CN108349737A - 用于制备双(氟磺酰基)-酰亚胺及其盐的方法 - Google Patents

用于制备双(氟磺酰基)-酰亚胺及其盐的方法 Download PDF

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Publication number
CN108349737A
CN108349737A CN201680064971.XA CN201680064971A CN108349737A CN 108349737 A CN108349737 A CN 108349737A CN 201680064971 A CN201680064971 A CN 201680064971A CN 108349737 A CN108349737 A CN 108349737A
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China
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formula
compound
mixture
reac1
step1
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English (en)
Chinese (zh)
Inventor
安娜-克里斯蒂娜·霍莫斯
安德里亚·克莱因
克里斯蒂安·施耐德
托马斯·格吕茨纳
迈克尔·贝西耶
菲力普·斯图特
斯蒂芬·蒂勒
德西蕾·洛伦兹
希尔克-玛丽·洛伦兹
汉斯·哈塞
埃里克·文哈尔博
乔纳斯·诺伊豪斯
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Lonza AG
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Lonza AG
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Publication of CN108349737A publication Critical patent/CN108349737A/zh
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/086—Compounds containing nitrogen and non-metals and optionally metals containing one or more sulfur atoms
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/087—Compounds containing nitrogen and non-metals and optionally metals containing one or more hydrogen atoms
    • C01B21/093—Compounds containing nitrogen and non-metals and optionally metals containing one or more hydrogen atoms containing also one or more sulfur atoms
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/087—Compounds containing nitrogen and non-metals and optionally metals containing one or more hydrogen atoms
    • C01B21/093—Compounds containing nitrogen and non-metals and optionally metals containing one or more hydrogen atoms containing also one or more sulfur atoms
    • C01B21/0935—Imidodisulfonic acid; Nitrilotrisulfonic acid; Salts thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/36—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids
    • C07C303/40—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids by reactions not involving the formation of sulfonamide groups

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CN201680064971.XA 2015-11-13 2016-10-26 用于制备双(氟磺酰基)-酰亚胺及其盐的方法 Pending CN108349737A (zh)

Applications Claiming Priority (63)

Application Number Priority Date Filing Date Title
US201562254860P 2015-11-13 2015-11-13
US62/254,860 2015-11-13
EP15194513 2015-11-13
EP15194513.6 2015-11-13
EP15195231 2015-11-18
EP15195231.4 2015-11-18
US201662290523P 2016-02-03 2016-02-03
EP16153983.8 2016-02-03
US62/290,523 2016-02-03
EP16153983 2016-02-03
US201662308313P 2016-03-15 2016-03-15
EP16160248 2016-03-15
EP16160248.7 2016-03-15
EP16160245.3 2016-03-15
EP16160245 2016-03-15
US62/308,313 2016-03-15
EP16163045.4 2016-03-30
EP16163043.9 2016-03-30
EP16163043 2016-03-30
EP16163045 2016-03-30
EP16163835 2016-04-05
EP16163835.8 2016-04-05
EP16164023 2016-04-06
EP16164023.0 2016-04-06
EP16164146 2016-04-07
EP16164146.9 2016-04-07
EP16164148.5 2016-04-07
EP16164148 2016-04-07
EP16164373.9 2016-04-08
EP16164371 2016-04-08
EP16164371.3 2016-04-08
EP16164373 2016-04-08
EP16164595 2016-04-11
EP16164595.7 2016-04-11
EP16164593.2 2016-04-11
EP16164593 2016-04-11
EP16167626.7 2016-04-29
EP16167634 2016-04-29
EP16167634.1 2016-04-29
EP16167626 2016-04-29
EP16180274.9 2016-07-20
EP16180255 2016-07-20
EP16180274 2016-07-20
EP16180255.8 2016-07-20
EP16180254.1 2016-07-20
EP16180254 2016-07-20
EP16188591.8 2016-09-13
EP16188590.0 2016-09-13
EP16188590 2016-09-13
EP16188591 2016-09-13
EP16189383 2016-09-19
EP16189474.6 2016-09-19
EP16189382.1 2016-09-19
EP16189382 2016-09-19
EP16189478.7 2016-09-19
EP16189383.9 2016-09-19
EP16189474 2016-09-19
EP16189478 2016-09-19
EP16193206.6 2016-10-11
EP16193206 2016-10-11
EP16195489 2016-10-25
EP16195489.6 2016-10-25
PCT/EP2016/075836 WO2017080831A1 (en) 2015-11-13 2016-10-26 Method for the preparation of bis(fluorosulfonyl)-imide and of its salts

