JP4489388B2 - 微粒銀粉の製造方法 - Google Patents
微粒銀粉の製造方法 Download PDFInfo
- Publication number
- JP4489388B2 JP4489388B2 JP2003281659A JP2003281659A JP4489388B2 JP 4489388 B2 JP4489388 B2 JP 4489388B2 JP 2003281659 A JP2003281659 A JP 2003281659A JP 2003281659 A JP2003281659 A JP 2003281659A JP 4489388 B2 JP4489388 B2 JP 4489388B2
- Authority
- JP
- Japan
- Prior art keywords
- silver powder
- silver
- powder
- fine
- fine silver
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 title claims description 194
- 239000010946 fine silver Substances 0.000 title claims description 98
- 238000004519 manufacturing process Methods 0.000 title claims description 38
- 229910052709 silver Inorganic materials 0.000 claims description 57
- 239000004332 silver Substances 0.000 claims description 57
- SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 claims description 50
- 239000002245 particle Substances 0.000 claims description 48
- 239000003638 chemical reducing agent Substances 0.000 claims description 40
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 claims description 31
- 239000007864 aqueous solution Substances 0.000 claims description 31
- 229910001961 silver nitrate Inorganic materials 0.000 claims description 25
- 239000000243 solution Substances 0.000 claims description 20
- 238000000034 method Methods 0.000 claims description 16
- 238000002156 mixing Methods 0.000 claims description 15
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims description 13
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 13
- 238000001035 drying Methods 0.000 claims description 4
- 239000002270 dispersing agent Substances 0.000 claims description 2
- 239000011259 mixed solution Substances 0.000 claims description 2
- 239000000843 powder Substances 0.000 description 36
- 230000002776 aggregation Effects 0.000 description 21
- 238000004220 aggregation Methods 0.000 description 19
- 238000005245 sintering Methods 0.000 description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 17
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 15
- 230000000052 comparative effect Effects 0.000 description 15
- 239000004020 conductor Substances 0.000 description 14
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 8
- 239000011164 primary particle Substances 0.000 description 8
- 238000006243 chemical reaction Methods 0.000 description 7
- 238000010191 image analysis Methods 0.000 description 7
- 238000001000 micrograph Methods 0.000 description 7
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 6
- 238000009826 distribution Methods 0.000 description 6
- 239000012535 impurity Substances 0.000 description 5
- 238000005259 measurement Methods 0.000 description 5
- 238000001878 scanning electron micrograph Methods 0.000 description 5
- 238000012360 testing method Methods 0.000 description 5
- 239000007788 liquid Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 150000003378 silver Chemical class 0.000 description 4
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 3
- 239000000654 additive Substances 0.000 description 3
- 229960005070 ascorbic acid Drugs 0.000 description 3
- 235000010323 ascorbic acid Nutrition 0.000 description 3
- 239000011668 ascorbic acid Substances 0.000 description 3
- 239000010419 fine particle Substances 0.000 description 3
- 238000000691 measurement method Methods 0.000 description 3
- 229910017604 nitric acid Inorganic materials 0.000 description 3
