JP2014237805A - 放熱性粉体塗料組成物、放熱性塗膜、及び被塗装物 - Google Patents
放熱性粉体塗料組成物、放熱性塗膜、及び被塗装物 Download PDFInfo
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- JP2014237805A JP2014237805A JP2014039012A JP2014039012A JP2014237805A JP 2014237805 A JP2014237805 A JP 2014237805A JP 2014039012 A JP2014039012 A JP 2014039012A JP 2014039012 A JP2014039012 A JP 2014039012A JP 2014237805 A JP2014237805 A JP 2014237805A
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K5/00—Heat-transfer, heat-exchange or heat-storage materials, e.g. refrigerants; Materials for the production of heat or cold by chemical reactions other than by combustion
- C09K5/08—Materials not undergoing a change of physical state when used
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
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- C08G18/8074—Lactams
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
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- C—CHEMISTRY; METALLURGY
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Abstract
【解決手段】エポキシ樹脂(a1)と、水酸基及び/又はカルボキシル基を有するポリエステル樹脂(a2)とからなる群から選択される少なくとも1種のバインダー樹脂(A)を含み、かつ、熱伝導度が0.2W/mK以上100W/mK未満の放熱性フィラー(B)を10質量%以上40質量%以下と、を含有する放熱性粉体塗料組成物。
【選択図】図1
Description
また、本願において「粉体塗料組成物」とは、揮発分を含まず、バインダー樹脂に放熱性フィラー(無機粒子)を配合したものであり、かつ常温において固体粉末状のものをいう。また、「放熱性粉体塗料組成物」とは、粉体塗料組成物のうち、組成物自体が熱伝導性や放射性による積極的な放熱性を備えているものをいう。
<実施例>
金属基材(アルミニウムの板、サイズは約120mm長×約50mm幅×約2mm厚)の表面に、熱源として抵抗器(シャント抵抗器、PCN社製、型番PBH1ΩD、定格電力10W、サイズ約2cm長×約1.5cm幅×約0.5cm厚)を、市販の熱伝導性両面テープ(商品名:NO.5046熱伝導性テープ、マクセルスリオンテック(株)製)によって固定した。測定雰囲気の温度を25℃に設定した後、該シャント抵抗器に一定の電流(3.2A)を印加することによって該シャント抵抗器の温度を100℃に上昇させ、温度を安定化させた。
市販のビスフェノールA型エポキシ樹脂(※1)32部、市販のオルトクレゾールノボラック型エポキシ樹脂(※4)3部、市販のビスフェノールA型フェノール樹脂(※8)8部、市販の多孔質シリカ粉末(※11)6部、市販のフッ化カルシウム粉末(※12)16部、市販の酸化チタン粉末(※13)20部、市販の重質炭酸カルシウム(※14)13部、及び市販のアクリル系表面調整剤1部からなる粉末塗料を上述の金属基材の表面に適用した。具体的には、該金属基材の表面上において該粉末塗料から形成された塗膜を約140℃の条件下で約15分間、加熱し軟化させた後又は溶融させた後に硬化することによって、放熱性硬化塗膜(約30μm)を備える試験基材を作製した。なお、※印で示された各製品の具体的な内容は後述する。
次いで、実施例1において作製された試験基材の裏面に、図1に示すように、上述の熱伝導性両面テープを用いて上述のシャント抵抗器を固定した。測定雰囲気の温度を25℃に設定した後、該シャント抵抗器に一定の電流(3.2A)を印加した上で、該シャント抵抗器の温度を測定した。その結果、上述の金属基材自身の基準温度(100℃)に対して、11.9℃低くなったことを確認した。なお、表1及び表2においては、基準温度から低くなった場合に、「マイナス」の数値として表している。