Publications (1)

Publication Number Publication Date
CN108349737A true CN108349737A (zh) 2018-07-31

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CN201680064971.XA Pending CN108349737A (zh) 2015-11-13 2016-10-26 用于制备双(氟磺酰基)-酰亚胺及其盐的方法

Country Status (7)

Country Link
US (1) US20180362343A1 (https=)
EP (1) EP3334684A1 (https=)
JP (1) JP2018535181A (https=)
KR (1) KR20180083896A (https=)
CN (1) CN108349737A (https=)
CA (1) CA3004503A1 (https=)
WO (1) WO2017080831A1 (https=)

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CN109264683A (zh) * 2018-10-16 2019-01-25 广州理文科技有限公司 一种双（氟磺酰）亚胺的提取与纯化方法
CN109928372A (zh) * 2019-04-12 2019-06-25 广州理文科技有限公司 一种双氟磺酰亚胺的制备方法

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CN109264682B (zh) * 2017-07-18 2019-11-29 九江天赐高新材料有限公司 一种高纯度二氟磺酰亚胺的制备方法
EP3489192A1 (en) * 2017-11-28 2019-05-29 Nippon Shokubai Co., Ltd. Lithium bis(fluorosulfonyl)imide composition
FR3081725A1 (fr) * 2018-06-01 2019-12-06 Arkema France Procede de purification d'un sel de lithium du bis(fluorosulfonyl)imide
FR3081723B1 (fr) * 2018-06-01 2022-04-15 Arkema France Procede de purification d'un sel de lithium de bis(fluorosulfonyl)imide
US10967295B2 (en) 2018-11-16 2021-04-06 Ses Holdings Pte. Ltd. Processes for removing reactive solvent from lithium bis(fluorosulfonyl)imide (LiFSI) using organic solvents that are stable toward anodes in lithium-ion and lithium-metal batteries
US10926190B2 (en) * 2018-11-16 2021-02-23 Ses Holdings Pte. Ltd. Purified lithium bis(fluorosulfonyl)imide (LiFSI) products, methods of purifying crude LiFSI, and uses of purified LiFSI products
US10734664B1 (en) * 2019-03-01 2020-08-04 Ses Holdings Pte. Ltd. Purified hydrogen bis(fluorosulfonyl)imide (HFSI) products, methods of purifying crude HFSI, and uses of purified HFSI products
CN109721037B (zh) * 2019-03-11 2019-12-24 上海如鲲新材料有限公司 一种双氟磺酰亚胺盐的新工艺
KR102285464B1 (ko) * 2019-03-28 2021-08-03 주식회사 천보 불소 음이온의 함유량이 저감된 비스(플루오로설포닐)이미드 리튬염(LiFSI)의 제조 방법
US11267707B2 (en) * 2019-04-16 2022-03-08 Honeywell International Inc Purification of bis(fluorosulfonyl) imide
FR3095440B1 (fr) * 2019-04-25 2022-03-25 Arkema France Procédé de préparation du bis(fluorosulfonyle) imide
JP7266092B2 (ja) * 2019-05-23 2023-04-27 株式会社日本触媒 ビス（フルオロスルホニル）イミド化合物及びその製造方法
JP2022510124A (ja) 2019-08-22 2022-01-26 フジアン ヨンジン テクノロジー カンパニー リミテッド リチウムイオン電池用のフッ素化導電性塩の新しい合成プロセス
KR102625099B1 (ko) * 2021-06-30 2024-01-15 주식회사 천보 비스(플루오로설포닐)이미드 알칼리금속염
CN121219231A (zh) * 2023-06-02 2025-12-26 法国特种经营公司 从粗氟磺酰亚胺化合物中去除一种或多种目标杂质的方法
CN119191240B (zh) * 2024-10-11 2025-11-18 福州大学 一种利用反应-萃取技术连续合成LiFSI的方法