- 238000011160 research Methods 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 108010010803 Gelatin Proteins 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 238000005054 agglomeration Methods 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 238000013459 approach Methods 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 229920000159 gelatin Polymers 0.000 description 2
- 239000008273 gelatin Substances 0.000 description 2
- 235000019322 gelatine Nutrition 0.000 description 2
- 235000011852 gelatine desserts Nutrition 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000012856 packing Methods 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 239000001856 Ethyl cellulose Substances 0.000 description 1
- ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- WUOACPNHFRMFPN-UHFFFAOYSA-N alpha-terpineol Chemical compound CC1=CCC(C(C)(C)O)CC1 WUOACPNHFRMFPN-UHFFFAOYSA-N 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 235000010980 cellulose Nutrition 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- SQIFACVGCPWBQZ-UHFFFAOYSA-N delta-terpineol Natural products CC(C)(O)C1CCC(=C)CC1 SQIFACVGCPWBQZ-UHFFFAOYSA-N 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000019325 ethyl cellulose Nutrition 0.000 description 1
- 229920001249 ethyl cellulose Polymers 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 125000000687 hydroquinonyl group Chemical group C1(O)=C(C=C(O)C=C1)* 0.000 description 1
- 238000009766 low-temperature sintering Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 239000008188 pellet Substances 0.000 description 1
- 239000011295 pitch Substances 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 229920000036 polyvinylpyrrolidone Polymers 0.000 description 1
- 239000001267 polyvinylpyrrolidone Substances 0.000 description 1
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 238000011946 reduction process Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- NDVLTYZPCACLMA-UHFFFAOYSA-N silver oxide Chemical compound [O-2].[Ag+].[Ag+] NDVLTYZPCACLMA-UHFFFAOYSA-N 0.000 description 1
- 229910001923 silver oxide Inorganic materials 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 229940116411 terpineol Drugs 0.000 description 1
- 230000000930 thermomechanical effect Effects 0.000 description 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
- 238000004065 wastewater treatment Methods 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/16—Making metallic powder or suspensions thereof using chemical processes
- B22F9/18—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
- B22F9/24—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from liquid metal compounds, e.g. solutions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/05—Metallic powder characterised by the size or surface area of the particles
- B22F1/054—Nanosized particles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Nanotechnology (AREA)
- Inorganic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Materials Engineering (AREA)
- Crystallography & Structural Chemistry (AREA)
- Composite Materials (AREA)
- Physics & Mathematics (AREA)
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
- Powder Metallurgy (AREA)
Priority Applications (9)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2003281659A JP4489388B2 (ja) | 2003-07-29 | 2003-07-29 | 微粒銀粉の製造方法 |
TW093118759A TW200504166A (en) | 2003-07-29 | 2004-06-28 | Fine-grain silver powder and process for producing the same (issue 1) |
US10/566,365 US20080138238A1 (en) | 2003-07-29 | 2004-07-15 | Fine Particulate Silver Powder and Production Method Thereof |
PCT/JP2004/010099 WO2005009651A1 (ja) | 2003-07-29 | 2004-07-15 | 微粒銀粉及びその微粒銀粉の製造方法 |
DE112004001399T DE112004001399T5 (de) | 2003-07-29 | 2004-07-15 | Feinpartikuläres Silberpulver und Verfahren zu dessen Herstellung |
