JP2024001023A5 - - Google Patents

Download PDF

Info

Publication number
JP2024001023A5
JP2024001023A5 JP2023148298A JP2023148298A JP2024001023A5 JP 2024001023 A5 JP2024001023 A5 JP 2024001023A5 JP 2023148298 A JP2023148298 A JP 2023148298A JP 2023148298 A JP2023148298 A JP 2023148298A JP 2024001023 A5 JP2024001023 A5 JP 2024001023A5
Authority
JP
Japan
Prior art keywords
glufosinate
crystal
peaks selected
xrpd
xrpd pattern
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP2023148298A
Other languages
English (en)
Japanese (ja)
Other versions
JP2024001023A (ja
Filing date
Publication date
Priority claimed from PCT/US2018/042503 external-priority patent/WO2019018406A1/en
Application filed filed Critical
Publication of JP2024001023A publication Critical patent/JP2024001023A/ja
Publication of JP2024001023A5 publication Critical patent/JP2024001023A5/ja
Pending legal-status Critical Current

Links

JP2023148298A 2017-07-18 2023-09-13 L-グルホシネートの精製方法 Pending JP2024001023A (ja)

Applications Claiming Priority (6)

Application Number Priority Date Filing Date Title
US201762533944P 2017-07-18 2017-07-18
US62/533,944 2017-07-18
US201862653736P 2018-04-06 2018-04-06
US62/653,736 2018-04-06
PCT/US2018/042503 WO2019018406A1 (en) 2017-07-18 2018-07-17 METHODS OF PURIFYING L-GLUFOSINATE
JP2020502197A JP2020527567A (ja) 2017-07-18 2018-07-17 L−グルホシネートの精製方法

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
JP2020502197A Division JP2020527567A (ja) 2017-07-18 2018-07-17 L−グルホシネートの精製方法

Publications (2)

Publication Number Publication Date
JP2024001023A JP2024001023A (ja) 2024-01-09
JP2024001023A5 true JP2024001023A5 (enExample) 2025-06-17

Family

ID=63104080

Family Applications (2)

Application Number Title Priority Date Filing Date
JP2020502197A Withdrawn JP2020527567A (ja) 2017-07-18 2018-07-17 L−グルホシネートの精製方法
JP2023148298A Pending JP2024001023A (ja) 2017-07-18 2023-09-13 L-グルホシネートの精製方法

Family Applications Before (1)

Application Number Title Priority Date Filing Date
JP2020502197A Withdrawn JP2020527567A (ja) 2017-07-18 2018-07-17 L−グルホシネートの精製方法

Country Status (13)

Country Link
US (6) US11634442B2 (enExample)
EP (1) EP3654771A1 (enExample)
JP (2) JP2020527567A (enExample)
KR (2) KR20240150519A (enExample)
CN (1) CN111065270A (enExample)
AU (2) AU2018304177B2 (enExample)
BR (1) BR112020001172A2 (enExample)
CA (3) CA3070104C (enExample)
CL (1) CL2020000133A1 (enExample)
IL (1) IL271990B2 (enExample)
MX (3) MX2023008215A (enExample)
WO (1) WO2019018406A1 (enExample)
ZA (1) ZA202000437B (enExample)