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WO2007068822A2 (fr) * 2005-12-12 2007-06-21 Phostech Lithium Inc. Sels de sulfonyl-1, 2, 4-triazole
CN101980955A (zh) * 2008-03-31 2011-02-23 株式会社日本触媒 磺酰亚胺盐及其制备方法
JPWO2010010613A1 (ja) * 2008-07-23 2012-01-05 第一工業製薬株式会社 ビス（フルオロスルホニル）イミドアニオン化合物の製造方法およびイオン対化合物
CN103347811A (zh) * 2011-02-10 2013-10-09 日本曹达株式会社 氟磺酰亚胺铵盐的制造方法
JP5401336B2 (ja) * 2010-01-15 2014-01-29 株式会社日本触媒 フルオロスルホニルイミド塩の製造方法
CN103562129A (zh) * 2011-05-24 2014-02-05 阿克马法国公司 双(氟代磺酰基)酰亚胺锂或双(氟代磺酰基)酰亚胺钠的生产方法
CN104755418A (zh) * 2012-11-22 2015-07-01 阿克马法国公司 用于制备含有氟磺酰基基团的酰亚胺盐的方法
CN104925765A (zh) * 2015-05-21 2015-09-23 上海康鹏化学有限公司 一种双氟磺酰亚胺锂盐的制备方法

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HUE042926T2 (hu) 2010-05-28 2019-07-29 Nippon Catalytic Chem Ind Fluorszulfonil-imid alkálifém só, és eljárás annak elõállítására
CA2826375C (en) 2011-03-03 2016-02-16 Nippon Soda Co., Ltd. Process for producing fluorine-containing sulfonylimide salt
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CA2527575A1 (en) * 2005-12-12 2007-06-12 Christophe Michot Salts and their utilization
WO2007068822A2 (fr) * 2005-12-12 2007-06-21 Phostech Lithium Inc. Sels de sulfonyl-1, 2, 4-triazole
CN101980955A (zh) * 2008-03-31 2011-02-23 株式会社日本触媒 磺酰亚胺盐及其制备方法
JPWO2010010613A1 (ja) * 2008-07-23 2012-01-05 第一工業製薬株式会社 ビス（フルオロスルホニル）イミドアニオン化合物の製造方法およびイオン対化合物
JP5401336B2 (ja) * 2010-01-15 2014-01-29 株式会社日本触媒 フルオロスルホニルイミド塩の製造方法
CN103347811A (zh) * 2011-02-10 2013-10-09 日本曹达株式会社 氟磺酰亚胺铵盐的制造方法
CN103562129A (zh) * 2011-05-24 2014-02-05 阿克马法国公司 双(氟代磺酰基)酰亚胺锂或双(氟代磺酰基)酰亚胺钠的生产方法
CN104755418A (zh) * 2012-11-22 2015-07-01 阿克马法国公司 用于制备含有氟磺酰基基团的酰亚胺盐的方法
CN104925765A (zh) * 2015-05-21 2015-09-23 上海康鹏化学有限公司 一种双氟磺酰亚胺锂盐的制备方法

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109264683A (zh) * 2018-10-16 2019-01-25 广州理文科技有限公司 一种双（氟磺酰）亚胺的提取与纯化方法
CN109264683B (zh) * 2018-10-16 2021-07-27 广州理文科技有限公司 一种双（氟磺酰）亚胺的提取与纯化方法
CN109928372A (zh) * 2019-04-12 2019-06-25 广州理文科技有限公司 一种双氟磺酰亚胺的制备方法

Also Published As

Publication number Publication date
CA3004503A1 (en) 2017-05-18
KR20180083896A (ko) 2018-07-23
US20180362343A1 (en) 2018-12-20
EP3334684A1 (en) 2018-06-20
WO2017080831A1 (en) 2017-05-18
JP2018535181A (ja) 2018-11-29

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