CA002534107A CA2534107A1 (en) | 2003-07-29 | 2004-07-15 | Fine-grain silver powder and process for producing the same |
CNB2004800209878A CN100455382C (zh) | 2003-07-29 | 2004-07-15 | 微粒银粉及其微粒银粉的制造方法 |
KR1020067001513A KR101132282B1 (ko) | 2003-07-29 | 2004-07-15 | 미립 은분의 제조 방법 |
HK06112769.8A HK1092101A1 (en) | 2003-07-29 | 2006-11-21 | Fine-grain silver powder and process for producing the same |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2003281659A JP4489388B2 (ja) | 2003-07-29 | 2003-07-29 | 微粒銀粉の製造方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2005048236A JP2005048236A (ja) | 2005-02-24 |
JP4489388B2 true JP4489388B2 (ja) | 2010-06-23 |
Family
ID=34100959
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2003281659A Expired - Lifetime JP4489388B2 (ja) | 2003-07-29 | 2003-07-29 | 微粒銀粉の製造方法 |
Country Status (9)
Country | Link |
---|---|
US (1) | US20080138238A1 (de) |
JP (1) | JP4489388B2 (de) |
KR (1) | KR101132282B1 (de) |
CN (1) | CN100455382C (de) |
CA (1) | CA2534107A1 (de) |
DE (1) | DE112004001399T5 (de) |
HK (1) | HK1092101A1 (de) |
TW (1) | TW200504166A (de) |
WO (1) | WO2005009651A1 (de) |
Families Citing this family (30)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2006126614A1 (ja) * | 2005-05-25 | 2006-11-30 | Nihon Handa Co., Ltd. | ペースト状銀組成物、その製造方法、固形状銀の製造方法、固形状銀、接着方法および回路板の製造方法 |
KR101136766B1 (ko) | 2006-07-28 | 2012-04-20 | 미쓰비시 마테리알 가부시키가이샤 | 은 미립자와 그 제조 방법 및 제조 장치 |
TWI468240B (zh) * | 2007-03-30 | 2015-01-11 | Mitsubishi Materials Corp | 銀微粒子、銀微粒子之製造方法、及銀微粒子之製造裝置 |
US8968608B2 (en) | 2008-01-17 | 2015-03-03 | Nichia Corporation | Method for producing conductive material, conductive material obtained by the method, electronic device containing the conductive material, light-emitting device, and method for producing light-emitting device |
JP5355007B2 (ja) * | 2008-09-17 | 2013-11-27 | Dowaエレクトロニクス株式会社 | 球状銀粉の製造方法 |
US8836130B2 (en) | 2009-01-23 | 2014-09-16 | Nichia Corporation | Light emitting semiconductor element bonded to a base by a silver coating |
JP5370372B2 (ja) | 2009-01-23 | 2013-12-18 | 日亜化学工業株式会社 | 半導体装置及びその製造方法 |
CN102292835B (zh) | 2009-01-23 | 2015-03-25 | 日亚化学工业株式会社 | 半导体装置及其制造方法 |
US8231704B2 (en) * | 2009-05-01 | 2012-07-31 | E I Du Pont De Nemours And Company | Silver particles and processes for making them |
US8372178B2 (en) * | 2009-05-01 | 2013-02-12 | E I Du Pont De Nemours And Company | Silver particles and processes for making them |
EP2407980B1 (de) | 2009-07-21 | 2019-01-23 | Nichia Corporation | Verfahren zur herstellung eines leitfähigen materials, in diesem verfahren gewonnenes leitfähiges material, elektronikgerät mit dem leitfähigen material und lichtemittierende vorrichtung damit |
TW201108249A (en) * | 2009-08-25 | 2011-03-01 | Du Pont | Silver thick film paste compositions and their use in conductors for photovoltaic cells |
JP2011080094A (ja) * | 2009-10-02 | 2011-04-21 | Toda Kogyo Corp | 銀微粒子及びその製造方法、並びに該銀微粒子を含有する導電性ペースト、導電性膜及び電子デバイス |
JP5659495B2 (ja) * | 2010-01-26 | 2015-01-28 | 三菱マテリアル株式会社 | 電極又は配線パターンの形成方法 |
US8366799B2 (en) | 2010-08-30 | 2013-02-05 | E I Du Pont De Nemours And Company | Silver particles and a process for making them |
US9186727B2 (en) * | 2010-11-08 | 2015-11-17 | Namics Corporation | Metal particle |
US8574338B2 (en) | 2010-11-17 | 2013-11-05 | E I Du Pont De Nemours And Company | Reactor and continuous process for producing silver powders |
CN102133635B (zh) * | 2011-05-02 | 2012-09-19 | 杨荣春 | 银粉及其制造方法 |
KR20140047663A (ko) * | 2011-07-29 | 2014-04-22 | 도다 고교 가부시끼가이샤 | 은미립자 및 이 은미립자를 함유하는 도전성 페이스트, 도전성 막 및 전자 디바이스 |
