JP2017532390A - 塗布ポリエステルフィルムを含む積層体 - Google Patents
塗布ポリエステルフィルムを含む積層体 Download PDFInfo
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- JP2017532390A JP2017532390A JP2017508018A JP2017508018A JP2017532390A JP 2017532390 A JP2017532390 A JP 2017532390A JP 2017508018 A JP2017508018 A JP 2017508018A JP 2017508018 A JP2017508018 A JP 2017508018A JP 2017532390 A JP2017532390 A JP 2017532390A
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- film
- polymer
- adhesive
- carboxylic acid
- coated
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- 229920000642 polymer Polymers 0.000 claims abstract description 81
- 239000000853 adhesive Substances 0.000 claims abstract description 76
- 230000001070 adhesive effect Effects 0.000 claims abstract description 76
- -1 polypropylene Polymers 0.000 claims abstract description 63
- 239000004743 Polypropylene Substances 0.000 claims abstract description 47
- 229920001155 polypropylene Polymers 0.000 claims abstract description 40
- 239000003431 cross linking reagent Substances 0.000 claims abstract description 32
- 229920006254 polymer film Polymers 0.000 claims abstract description 26
- 150000001732 carboxylic acid derivatives Chemical class 0.000 claims abstract description 18
- 229920005629 polypropylene homopolymer Polymers 0.000 claims abstract description 15
- 229920005606 polypropylene copolymer Polymers 0.000 claims abstract description 11
- 150000008064 anhydrides Chemical class 0.000 claims abstract description 10
- IMSODMZESSGVBE-UHFFFAOYSA-N 2-Oxazoline Chemical compound C1CN=CO1 IMSODMZESSGVBE-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000011247 coating layer Substances 0.000 claims description 50
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- 150000002918 oxazolines Chemical class 0.000 claims description 28
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- 239000000203 mixture Substances 0.000 claims description 21
- 239000002245 particle Substances 0.000 claims description 20
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- 150000001875 compounds Chemical class 0.000 claims description 15
- 229920000139 polyethylene terephthalate Polymers 0.000 claims description 15
- 239000005020 polyethylene terephthalate Substances 0.000 claims description 15
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 14
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 claims description 12
- 239000004814 polyurethane Substances 0.000 claims description 11
- 229920002635 polyurethane Polymers 0.000 claims description 11
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims description 10
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- 125000004432 carbon atom Chemical group C* 0.000 claims description 8
- 229910052751 metal Inorganic materials 0.000 claims description 7
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- 239000004408 titanium dioxide Substances 0.000 claims description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- 229920000877 Melamine resin Polymers 0.000 claims description 6
