluids is near-critical or supercritical water.
23. Use as claimed in any of claims 20 to 22, in which one of the fluids is an aqueous salt solution.
24. Use as claimed in any of claims 20 to 23, in which the device of claims 16 to 19 is used in the synthesis of metal nanoparticles. 22
25. Use as claimed in claim 24 in which the device of claims 16 to 19 is used to produce nano-particulate cerium oxide.
26. Use as claimed in claim 24 in which the device of claims 16 to 19 is used to produce nano-particulate titanium oxide.
27. Use as claimed in claim 24 in which the device of claims 16 to 19 is used to produce nano-particulate zirconium oxide.
28. Use as claimed in claim 24 in which the device of claims 16 to 19 is used to produce nano-particulate copper oxide.
29. Use as claimed in claim 24 in which the device of claims 16 to 19 is used to produce nano-particulate silver oxide.
30. Use as claimed in claim 24 in which the device of claims 16 to 19 is used to produce mixed metal oxides, specifically mixed copper and zinc oxides .
31. A process for continuously mixing two or more fluids of different densities comprising delivering a first fluid in a first direction of flow and delivering of one or more further fluids in a second direction of flow diametrically opposed to the first direction of flow so that the fluids mix at a mixing region the mixed fluids being carried away from the mixing region by the flow of one of the fluids, and wherein at least one of the fluids is in the subcritical, near critical or supercritical state.
Priority Applications (9)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2006552685A JP5084266B2 (en) | 2004-02-11 | 2005-02-11 | Countercurrent mixing reactor |
EP05708308A EP1713569B1 (en) | 2004-02-11 | 2005-02-11 | Counter current mixing reactor and related process |
US10/589,311 US7566436B2 (en) | 2004-02-11 | 2005-02-11 | Counter current mixing reactor |
DK05708308T DK1713569T3 (en) | 2004-02-11 | 2005-02-11 | Counter current mixing plant and associated process |
AU2005211990A AU2005211990B2 (en) | 2004-02-11 | 2005-02-11 | Counter current mixing reactor |
DE602005014740T DE602005014740D1 (en) | 2004-02-11 | 2005-02-11 | COUNTER-MIXED REACTOR AND RELATED PROCESS |
KR1020067018374A KR101153043B1 (en) | 2004-02-11 | 2005-02-11 | Counter current mixing reactor |
CA2597480A CA2597480C (en) | 2004-02-11 | 2005-02-11 | Counter current mixing reactor |
AT05708308T ATE432761T1 (en) | 2004-02-11 | 2005-02-11 | COUNTERFLOW MIXING REACTOR AND RELATED PROCESS |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GBGB0402963.3A GB0402963D0 (en) | 2004-02-11 | 2004-02-11 | Counter current mixing device for two different fluids |
GB0402963.3 | 2005-02-11 |
Publications (3)
Publication Number | Publication Date |
---|---|
WO2005077505A2 WO2005077505A2 (en) | 2005-08-25 |
WO2005077505A3 WO2005077505A3 (en) | 2005-11-10 |
WO2005077505B1 true WO2005077505B1 (en) | 2006-01-12 |
Family
ID=32011683
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/GB2005/000483 WO2005077505A2 (en) | 2004-02-11 | 2005-02-11 | Counter current mixing reactor |
Country Status (13)
Country | Link |
---|---|
US (1) | US7566436B2 (en) |
EP (1) | EP1713569B1 (en) |
JP (1) | JP5084266B2 (en) |
KR (1) | KR101153043B1 (en) |
CN (2) | CN103831074B (en) |
AT (1) | ATE432761T1 (en) |
AU (1) | AU2005211990B2 (en) |
CA (1) | CA2597480C (en) |
DE (1) | DE602005014740D1 (en) |
DK (1) | DK1713569T3 (en) |
ES (1) | ES2327755T3 (en) |
GB (1) | GB0402963D0 (en) |
WO (1) | WO2005077505A2 (en) |
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2004
- 2004-02-11 GB GBGB0402963.3A patent/GB0402963D0/en not_active Ceased
-
2005
- 2005-02-11 CA CA2597480A patent/CA2597480C/en not_active Expired - Fee Related
- 2005-02-11 CN CN201310588991.5A patent/CN103831074B/en active Active
- 2005-02-11 DK DK05708308T patent/DK1713569T3/en active
- 2005-02-11 CN CNA2005800047670A patent/CN1917936A/en active Pending
- 2005-02-11 US US10/589,311 patent/US7566436B2/en active Active
- 2005-02-11 JP JP2006552685A patent/JP5084266B2/en active Active
- 2005-02-11 AU AU2005211990A patent/AU2005211990B2/en not_active Ceased
- 2005-02-11 WO PCT/GB2005/000483 patent/WO2005077505A2/en active Application Filing
- 2005-02-11 AT AT05708308T patent/ATE432761T1/en not_active IP Right Cessation
- 2005-02-11 KR KR1020067018374A patent/KR101153043B1/en active IP Right Grant
- 2005-02-11 DE DE602005014740T patent/DE602005014740D1/en active Active
- 2005-02-11 ES ES05708308T patent/ES2327755T3/en active Active
- 2005-02-11 EP EP05708308A patent/EP1713569B1/en active Active
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