Families Citing this family (38)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2019018406A1 (en) * 2017-07-18 2019-01-24 Agrimetis, Llc METHODS OF PURIFYING L-GLUFOSINATE
EP3870960B1 (en) * 2018-10-24 2026-04-15 FUJIFILM Electronic Materials U.S.A, Inc. Chemical liquid manufacturing apparatus and method of manufacturing chemical liquid
CN113767107A (zh) * 2019-04-16 2021-12-07 巴斯夫欧洲公司 生产结晶l-草铵膦铵盐一水合物的方法
CN110749612A (zh) * 2019-11-27 2020-02-04 湖北富邦科技股份有限公司 一种新型测量肥料中钾含量的方法
CN111363775B (zh) 2020-03-18 2022-08-05 浙江工业大学 一种生物酶法去消旋化制备l-草铵膦的方法、草铵膦脱氢酶突变体及应用
CN111574559A (zh) * 2020-04-30 2020-08-25 河北威远生物化工有限公司 L-草铵膦酶水解液的后处理方法
US11555046B2 (en) 2020-07-31 2023-01-17 Upl Ltd Crystalline form of L-glufosinate ammonium salt and process for production thereof
UY39360A (es) * 2020-07-31 2022-01-31 Upl Ltd Forma cristalina de la sal de l-glufosinato de amonio y proceso para su producción
CN112321635A (zh) * 2020-11-23 2021-02-05 北京鑫佰利科技发展有限公司 一种草铵膦清洁生产工艺和方法
CN112760353A (zh) * 2021-03-16 2021-05-07 北京鑫佰利科技发展有限公司 一种l-草铵膦的生产方法
CN115109085A (zh) * 2021-03-23 2022-09-27 利尔化学股份有限公司 L-草铵膦铵盐的固体形式及其制备方法和用途
EP4312558A1 (en) * 2021-04-01 2024-02-07 Evonik Operations GmbH Enzymatic method for producing l-glufosinate and its phosphoesters
CN113234767B (zh) * 2021-05-13 2022-05-17 永农生物科学有限公司 制备不含结晶水的l-草铵膦铵盐的固体粉末的方法
EP4105335A1 (en) 2021-06-16 2022-12-21 Evonik Operations GmbH Enzymatic method for the production of l-glufosinate p-alkyl esters
CN113480573B (zh) * 2021-06-21 2023-08-15 上海七洲紫岳生物科技有限公司 L-草铵膦的晶型及其制备方法和应用
EP4151643A1 (en) 2021-09-16 2023-03-22 Evonik Operations GmbH Improved process for production of phosphoesters of glufosinate precursors
WO2023174511A1 (en) 2022-03-14 2023-09-21 Evonik Operations Gmbh Enzymatic method for the production of l-glufosinate p-esters
CN114773384B (zh) * 2022-03-25 2024-04-16 内蒙古灵圣作物科技有限公司 一种草铵膦结晶母液的处理方法
CN114605470B (zh) * 2022-04-06 2023-08-04 中国林业科学研究院林产化学工业研究所 一种草铵膦原液精制脱色的方法
WO2023222226A1 (en) 2022-05-19 2023-11-23 Evonik Operations Gmbh Enzymatic method for producing l-glufosinate
WO2023222227A1 (en) 2022-05-19 2023-11-23 Evonik Operations Gmbh Enzymatic method for producing l-glufosinate
WO2023232225A1 (en) 2022-05-31 2023-12-07 Evonik Operations Gmbh Enzymatic method for the diastereoselective production of l-glufosinate p-esters
CN119325479A (zh) * 2022-06-10 2025-01-17 江苏七洲绿色科技研究院有限公司 L-草铵膦铵盐的结晶及其制备方法和应用
CN115368409B (zh) * 2022-08-31 2024-10-18 湖北泰盛化工有限公司 一种草甘膦低质料的回收利用方法
JP2025531377A (ja) 2022-09-21 2025-09-19 エボニック オペレーションズ ゲーエムベーハー L-グルホシネート及びそのホスホエステルを製造するための酵素法
WO2024061456A1 (en) 2022-09-21 2024-03-28 Evonik Operations Gmbh Enzymatic method for producing l-glufosinate and its phosphoesters
WO2025114125A1 (en) 2023-12-01 2025-06-05 Basf Se Herbicidal compositions comprising glufosinate
WO2025124944A1 (en) 2023-12-12 2025-06-19 Basf Se Herbicidal compositions comprising 2,4-d
WO2025172125A1 (en) 2024-02-16 2025-08-21 Basf Se Herbicidal compositions comprising pyroxasulfone
WO2025172127A1 (en) 2024-02-16 2025-08-21 Basf Se Herbicidal compositions comprising imazethapyr
WO2025176575A1 (en) 2024-02-23 2025-08-28 Basf Se Herbicidal compositions comprising dimethenamid
WO2025180968A1 (en) 2024-02-27 2025-09-04 Basf Se Herbicidal compositions comprising mesotrione
WO2025209887A1 (en) 2024-04-05 2025-10-09 Basf Se Herbicidal compositions comprising topramezone
WO2025228721A1 (en) 2024-04-30 2025-11-06 Basf Se Herbicidal compositions comprising isoxaflutole
WO2025237738A1 (en) 2024-05-16 2025-11-20 Basf Se Herbicidal compositions comprising clethodim
WO2025237737A1 (en) 2024-05-16 2025-11-20 Basf Se Herbicidal compositions comprising acetochlor
WO2025237741A1 (en) 2024-05-16 2025-11-20 Basf Se Herbicidal compositions comprising diclosulam
EP4696139A1 (en) 2024-08-12 2026-02-18 Basf Se Herbicidal compositions comprising herbicide b