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 claims description 6
- 239000004593 Epoxy Substances 0.000 claims description 5
- 150000008065 acid anhydrides Chemical class 0.000 claims description 5
- 239000012948 isocyanate Substances 0.000 claims description 5
- 150000002513 isocyanates Chemical class 0.000 claims description 5
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 5
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 4
- 125000000217 alkyl group Chemical group 0.000 claims description 4
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- 238000010438 heat treatment Methods 0.000 claims description 4
- 229920000058 polyacrylate Polymers 0.000 claims description 4
- 239000012463 white pigment Substances 0.000 claims description 4
- 239000004698 Polyethylene Substances 0.000 claims description 3
- 125000002015 acyclic group Chemical group 0.000 claims description 3
- 125000003710 aryl alkyl group Chemical group 0.000 claims description 3
- 150000001718 carbodiimides Chemical class 0.000 claims description 3
- 239000000919 ceramic Substances 0.000 claims description 3
- 150000001991 dicarboxylic acids Chemical class 0.000 claims description 3
- 125000005843 halogen group Chemical group 0.000 claims description 3
- 239000000123 paper Substances 0.000 claims description 3
- 229920000573 polyethylene Polymers 0.000 claims description 3
- QYKIQEUNHZKYBP-UHFFFAOYSA-N Vinyl ether Chemical compound C=COC=C QYKIQEUNHZKYBP-UHFFFAOYSA-N 0.000 claims description 2
- 150000001408 amides Chemical class 0.000 claims description 2
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- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 2
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- 229920000554 ionomer Polymers 0.000 abstract description 2
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- 239000012790 adhesive layer Substances 0.000 description 17
- 239000006185 dispersion Substances 0.000 description 10
- 125000003504 2-oxazolinyl group Chemical group O1C(=NCC1)* 0.000 description 9
- 239000007788 liquid Substances 0.000 description 9
- 239000004971 Cross linker Substances 0.000 description 8
- 238000000034 method Methods 0.000 description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 7
- 239000012963 UV stabilizer Substances 0.000 description 7
- 230000008901 benefit Effects 0.000 description 7
- 238000003851 corona treatment Methods 0.000 description 7
- 239000000945 filler Substances 0.000 description 7
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 6
- 150000001298 alcohols Chemical class 0.000 description 6
- VPKDCDLSJZCGKE-UHFFFAOYSA-N carbodiimide group Chemical group N=C=N VPKDCDLSJZCGKE-UHFFFAOYSA-N 0.000 description 6
- 238000007756 gravure coating Methods 0.000 description 6
- 229920001519 homopolymer Polymers 0.000 description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 5
