JP2018535181A5 - - Google Patents
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- JP2018535181A5 JP2018535181A5 JP2018524477A JP2018524477A JP2018535181A5 JP 2018535181 A5 JP2018535181 A5 JP 2018535181A5 JP 2018524477 A JP2018524477 A JP 2018524477A JP 2018524477 A JP2018524477 A JP 2018524477A JP 2018535181 A5 JP2018535181 A5 JP 2018535181A5
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- Japan
- Prior art keywords
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- 150000001875 compounds Chemical class 0.000 claims 25
- 238000000034 method Methods 0.000 claims 13
- 239000000203 mixture Substances 0.000 claims 6
- 125000000217 alkyl group Chemical group 0.000 claims 5
- 238000004519 manufacturing process Methods 0.000 claims 5
- 239000011541 reaction mixture Substances 0.000 claims 4
- 229910052799 carbon Inorganic materials 0.000 claims 3
- 238000000605 extraction Methods 0.000 claims 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 3
- 125000002373 5 membered heterocyclic group Chemical group 0.000 claims 2
- 125000004070 6 membered heterocyclic group Chemical group 0.000 claims 2
- 125000003341 7 membered heterocyclic group Chemical group 0.000 claims 2
- 125000005330 8 membered heterocyclic group Chemical group 0.000 claims 2
- 229910052739 hydrogen Inorganic materials 0.000 claims 2
- 229910052757 nitrogen Inorganic materials 0.000 claims 2
- 239000003960 organic solvent Substances 0.000 claims 2
- 125000006704 (C5-C6) cycloalkyl group Chemical group 0.000 claims 1
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 claims 1
- 101001137337 Homo sapiens Transcriptional activator protein Pur-alpha Proteins 0.000 claims 1
- 102100035715 Transcriptional activator protein Pur-alpha Human genes 0.000 claims 1
- 229910052783 alkali metal Inorganic materials 0.000 claims 1
- 150000001340 alkali metals Chemical class 0.000 claims 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims 1
- 150000001342 alkaline earth metals Chemical class 0.000 claims 1
- 125000003545 alkoxy group Chemical group 0.000 claims 1
- 229910052782 aluminium Inorganic materials 0.000 claims 1
- 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 claims 1
- 238000004821 distillation Methods 0.000 claims 1
- 238000001704 evaporation Methods 0.000 claims 1
- 230000008020 evaporation Effects 0.000 claims 1
- 229910052736 halogen Inorganic materials 0.000 claims 1
- 150000002367 halogens Chemical class 0.000 claims 1
- 125000005842 heteroatom Chemical group 0.000 claims 1
- 229910052744 lithium Inorganic materials 0.000 claims 1
- 229910052749 magnesium Inorganic materials 0.000 claims 1
- 239000012528 membrane Substances 0.000 claims 1
- 229910052760 oxygen Inorganic materials 0.000 claims 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims 1
- 229910052700 potassium Inorganic materials 0.000 claims 1
- 238000000926 separation method Methods 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- 229910052717 sulfur Inorganic materials 0.000 claims 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims 1
- 229920002554 vinyl polymer Polymers 0.000 claims 1
- 0 *S(NC=C=O)(=C)=O Chemical compound *S(NC=C=O)(=C)=O 0.000 description 2
Applications Claiming Priority (63)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201562254860P | 2015-11-13 | 2015-11-13 | |
| US62/254,860 | 2015-11-13 | ||
| EP15194513 | 2015-11-13 | ||
| EP15194513.6 | 2015-11-13 | ||
| EP15195231 | 2015-11-18 | ||
| EP15195231.4 | 2015-11-18 | ||
| US201662290523P | 2016-02-03 | 2016-02-03 | |
| US62/290,523 | 2016-02-03 | ||
| EP16153983.8 | 2016-02-03 | ||
| EP16153983 | 2016-02-03 | ||
| US201662308313P | 2016-03-15 | 2016-03-15 | |
| US62/308,313 | 2016-03-15 | ||