JP5354041B2 (ja) * | 2012-02-24 | 2013-11-27 | 住友金属鉱山株式会社 | 銀粉の製造方法 |
WO2013133085A1 (ja) * | 2012-03-05 | 2013-09-12 | ナミックス株式会社 | 銀微粒子焼結体 |
JP5510531B1 (ja) * | 2012-11-29 | 2014-06-04 | 住友金属鉱山株式会社 | 銀粉及び銀ペースト |
TWI508799B (zh) * | 2012-12-06 | 2015-11-21 | China Steel Corp | A Method for Synthesis of Silver Powder with Adjustable Particle Size |
JP6115405B2 (ja) * | 2013-08-28 | 2017-04-19 | 住友金属鉱山株式会社 | 銀粉の製造方法 |
JP6086145B2 (ja) * | 2015-12-22 | 2017-03-01 | 住友金属鉱山株式会社 | 銀粉の製造方法 |
KR102033545B1 (ko) * | 2017-06-05 | 2019-10-17 | 대주전자재료 주식회사 | 은 입자 및 이의 제조방법 |
CN107520460A (zh) * | 2017-07-26 | 2017-12-29 | 华南理工大学 | 一种超细纳米金/纳米纤维素复合溶液及其制备方法 |
EP4066968A4 (de) | 2019-11-28 | 2023-08-02 | M. Technique Co., Ltd. | Verfahren zur herstellung von feinen silberpartikeln |
CN114682792B (zh) * | 2022-04-14 | 2024-02-13 | 宁夏中色新材料有限公司 | 一种高比表面球形银粉及其制备方法 |
JP2023164097A (ja) * | 2022-04-28 | 2023-11-10 | Dowaエレクトロニクス株式会社 | 球状銀粉、球状銀粉の製造方法、球状銀粉製造装置、及び導電性ペースト |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2001107101A (ja) * | 1999-10-12 | 2001-04-17 | Mitsui Mining & Smelting Co Ltd | 高分散性球状銀粉末及びその製造方法 |
JP2003034802A (ja) * | 2001-07-25 | 2003-02-07 | Mitsui Mining & Smelting Co Ltd | 銅粉、その銅粉の製造方法、その銅粉を用いた銅ペースト、及びその銅ペーストを用いたプリント配線板 |
JP2003129106A (ja) * | 2001-10-25 | 2003-05-08 | Murata Mfg Co Ltd | ニッケル粉末の製造方法、ニッケル粉末、ニッケルペースト、積層セラミック電子部品 |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH01287210A (ja) * | 1988-05-12 | 1989-11-17 | Tanaka Kikinzoku Kogyo Kk | 銀微粒子の製造方法 |
US4979985A (en) * | 1990-02-06 | 1990-12-25 | E. I. Du Pont De Nemours And Company | Process for making finely divided particles of silver metal |
JPH04333504A (ja) * | 1991-05-10 | 1992-11-20 | Sumitomo Metal Mining Co Ltd | 単分散銀微粉の連続製造方法 |
CN1174827C (zh) * | 2001-08-17 | 2004-11-10 | 中国科学院过程工程研究所 | 化学还原法制备六方片状银粉 |
JP4109520B2 (ja) * | 2002-09-12 | 2008-07-02 | 三井金属鉱業株式会社 | 低凝集性銀粉並びにその低凝集性銀粉の製造方法及びその低凝集性銀粉を用いた導電性ペースト |
-
2003
- 2003-07-29 JP JP2003281659A patent/JP4489388B2/ja not_active Expired - Lifetime
-
2004
- 2004-06-28 TW TW093118759A patent/TW200504166A/zh not_active IP Right Cessation
- 2004-07-15 CN CNB2004800209878A patent/CN100455382C/zh not_active Expired - Fee Related
- 2004-07-15 US US10/566,365 patent/US20080138238A1/en not_active Abandoned
- 2004-07-15 DE DE112004001399T patent/DE112004001399T5/de not_active Withdrawn
- 2004-07-15 WO PCT/JP2004/010099 patent/WO2005009651A1/ja active Application Filing
- 2004-07-15 CA CA002534107A patent/CA2534107A1/en not_active Abandoned
- 2004-07-15 KR KR1020067001513A patent/KR101132282B1/ko not_active IP Right Cessation
-
2006
- 2006-11-21 HK HK06112769.8A patent/HK1092101A1/xx not_active IP Right Cessation
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2001107101A (ja) * | 1999-10-12 | 2001-04-17 | Mitsui Mining & Smelting Co Ltd | 高分散性球状銀粉末及びその製造方法 |
JP2003034802A (ja) * | 2001-07-25 | 2003-02-07 | Mitsui Mining & Smelting Co Ltd | 銅粉、その銅粉の製造方法、その銅粉を用いた銅ペースト、及びその銅ペーストを用いたプリント配線板 |
JP2003129106A (ja) * | 2001-10-25 | 2003-05-08 | Murata Mfg Co Ltd | ニッケル粉末の製造方法、ニッケル粉末、ニッケルペースト、積層セラミック電子部品 |
Also Published As
Publication number | Publication date |
---|---|
KR101132282B1 (ko) | 2012-04-02 |
HK1092101A1 (en) | 2007-02-02 |
CN100455382C (zh) | 2009-01-28 |
JP2005048236A (ja) | 2005-02-24 |
CA2534107A1 (en) | 2005-02-03 |
TW200504166A (en) | 2005-02-01 |
KR20060035781A (ko) | 2006-04-26 |
WO2005009651A1 (ja) | 2005-02-03 |
DE112004001399T5 (de) | 2006-06-22 |
US20080138238A1 (en) | 2008-06-12 |
CN1826197A (zh) | 2006-08-30 |
TWI304832B (de) | 2009-01-01 |
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