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 5
- 125000005442 diisocyanate group Chemical group 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
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- 239000003795 chemical substances by application Substances 0.000 description 4
- 239000008199 coating composition Substances 0.000 description 4
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- 239000000155 melt Substances 0.000 description 4
- 229920006280 packaging film Polymers 0.000 description 4
- 239000012785 packaging film Substances 0.000 description 4
- 229920000728 polyester Polymers 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- HIXDQWDOVZUNNA-UHFFFAOYSA-N 2-(3,4-dimethoxyphenyl)-5-hydroxy-7-methoxychromen-4-one Chemical compound C=1C(OC)=CC(O)=C(C(C=2)=O)C=1OC=2C1=CC=C(OC)C(OC)=C1 HIXDQWDOVZUNNA-UHFFFAOYSA-N 0.000 description 3
- AOBIOSPNXBMOAT-UHFFFAOYSA-N 2-[2-(oxiran-2-ylmethoxy)ethoxymethyl]oxirane Chemical compound C1OC1COCCOCC1CO1 AOBIOSPNXBMOAT-UHFFFAOYSA-N 0.000 description 3
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 3
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- MBHRHUJRKGNOKX-UHFFFAOYSA-N [(4,6-diamino-1,3,5-triazin-2-yl)amino]methanol Chemical class NC1=NC(N)=NC(NCO)=N1 MBHRHUJRKGNOKX-UHFFFAOYSA-N 0.000 description 3
- 229910000019 calcium carbonate Inorganic materials 0.000 description 3
- 150000001735 carboxylic acids Chemical class 0.000 description 3
- 238000004132 cross linking Methods 0.000 description 3
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 3
- 239000000835 fiber Substances 0.000 description 3
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- HJIAMFHSAAEUKR-UHFFFAOYSA-N (2-hydroxyphenyl)-phenylmethanone Chemical compound OC1=CC=CC=C1C(=O)C1=CC=CC=C1 HJIAMFHSAAEUKR-UHFFFAOYSA-N 0.000 description 2
- OZAIFHULBGXAKX-UHFFFAOYSA-N 2-(2-cyanopropan-2-yldiazenyl)-2-methylpropanenitrile Chemical compound N#CC(C)(C)N=NC(C)(C)C#N OZAIFHULBGXAKX-UHFFFAOYSA-N 0.000 description 2
- PHBCDAHASFSLMJ-UHFFFAOYSA-N 2-hydroxybenzotriazole Chemical compound C1=CC=CC2=NN(O)N=C21 PHBCDAHASFSLMJ-UHFFFAOYSA-N 0.000 description 2
- LPIQIQPLUVLISR-UHFFFAOYSA-N 2-prop-1-en-2-yl-4,5-dihydro-1,3-oxazole Chemical compound CC(=C)C1=NCCO1 LPIQIQPLUVLISR-UHFFFAOYSA-N 0.000 description 2
- UPMLOUAZCHDJJD-UHFFFAOYSA-N 4,4'-Diphenylmethane Diisocyanate Chemical compound C1=CC(N=C=O)=CC=C1CC1=CC=C(N=C=O)C=C1 UPMLOUAZCHDJJD-UHFFFAOYSA-N 0.000 description 2
- HQQTZCPKNZVLFF-UHFFFAOYSA-N 4h-1,2-benzoxazin-3-one Chemical class C1=CC=C2ONC(=O)CC2=C1 HQQTZCPKNZVLFF-UHFFFAOYSA-N 0.000 description 2
- 239000005995 Aluminium silicate Substances 0.000 description 2
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 2
- SOGAXMICEFXMKE-UHFFFAOYSA-N Butylmethacrylate Chemical compound CCCCOC(=O)C(C)=C SOGAXMICEFXMKE-UHFFFAOYSA-N 0.000 description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 2
- 239000005058 Isophorone diisocyanate Substances 0.000 description 2