| EP16160245 | 2016-03-15 | ||
| EP16160248.7 | 2016-03-15 | ||
| EP16160248 | 2016-03-15 | ||
| EP16160245.3 | 2016-03-15 | ||
| EP16163045 | 2016-03-30 | ||
| EP16163043.9 | 2016-03-30 | ||
| EP16163045.4 | 2016-03-30 | ||
| EP16163043 | 2016-03-30 | ||
| EP16163835.8 | 2016-04-05 | ||
| EP16163835 | 2016-04-05 | ||
| EP16164023 | 2016-04-06 | ||
| EP16164023.0 | 2016-04-06 | ||
| EP16164146.9 | 2016-04-07 | ||
| EP16164146 | 2016-04-07 | ||
| EP16164148.5 | 2016-04-07 | ||
| EP16164148 | 2016-04-07 | ||
| EP16164371.3 | 2016-04-08 | ||
| EP16164373.9 | 2016-04-08 | ||
| EP16164371 | 2016-04-08 | ||
| EP16164373 | 2016-04-08 | ||
| EP16164595 | 2016-04-11 | ||
| EP16164595.7 | 2016-04-11 | ||
| EP16164593 | 2016-04-11 | ||
| EP16164593.2 | 2016-04-11 | ||
| EP16167626 | 2016-04-29 | ||
| EP16167626.7 | 2016-04-29 | ||
| EP16167634 | 2016-04-29 | ||
| EP16167634.1 | 2016-04-29 | ||
| EP16180274.9 | 2016-07-20 | ||
| EP16180274 | 2016-07-20 | ||
| EP16180255.8 | 2016-07-20 | ||
| EP16180254.1 | 2016-07-20 | ||
| EP16180255 | 2016-07-20 | ||
| EP16180254 | 2016-07-20 | ||
| EP16188591.8 | 2016-09-13 | ||
| EP16188591 | 2016-09-13 | ||
| EP16188590 | 2016-09-13 | ||
| EP16188590.0 | 2016-09-13 | ||
| EP16189478 | 2016-09-19 | ||
| EP16189382.1 | 2016-09-19 | ||
| EP16189383.9 | 2016-09-19 | ||
| EP16189478.7 | 2016-09-19 | ||
| EP16189383 | 2016-09-19 | ||
| EP16189382 | 2016-09-19 | ||
| EP16189474.6 | 2016-09-19 | ||
| EP16189474 | 2016-09-19 | ||
| EP16193206.6 | 2016-10-11 | ||
| EP16193206 | 2016-10-11 | ||
| EP16195489 | 2016-10-25 | ||
| EP16195489.6 | 2016-10-25 | ||
| PCT/EP2016/075836 WO2017080831A1 (en) | 2015-11-13 | 2016-10-26 | Method for the preparation of bis(fluorosulfonyl)-imide and of its salts |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2018535181A JP2018535181A (ja) | 2018-11-29 |
| JP2018535181A5 true JP2018535181A5 (https=) | 2019-12-05 |
Family
ID=58694705
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2018524477A Withdrawn JP2018535181A (ja) | 2015-11-13 | 2016-10-26 | ビス（フルオロスルホニル）−イミド及びこの塩を調製する方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US20180362343A1 (https=) |
| EP (1) | EP3334684A1 (https=) |
| JP (1) | JP2018535181A (https=) |
| KR (1) | KR20180083896A (https=) |
| CN (1) | CN108349737A (https=) |
| CA (1) | CA3004503A1 (https=) |
| WO (1) | WO2017080831A1 (https=) |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109264682B (zh) * | 2017-07-18 | 2019-11-29 | 九江天赐高新材料有限公司 | 一种高纯度二氟磺酰亚胺的制备方法 |
| EP3489192A1 (en) * | 2017-11-28 | 2019-05-29 | Nippon Shokubai Co., Ltd. | Lithium bis(fluorosulfonyl)imide composition |
| FR3081725A1 (fr) * | 2018-06-01 | 2019-12-06 | Arkema France | Procede de purification d'un sel de lithium du bis(fluorosulfonyl)imide |
| FR3081723B1 (fr) * | 2018-06-01 | 2022-04-15 | Arkema France | Procede de purification d'un sel de lithium de bis(fluorosulfonyl)imide |
| CN109264683B (zh) * | 2018-10-16 | 2021-07-27 | 广州理文科技有限公司 | 一种双（氟磺酰）亚胺的提取与纯化方法 |
| US10926190B2 (en) * | 2018-11-16 | 2021-02-23 | Ses Holdings Pte. Ltd. | Purified lithium bis(fluorosulfonyl)imide (LiFSI) products, methods of purifying crude LiFSI, and uses of purified LiFSI products |
| US10967295B2 (en) | 2018-11-16 | 2021-04-06 | Ses Holdings Pte. Ltd. | Processes for removing reactive solvent from lithium bis(fluorosulfonyl)imide (LiFSI) using organic solvents that are stable toward anodes in lithium-ion and lithium-metal batteries |
| US10734664B1 (en) * | 2019-03-01 | 2020-08-04 | Ses Holdings Pte. Ltd. | Purified hydrogen bis(fluorosulfonyl)imide (HFSI) products, methods of purifying crude HFSI, and uses of purified HFSI products |
| CN109721037B (zh) * | 2019-03-11 | 2019-12-24 | 上海如鲲新材料有限公司 | 一种双氟磺酰亚胺盐的新工艺 |