Family Cites Families (74)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR7199E (fr) 1907-06-01 Societe Muller Et Roger Et Cie Dispositif de robinet bivalve
US2500149A (en) 1947-02-21 1950-03-14 Dow Chemical Co Sulfonation of copolymers of monovinyl-and polyvinyl-aromatic compounds
US2527300A (en) 1948-03-18 1950-10-24 American Cyanamid Co Copolymers of unsaturated sulfonic acids and polyunsaturated compounds
US2597439A (en) 1951-05-12 1952-05-20 Rohm & Haas Weakly basic anion-exchange polymers
US2985589A (en) 1957-05-22 1961-05-23 Universal Oil Prod Co Continuous sorption process employing fixed bed of sorbent and moving inlets and outlets
US4224415A (en) 1958-07-18 1980-09-23 Rohm And Haas Company Polymerization processes and products therefrom
DE123476C (enExample) 1960-09-19
US3086916A (en) 1961-08-02 1963-04-23 Kyowa Hakko Kogyo Kk Process for producing l-glutamic acid from racemic glutamic acid
US3360554A (en) 1963-12-18 1967-12-26 Asahi Chemical Ind Process for crystallizing out l-glutamic acid
US3401798A (en) 1965-01-04 1968-09-17 Dorr Oliver Inc Cylindrically stacked and spirally configured semi-permeable membrane laminate apparatus
US3458439A (en) 1965-02-08 1969-07-29 Nalco Chemical Co Ion exchange process and regeneration of anion exchange resins
NL6702806A (enExample) 1966-03-31 1967-10-02
US3458976A (en) 1967-10-30 1969-08-05 Dow Chemical Co Article of manufacture for making chromatographic separations
US3556305A (en) 1968-03-28 1971-01-19 Amicon Corp Composite membrane and process for making same
US3556992A (en) 1969-07-22 1971-01-19 Amicon Corp Anisotropic ultrafiltration membrane having adhering coating and methods of forming and using this membrane
US3628669A (en) 1969-12-22 1971-12-21 Owens Corning Fiberglass Corp Semipermeable membranes
US3857824A (en) 1972-07-05 1974-12-31 Dow Chemical Co Process for the preparation of bead polymers useful in gel permeation chromatography
JPS5215398B2 (enExample) 1973-11-09 1977-04-28
US4001113A (en) 1975-01-28 1977-01-04 The Amalgamated Sugar Company Ion exchange method
FI69248C (fi) 1976-12-21 1986-01-10 Mitsubishi Chem Ind Foerfarande foer reglering av operationsprocessen av en simulerad roerlig baedd
US4062817A (en) 1977-04-04 1977-12-13 The B.F. Goodrich Company Water absorbent polymers comprising unsaturated carboxylic acid, acrylic ester containing alkyl group 10-30 carbon atoms, and another acrylic ester containing alkyl group 2-8 carbon atoms
DE2839087A1 (de) 1978-09-08 1980-03-20 Hoechst Ag Herbizide mittel
US4314032A (en) 1978-10-26 1982-02-02 Kureha Kagaku Kogyo Kabushiki Kaisha Crosslinked polyvinyl alcohol gel
US4319929A (en) 1979-11-19 1982-03-16 Uop Inc. Simulated countercurrent sorption process employing ion exchange resins with periodic backflushing
US4412866A (en) 1981-05-26 1983-11-01 The Amalgamated Sugar Company Method and apparatus for the sorption and separation of dissolved constituents
JPS59219297A (ja) 1983-05-27 1984-12-10 Meiji Seika Kaisha Ltd 光学活性な〔(3−アミノ−3−カルボキシ)プロピル−1〕−ホスフイン酸誘導体の製造法
US4614751A (en) 1984-04-05 1986-09-30 The Dow Chemical Company Process for preparing improved weak acid resins and porous weak acid resins
AU599985B2 (en) 1986-06-09 1990-08-02 Meiji Seika Kaisha Ltd. New process for the production of L-2-amino-4- (hydroxymethyl-phosphinyl)-butyric acid
US4950332A (en) 1988-03-17 1990-08-21 The Dow Chemical Company Process for decolorizing aqueous sugar solutions via adsorbent resins, and desorption of color bodies from the adsorbent resins
US5102553A (en) 1988-12-16 1992-04-07 The Amalgamated Sugar Company Time variable simulated moving bed process
DE3920570A1 (de) 1989-06-23 1991-01-03 Hoechst Ag Verfahren zur isolierung von l-2-amino-4-methylphosphinobuttersaeure-ammoniumsalz aus einer enzymatischen transaminierungsloesung
US5447635A (en) 1991-02-26 1995-09-05 Bracco International B.V. Process of concentration and purification of organic compounds
IL101539A (en) * 1991-04-16 1998-09-24 Monsanto Europe Sa Non-hygroscopic mono-ammonium salts of n-phosphonomethyl glycine derivatives their preparation and pesticidal compositons containing them
CA2067060C (en) 1991-04-27 2002-11-26 Jean Kocur Liquid herbicidal compositions