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
- MZRVEZGGRBJDDB-UHFFFAOYSA-N N-Butyllithium Chemical compound [Li]CCCC MZRVEZGGRBJDDB-UHFFFAOYSA-N 0.000 description 2
- IIGAAOXXRKTFAM-UHFFFAOYSA-N N=C=O.N=C=O.CC1=C(C)C(C)=C(C)C(C)=C1C Chemical compound N=C=O.N=C=O.CC1=C(C)C(C)=C(C)C(C)=C1C IIGAAOXXRKTFAM-UHFFFAOYSA-N 0.000 description 2
- 239000002202 Polyethylene glycol Substances 0.000 description 2
- QQONPFPTGQHPMA-UHFFFAOYSA-N Propene Chemical compound CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 2
- 235000012211 aluminium silicate Nutrition 0.000 description 2
- 239000002518 antifoaming agent Substances 0.000 description 2
- 239000003963 antioxidant agent Substances 0.000 description 2
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 2
- 229910052794 bromium Inorganic materials 0.000 description 2
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 description 2
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- HGCIXCUEYOPUTN-UHFFFAOYSA-N cyclohexene Chemical compound C1CCC=CC1 HGCIXCUEYOPUTN-UHFFFAOYSA-N 0.000 description 2
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- RRAMGCGOFNQTLD-UHFFFAOYSA-N hexamethylene diisocyanate Chemical compound O=C=NCCCCCCN=C=O RRAMGCGOFNQTLD-UHFFFAOYSA-N 0.000 description 2
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- IQPQWNKOIGAROB-UHFFFAOYSA-N isocyanate group Chemical group [N-]=C=O IQPQWNKOIGAROB-UHFFFAOYSA-N 0.000 description 2
- NIMLQBUJDJZYEJ-UHFFFAOYSA-N isophorone diisocyanate Chemical compound CC1(C)CC(N=C=O)CC(C)(CN=C=O)C1 NIMLQBUJDJZYEJ-UHFFFAOYSA-N 0.000 description 2
- QQVIHTHCMHWDBS-UHFFFAOYSA-N isophthalic acid Chemical compound OC(=O)C1=CC=CC(C(O)=O)=C1 QQVIHTHCMHWDBS-UHFFFAOYSA-N 0.000 description 2
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 2
- 239000004611 light stabiliser Substances 0.000 description 2
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- BDJRBEYXGGNYIS-UHFFFAOYSA-N nonanedioic acid Chemical compound OC(=O)CCCCCCCC(O)=O BDJRBEYXGGNYIS-UHFFFAOYSA-N 0.000 description 2
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- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 2
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- 239000002904 solvent Substances 0.000 description 2
- TYFQFVWCELRYAO-UHFFFAOYSA-N suberic acid Chemical compound OC(=O)CCCCCCC(O)=O TYFQFVWCELRYAO-UHFFFAOYSA-N 0.000 description 2
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- GNQKHBSIBXSFFD-UHFFFAOYSA-N 1,3-diisocyanatocyclohexane Chemical compound O=C=NC1CCCC(N=C=O)C1 GNQKHBSIBXSFFD-UHFFFAOYSA-N 0.000 description 1
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- OVBFMUAFNIIQAL-UHFFFAOYSA-N 1,4-diisocyanatobutane Chemical compound O=C=NCCCCN=C=O OVBFMUAFNIIQAL-UHFFFAOYSA-N 0.000 description 1
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- VZXPHDGHQXLXJC-UHFFFAOYSA-N 1,6-diisocyanato-5,6-dimethylheptane Chemical compound O=C=NC(C)(C)C(C)CCCCN=C=O VZXPHDGHQXLXJC-UHFFFAOYSA-N 0.000 description 1