| KR102285464B1 (ko) * | 2019-03-28 | 2021-08-03 | 주식회사 천보 | 불소 음이온의 함유량이 저감된 비스(플루오로설포닐)이미드 리튬염(LiFSI)의 제조 방법 |
| CN109928372A (zh) * | 2019-04-12 | 2019-06-25 | 广州理文科技有限公司 | 一种双氟磺酰亚胺的制备方法 |
| US11267707B2 (en) | 2019-04-16 | 2022-03-08 | Honeywell International Inc | Purification of bis(fluorosulfonyl) imide |
| FR3095440B1 (fr) * | 2019-04-25 | 2022-03-25 | Arkema France | Procédé de préparation du bis(fluorosulfonyle) imide |
| US12319571B2 (en) | 2019-05-23 | 2025-06-03 | Nippon Shokubai Co., Ltd. | Bis(fluorosulfonyl)imide compound and method for producing same |
| JP2022510124A (ja) | 2019-08-22 | 2022-01-26 | フジアン ヨンジン テクノロジー カンパニー リミテッド | リチウムイオン電池用のフッ素化導電性塩の新しい合成プロセス |
| KR102625099B1 (ko) * | 2021-06-30 | 2024-01-15 | 주식회사 천보 | 비스(플루오로설포닐)이미드 알칼리금속염 |
| FR3130787B1 (fr) * | 2021-12-16 | 2023-11-03 | Arkema France | Procédé de préparation du bis(fluorosulfonyl)imidure de lithium |
| EP4719979A1 (en) * | 2023-06-02 | 2026-04-08 | Specialty Operations France | Method of removing one or more target impurities from crude fluorosulfonylimide compound |
| CN119191240B (zh) * | 2024-10-11 | 2025-11-18 | 福州大学 | 一种利用反应-萃取技术连续合成LiFSI的方法 |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4385047A (en) | 1981-01-05 | 1983-05-24 | Smithkline Beckman Corporation | Antiallergic imidodisulfamides |
| WO2007068822A2 (fr) * | 2005-12-12 | 2007-06-21 | Phostech Lithium Inc. | Sels de sulfonyl-1, 2, 4-triazole |
| CA2527575A1 (en) * | 2005-12-12 | 2007-06-12 | Christophe Michot | Salts and their utilization |
| CA2527802A1 (en) * | 2005-12-12 | 2007-06-12 | Christophe Michot | Synthesis of anhydrous imides lithium salts containing fluorosulfonyl or fluorophosphoryl substituent |
| WO2009123328A1 (en) | 2008-03-31 | 2009-10-08 | Nippon Shokubai Co., Ltd. | Sulfonylimide salt and method for producing the same |
| KR101291903B1 (ko) * | 2008-07-23 | 2013-07-31 | 다이이치 고교 세이야쿠 가부시키가이샤 | 비스(플루오로설포닐)이미드 음이온 화합물의 제조 방법과 이온대화합물 |
| KR101345271B1 (ko) | 2009-11-27 | 2013-12-27 | 가부시기가이샤 닛뽕쇼꾸바이 | 플루오로설포닐이미드염 및 플루오로설포닐이미드염의 제조방법 |
| JP5401336B2 (ja) * | 2010-01-15 | 2014-01-29 | 株式会社日本触媒 | フルオロスルホニルイミド塩の製造方法 |
| WO2011149095A1 (ja) | 2010-05-28 | 2011-12-01 | 株式会社日本触媒 | フルオロスルホニルイミドのアルカリ金属塩およびその製造方法 |
| WO2012108284A1 (ja) | 2011-02-10 | 2012-08-16 | 日本曹達株式会社 | フルオロスルホニルイミドアンモニウム塩の製造方法 |
| SG192235A1 (en) | 2011-03-03 | 2013-09-30 | Nippon Soda Co | Process for producing fluorine-containing sulfonylimide salt |
| KR20150061024A (ko) | 2011-03-03 | 2015-06-03 | 닛뽕소다 가부시키가이샤 | 플루오로술포닐이미드암모늄염의 제조 방법 |
| FR2975694B1 (fr) * | 2011-05-24 | 2013-08-02 | Arkema France | Procede de preparation de bis(fluorosulfonyl)imidure de lithium |
| FR2998297B1 (fr) * | 2012-11-22 | 2014-11-14 | Arkema France | Procede de preparation de sel d'imides contenant un groupement fluorosulfonyle |
| ES2545898T3 (es) | 2013-07-11 | 2015-09-16 | Lonza Ltd | Método para la preparación de compuestos de imidodisulfurilo |
| US8722005B1 (en) | 2013-07-26 | 2014-05-13 | Boulder Ionics Corporation | Synthesis of hydrogen bis(fluorosulfonyl)imide |
| CN104925765B (zh) * | 2015-05-21 | 2017-08-08 | 上海康鹏科技有限公司 | 一种双氟磺酰亚胺锂盐的制备方法 |
-
2016
- 2016-10-26 KR KR1020187016542A patent/KR20180083896A/ko not_active Withdrawn
- 2016-10-26 CA CA3004503A patent/CA3004503A1/en not_active Abandoned
- 2016-10-26 US US15/775,687 patent/US20180362343A1/en not_active Abandoned
- 2016-10-26 CN CN201680064971.XA patent/CN108349737A/zh active Pending
- 2016-10-26 JP JP2018524477A patent/JP2018535181A/ja not_active Withdrawn
- 2016-10-26 EP EP16788084.8A patent/EP3334684A1/en not_active Withdrawn
- 2016-10-26 WO PCT/EP2016/075836 patent/WO2017080831A1/en not_active Ceased
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