JP3294647B2 (ja) 1991-12-13 2002-06-24 ヘキスト・アクチェンゲゼルシャフト L−ホスフィノトリシンおよびその誘導体の製造方法
US5244926A (en) 1992-06-16 1993-09-14 The Dow Chemical Company Preparation of ion exchange and adsorbent copolymers
DE4407197A1 (de) * 1994-03-04 1995-09-07 Hoechst Schering Agrevo Gmbh Verfahren zur Herstellung von /L/-Homoalanin-4-yl-(methyl)phosphinsäure und deren Salze durch Racematspaltung
US5811581A (en) 1994-08-04 1998-09-22 Dibra S.P.A. Process for the purification of opacifying contrast agents
JP2698056B2 (ja) 1995-06-22 1998-01-19 イチビキ株式会社 L−グルタミン酸・l−ピログルタミン酸相互変換酵素
US5737309A (en) * 1995-11-09 1998-04-07 Conklin Instrument Corporation Method and apparatus for interface communications in a tandem cross connect
DE19736125A1 (de) * 1997-08-20 1999-02-25 Hoechst Schering Agrevo Gmbh Verfahren zur Herstellung von Glufosinate und phosphorhaltige alpha-Aminonitrile als Zwischenprodukte
US6431202B1 (en) 1999-12-01 2002-08-13 Calgon Carbon Corporation Fluid-directing multiport rotary valve
JP4292724B2 (ja) * 2001-02-20 2009-07-08 味の素株式会社 有機態窒素含有組成物及びそれを含む肥料
FI20010977L (fi) 2001-05-09 2002-11-10 Danisco Sweeteners Oy Kromatografinen erotusmenetelmä
JP2003034680A (ja) 2001-07-19 2003-02-07 Ajinomoto Co Inc ピロリドンカルボン酸又はその塩の製造法
US8076373B2 (en) 2001-09-11 2011-12-13 North Cell Pharmacetical Method for treating mammalian diseases and injuries caused by the over-expression of peroxynitrite
DE10214844A1 (de) 2002-04-04 2003-10-16 Bayer Ag Verfahren zur Herstellung von grobkörnigen gelförmigen Anionenaustauschern
PT1649068E (pt) 2003-07-16 2013-01-10 Amalgamated Res Inc Um método para purificação de material de sacarose de elevada pureza
US7772426B2 (en) 2005-03-29 2010-08-10 Meiji Seika Kaisha, Ltd. Method for producing L-2-amino-4-(hydroxymethylphosphinyl)-butanoic acid
NZ576524A (en) * 2006-11-10 2012-01-12 Basf Se Crystalline modification of fipronil
EP2201018B1 (en) * 2007-09-19 2016-03-16 Ambit Biosciences Corporation Solid forms comprising n-(5-tert-butyl-isoxazol-3-yl)-n'-{4-ý7-(2-morpholin-4-yl-ethoxy)imidazoý2,1-b¨ý1,3¨benzothiazol-2-yl¨phenyl}urea, compositions thereof, and uses therewith
WO2010013242A1 (en) 2008-07-29 2010-02-04 Alcobra Ltd. Substituted pyridoxine-lactam carboxylate salts
JP5909185B2 (ja) * 2009-10-01 2016-04-26 シマベイ セラピューティクス, インコーポレーテッド 置換テトラゾール−1−イルフェノキシメチルチアゾール−2−イルピペリジニルピリミジン塩
WO2011105349A1 (ja) * 2010-02-23 2011-09-01 日本化薬株式会社 2-エチル-3,7-ジメチル-6-(4-(トリフルオロメトキシ)フェノキシ)キノリン-4-イルメチルカーボネートの安定型結晶およびその製造方法並びにその結晶を含有する農薬組成物
CN101863819A (zh) 2010-06-30 2010-10-20 宜兴市前成生物有限公司 一种制备l-焦谷氨酸镁的方法
PH12014500673A1 (en) * 2011-09-30 2014-05-05 Meiji Seika Pharma Co Ltd Method for producing glufosinate p free acid
GB201202393D0 (en) * 2012-02-09 2012-03-28 Syngenta Ltd Polymorphs
BR112014028872A2 (pt) 2012-05-25 2017-06-27 Basf Se forma b cristalina, processo para a produção das formas b e ab, mistura da forma b cristalina, agente de proteção, uso da forma b cristalina e método para o combate do crescimento indesejado dos vegetais
CN103351323A (zh) 2013-06-07 2013-10-16 浙江天瑞化学有限公司 一种焦谷氨酸的制备方法
CN103342718B (zh) * 2013-07-22 2016-02-03 重庆紫光化工股份有限公司 一种3-(甲基烷氧基磷酰基)丙酸酯类化合物的制备方法
CN104059102B (zh) * 2014-06-12 2017-04-12 浙江工业大学 有机碱脱酸法制备高纯草铵膦的方法
SG11201701520TA (en) * 2014-09-16 2017-04-27 Gilead Sciences Inc Solid forms of a toll-like receptor modulator
CN114766484A (zh) * 2015-01-19 2022-07-22 Upl 有限公司 敌稗的结晶变型
CN105131032A (zh) * 2015-07-28 2015-12-09 西安近代化学研究所 一种合成l-草铵膦的方法
CN108367212A (zh) 2015-12-01 2018-08-03 陶氏环球技术有限责任公司 使用聚合物大孔吸附剂色谱分离有机酸
CN105669742B (zh) * 2016-01-14 2018-06-08 江苏七洲绿色化工股份有限公司 一种草铵膦的纯化方法
CN105732706A (zh) * 2016-01-29 2016-07-06 浙江大学 有机碱法制备高纯草铵膦的方法
IL261271B2 (en) 2016-03-02 2025-03-01 Agrimetis Llc Methods for preparing L-glucosinate
CN106188134B (zh) * 2016-07-01 2018-03-20 永农生物科学有限公司 一种l‑草铵膦或其盐的分离及精制方法
CN106083922B (zh) 2016-08-23 2018-08-31 山东省农药科学研究院 一种精草铵膦的制备方法
WO2018108797A1 (de) * 2016-12-15 2018-06-21 Bayer Cropscience Aktiengesellschaft Verfahren zur herstellung von l-glufosinat oder dessen salzen unter verwendung von ephedrin
CN106916857B (zh) 2017-03-09 2019-08-27 浙江大学 一种生产l-草铵膦的方法
WO2019018406A1 (en) * 2017-07-18 2019-01-24 Agrimetis, Llc METHODS OF PURIFYING L-GLUFOSINATE
CN113767107A (zh) 2019-04-16 2021-12-07 巴斯夫欧洲公司 生产结晶l-草铵膦铵盐一水合物的方法