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- LFSYUSUFCBOHGU-UHFFFAOYSA-N 1-isocyanato-2-[(4-isocyanatophenyl)methyl]benzene Chemical compound C1=CC(N=C=O)=CC=C1CC1=CC=CC=C1N=C=O LFSYUSUFCBOHGU-UHFFFAOYSA-N 0.000 description 1
- ICLCCFKUSALICQ-UHFFFAOYSA-N 1-isocyanato-4-(4-isocyanato-3-methylphenyl)-2-methylbenzene Chemical compound C1=C(N=C=O)C(C)=CC(C=2C=C(C)C(N=C=O)=CC=2)=C1 ICLCCFKUSALICQ-UHFFFAOYSA-N 0.000 description 1
- RTBFRGCFXZNCOE-UHFFFAOYSA-N 1-methylsulfonylpiperidin-4-one Chemical compound CS(=O)(=O)N1CCC(=O)CC1 RTBFRGCFXZNCOE-UHFFFAOYSA-N 0.000 description 1
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 1
- JAHNSTQSQJOJLO-UHFFFAOYSA-N 2-(3-fluorophenyl)-1h-imidazole Chemical compound FC1=CC=CC(C=2NC=CN=2)=C1 JAHNSTQSQJOJLO-UHFFFAOYSA-N 0.000 description 1
- OEPOKWHJYJXUGD-UHFFFAOYSA-N 2-(3-phenylmethoxyphenyl)-1,3-thiazole-4-carbaldehyde Chemical compound O=CC1=CSC(C=2C=C(OCC=3C=CC=CC=3)C=CC=2)=N1 OEPOKWHJYJXUGD-UHFFFAOYSA-N 0.000 description 1
- OOYBPMOLCOFJHM-UHFFFAOYSA-N 2-(benzotriazol-2-yl)-4-(2,3,3-trimethylbutan-2-yl)phenol Chemical compound CC(C)(C)C(C)(C)C1=CC=C(O)C(N2N=C3C=CC=CC3=N2)=C1 OOYBPMOLCOFJHM-UHFFFAOYSA-N 0.000 description 1
- BBITXNWQALLODC-UHFFFAOYSA-N 2-[4-(4-oxo-3,1-benzoxazin-2-yl)phenyl]-3,1-benzoxazin-4-one Chemical compound C1=CC=C2C(=O)OC(C3=CC=C(C=C3)C=3OC(C4=CC=CC=C4N=3)=O)=NC2=C1 BBITXNWQALLODC-UHFFFAOYSA-N 0.000 description 1
- KUAUJXBLDYVELT-UHFFFAOYSA-N 2-[[2,2-dimethyl-3-(oxiran-2-ylmethoxy)propoxy]methyl]oxirane Chemical compound C1OC1COCC(C)(C)COCC1CO1 KUAUJXBLDYVELT-UHFFFAOYSA-N 0.000 description 1
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Abstract
Description
本明細書および図面における符号の繰返し使用は、本発明の同じ又は類似の特徴または要素を意図するものである。
PETペレットを単軸押出器に導入し、加熱圧縮して溶融状態にした。スロットダイを介してこの溶融体を押出し、20℃のキャストロール上に製膜し、固化して非晶プレフィルムを作成した。このプレフィルムを長手方向に95℃で3.6:1の延伸比で延伸した。次いでこの延伸フィルムはコロナ処理機(Enercon Industries社製)を通過した。コロナ処理は1.5W/ft2分で行った。
実施例1に記載の方法によってフィルムサンプルを調製した。フィルムサンプルは、塗布PETフィルムの塗布層とは反対側にLDPE系シール層を有する3.5ミル厚の共押出包装用フィルムを直接シールした。重ね合わせたシートは2秒間、熱積層された。熱積層後、それぞれの積層体を冷却し、剥離テスト用に幅1インチ、長さ6インチの積層体片にカットした。積層体を加圧室に配置し、レトルトと同様の121℃で相対湿度100%の熱処理サイクルを180分行った。サンプルを取りだし、乾燥したのち、MTSテストリグ上で180°剥離テストを行うことにより評価した。レトルト処理テストしたサンプルから4積層体について評価した。シール時間2秒および4秒で同じ条件によって作成され且つレトルト処理していないサンプルについて平均剥離力値と共に、平均剥離力値を以下の表に示す。
18%の硫酸バリウムを充填したPETペレットを単軸押出器に導入し、加熱圧縮して溶融状態にした。スロットダイを介してこの溶融体を押出し、20℃のキャストロール上に製膜し、固化して非晶プレフィルムを作成した。このプレフィルムを長手方向に95℃で3.6:1の延伸比で延伸した。次いでこの延伸フィルムはコロナ処理機(Enercon Industries社製)を通過した。コロナ処理は1.5W/ft2分で行った。
PETペレットを二酸化チタンPETマスターバッチに混合し、一軸押出機に導入し、加熱圧縮して溶融状態にした。溶融体は13%のTiO2を含有し、スロットダイを通じて押出し、20℃に保持した製膜ロール上で製膜し、固化して非晶フィルム前駆体を得た。フィルム前駆体は、95℃で3.6:1の比で長手方向に延伸した。延伸フィルムはコロナ処理機(Enercon Industries)を通過させ、1.5W/ft2・分の出力でコロナ処理を行った。
Claims (35)
- 第1表面と第2表面を有する二軸延伸ポリエステルフィルムと、当該二軸延伸ポリエステルフィルムの第1表面上の塗布層とから成る塗布フィルムであって、当該塗布層は接着剤および架橋剤から成り、当該接着剤は酸または酸無水物で変性されたポリプロピレンホモポリマー又はコポリマーから成り、当該ポリプロピレンホモポリマー又はコポリマーを変性するために使用される酸または酸無水物が、1〜28の炭素原子数を有する炭素鎖から成ることを特徴とする塗布フィルム。