Similar Documents

Publication Publication Date Title
JP2024001023A5 (enExample)
JP2023002516A5 (enExample)
CN103601211B (zh) 一种合成分子筛ssz-13的方法
JP2023036708A5 (enExample)
JP2023082086A5 (enExample)
JP2018024682A5 (enExample)
JP2021530565A5 (enExample)
JP2009502795A5 (enExample)
JP2024103495A5 (enExample)
JP2003012373A5 (enExample)
JP2003516394A5 (enExample)
HRP20170634T4 (hr) Kristalni oblik od 4-metil-n-[3-(4-metil-imidazol-1-il)-5-trifluorometil-fenil]-3-(4-piridin-3-il-pirimidin-2-ilamino)-benzamida
BRPI0519913A2 (pt) métodos de produzir titánio metálico, de fabricar pó de titánio metálico, de preparar um artefato de titãnio e de recuperar titánio, e, pó de titánio
JP2009521414A5 (enExample)
GEP20105086B (en) Potassium salt of an hiv integrase inhibitor
JP2007532560A5 (enExample)
JP2006137778A5 (enExample)
JP2013527246A5 (enExample)
JP2022511800A5 (enExample)
JP2013503134A5 (enExample)
JP2019504103A5 (enExample)
JP2022551316A5 (enExample)
HRP20230813T1 (hr) Upadacitinib solni spoj i postupak njegove pripreme
JP2021517111A5 (enExample)
JP2022088524A5 (enExample)