- 酸または酸無水物で変性されたポリプロピレンホモポリマー又はコポリマーが、カルボン酸またはカルボン酸無水物で変性されたポリプロピレンホモポリマー又はコポリマーから成る請求項1に記載の塗布フィルム。
- カルボン酸またはカルボン酸無水物で変性されたポリプロピレンホモポリマー又はコポリマーが、1〜10の炭素原子数を有する炭素鎖から成るカルボン酸またはカルボン酸無水物で変性された請求項2に記載の塗布フィルム。
- カルボン酸またはカルボン酸無水物で変性されたポリプロピレンが、ジカルボン酸またはジカルボン酸無水物を使用して形成される請求項2に記載の塗布フィルム。
- カルボン酸またはカルボン酸無水物で変性されたポリプロピレンが、不飽和ジカルボン酸または不飽和ジカルボン酸無水物を使用して形成される請求項2〜4の何れかに記載の塗布フィルム。
- カルボン酸またはカルボン酸無水物で変性されたポリプロピレンが、ジカルボン酸無水物を使用して形成される請求項2〜5の何れかに記載の塗布フィルム。
- カルボン酸またはカルボン酸無水物で変性されたポリプロピレンが、無水マレイン酸を使用して形成される請求項2〜6の何れかに記載の塗布フィルム。
- 塗布層の架橋剤に対する接着剤の重量比(接着剤:架橋剤)が3:7〜20:1、好ましくは1:1〜9:1である請求項1〜7の何れかに記載の塗布フィルム。
- 塗布層に含まれる架橋剤がオキサゾリンポリマーから成る請求項1〜8の何れかに記載の塗布フィルム。
- ポリマーフィルムが、フィルムに白色を付与するのに十分な顔料粒子を含有する請求項1〜9の何れかに記載の塗布フィルム。
- 白色顔料粒子が硫酸バリウム粒子から成り、ポリマーフィルムのBerger白色度が70を超える請求項10に記載の塗布フィルム。
- 白色顔料粒子が二酸化チタン粒子から成り、フィルム中の含有量が5〜20重量%である請求項10に記載の塗布フィルム。
- ポリマーフィルムが0.1〜15ミルの厚さの二軸延伸ポリエステルフィルムから成り、塗布層の厚さが10〜60nmである請求項1〜12の何れかに記載の塗布フィルム。
- ポリエステルフィルムの第1表面上に塗布層が印刷されている請求項1〜13の何れかに記載の塗布フィルム。
- ポリエステルフィルムの第2表面上に第2塗布層を更に有し、第2塗布層は架橋剤から成る請求項1〜14の何れかに記載の塗布フィルム。
- 第2塗布層が架橋剤と接着剤との組合せから成る請求項15に記載の塗布フィルム。
- 塗布層が熱処理によってポリエステルフィルムの第1表面に接着されている請求項1〜16の何れかに記載の塗布フィルム。
- 共重合モノマー(b)が、メタクリル酸エステル、不飽和カルボン酸、不飽和ニトリル、不飽和アミド、ビニルエステル、ビニルエーテル、α−オレフィン,ハロゲン化α,β−不飽和化合物およびα,β−不飽和芳香族化合物から選択される1つ以上から成る請求項18に記載の塗布フィルム。
- ポリエステルフィルムがポリエチレンテレフタレートから成る請求項1〜19の何れかに記載の塗布フィルム。
- 架橋剤がオキサゾリン変性アクリルポリマーから成る請求項1〜20の何れかに記載の塗布フィルム。
- 第1表面と第2表面とを有するポリエステルフィルムと、ポリエステルフィルムの第1表面上の塗布層と、当該塗布層を介してポリエステルフィルムに接着されるポリマー物品とから成る積層体であって、当該塗布層は接着剤と架橋剤とからなり、当該接着剤はカルボン酸変性ポリプロピレンホモポリマー又はコポリマーから成り、当該変性に使用されるカルボン酸が無水カルボン酸から成りかつ1〜10の炭素原子数を有する炭素鎖を有し、当該架橋剤が、オキサゾリン、カルボジイミド、エポキシ、イソシアネート又はメラミンから成り、当該塗布層はポリエステルフィルムをポリマー物品に接着し、当該ポリマー物品はポリオレフィンから成ることを特徴とする積層体。
- ポリマー物品がポリオレフィンフィルムから成る請求項22に記載の積層体。
- ポリオレフィンポリプロピレンホモポリマーから成る請求項23に記載の積層体。
- ポリマー物品が成形品である請求項22に記載の積層体。
- 成形品がポリプロピレンポリマーから成る請求項25に記載の積層体。
- 成形品がポリプロピレンホモポリマーから成る請求項25に記載の積層体。
- 成形品が繊維強化ポリプロピレンから形成されている請求項25〜27の何れかに記載の積層体。
- 塗布層に含有される接着剤がマレイン酸変性ポリプロピレンコポリマーから成り、塗布層に含有される架橋剤がオキサゾリンポリマーから成る請求項22〜28の何れかに記載の積層体。
- 成形品がポリエチレンポリマーから成る請求項25に記載の積層体。
- 成形品がエチレン−プロピレンコポリマーから成る請求項25に記載の積層体。
- ポリエステルフィルムが第2表面に第2塗布層を有し、第2塗布層が架橋剤から成る請求項22に記載の積層体。
- 更に、ポリエステルフィルムの第2表面にポリウレタン組成物が接着されている請求項32に記載の積層体。
- 更に、積層体が、ポリウレタン組成物に接着されている造形品を有する請求項33に記載の積層体。
- 造形品が、金属製、セラミック製、紙製または木製の物品から成る請求項34に記載の積層体。
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US9987818B2 (en) * | 2014-01-16 | 2018-06-05 | Research Foundation Of The City University Of New York | Center-side method of producing superhydrophobic surface |
KR102516807B1 (ko) | 2014-08-14 | 2023-03-31 | 미츠비시 폴리에스테르 필름 인코포레이티드 | 코팅된 폴리에스테르 필름을 함유하는 적층 |
WO2016025907A1 (en) | 2014-08-15 | 2016-02-18 | Xamax Industries, Inc. | Composite thermoplastic laminate |
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US10882284B2 (en) | 2021-01-05 |
US20210086486A1 (en) | 2021-03-25 |
KR102516807B1 (ko) | 2023-03-31 |
WO2016025563A1 (en) | 2016-02-18 |
US11725089B2 (en) | 2023-08-15 |
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