実施例1に係る焼付処理板について、塗膜の密着力をJIS D0202で定める碁盤目試験に準拠して評価した。具体的には、塗膜表面にカッターナイフで100個の碁盤目を作製し、市販の粘着テープを圧着させた後1〜2分間放置し、垂直方向に剥離したときの塗膜の残存程度を、以下の基準で目視評価した。評価結果を表1に示す。後述するその他の実施例、及び各比較例の処理板についても同様に処理及び評価した。比較例の結果は表2に示す。
1:密着性良好(残存率95以上100%以下)
2:密着性やや良好(残存率65%以上95%未満)
3:密着性不良(残存率65%未満〜全剥離)
1:耐熱性(密着性)良好(残存率95以上100%以下)
2:耐熱性(密着性)やや良好(残存率65%以上95%未満)
3:耐熱性(密着性)不良(残存率65%未満〜全剥離)
JIS K5400の鉛筆硬度試験に準拠した。まず9H〜6Bの各硬度の鉛筆を準備して所定の冶具を用いて塗膜表面をスクラッチし、塗膜表面に傷が付くようになる鉛筆の硬度を評価した。評価基準は、硬い順に9H、8H、7H、6H、5H、4H、3H、2H、H、F、HB、B、2B、3B、4B、5B、6Bであり、鉛筆硬度がB以上の場合に実用上の問題はないと評価した。各実施例の結果を表1に示し、各比較例の結果は表2に示す。
JIS K5600の促進耐候性試験に準拠した。未曝露の塗膜と、キセノンランプを用いたサンシャインウェザオメーターに暴露して3000時間経過後の塗膜を目視観察にて比較し以下の基準にて評価した。各実施例の結果を表1に示し、各比較例の結果は表2に示す。
1.表面状態等に変化がない
2.局所的に明確な着色やクラックの発生が認められる
3.全面的に着色やクラックの発生が認められる
なお、上記評価結果において、2以上の場合に実用上の問題はないと評価した。
実施例2〜16、及び比較例1〜8において用いた原料及び部数を表1及び表2に示す。表1及び表2に示した原料及び部数を採用した点以外は実施例1と同様にして放熱塗料を調製し、試験基材を作製した後、その塗膜について実施例1と同様にして放熱性を評価した。
※1…商品名「エポトートYD−014」、新日鐵住金化学(株)製、エポキシ当量950、軟化点97℃
※2…商品名「エポトートYD−012」、新日鐵住金化学(株)製、エポキシ当量650、軟化点80℃
※3…商品名「jER1002」、三菱化学(株)、エポキシ当量650、軟化点78℃
※4…商品名「エピクロンN−675」、DIC(株)製
※5…商品名「ファインディックM−8020」、DIC(株)製、水酸基価30、軟化点110℃
※6…商品名「ユピカコートGV−820」、日本ユピカ(株)製、水酸基価38、軟化点113℃
※7…商品名「ユピカコートGV−230」、日本ユピカ(株)製、酸価53、軟化点121℃
※8…商品名「jERキュア171N」、三菱化学(株)製
※9…商品名「ベスタゴンB−1530」、エボニック デグサ ジャパン製、εカプロラクタムでブロックされたイソホロンジイソシアネートの三量体
※10…商品名「キュアゾールC11Z」、四国化成工業(株)製2,4−ジアミノ−6−[2’−ウンデシルイミダゾリル−(1’)]−エチル−s−トリアジン
※11…商品名「サイシリア470」、富士シリシア化学(株)製、熱伝導率1.1W/m、平均一次粒子径14.1μm
※12…商品名「FLUORITE POWDER CALCIUM FLUORIDE」、China Tuhsu Flavours&Fragrances Import&Export Co. Lt製、熱伝導率9.7W/m、平均一次粒子径38.0μm
※13…商品名「TITONE R−32」、堺化学工業(株)製、熱伝導率21W/m、平均一次粒子径0.2μm
※14…商品名「SL−100」、竹原化学工業(株)製、平均一次粒子径6.0μm
※15…商品名「レジフローP−67」、ESTRON CHEMICAL社製
※16…商品名「BORONID S3」、ESK Ceramics社製、熱伝導率60W/m、平均一次粒子径約10μm
※17…商品名「PDM−8DF」、トピ−工業(株)社製、熱伝導率0.67W/m、平均一次粒子径約12μm
※18…商品名「FF−200・M40」、丸ス釉薬合資会社製、熱伝導率5W/m、平均一次粒子径約2.5μm
Claims (10)
- エポキシ樹脂(a1)と、水酸基及び/又はカルボキシル基を有するポリエステル樹脂(a2)とからなる群から選択される少なくとも1種のバインダー樹脂(A)を含みかつ、
熱伝導度が0.2W/mK以上100W/mK未満の放熱性フィラー(B)を10質量%以上40質量%以下と、を含有する、
放熱性粉体塗料組成物。 - 前記バインダー樹脂(A)の含有量が、30質量%以上85質量%以下である、
請求項1に記載の放熱性粉体塗料組成物。 - 前記(a1)成分が、ビスフェノール型エポキシ樹脂及び/又はノボラック型エポキシ樹脂である、
請求項1又は請求項2に記載の放熱性粉体塗料組成物。 - 前記(B)成分が、マイカ微粒子、フォルステライト微粒子、酸化ケイ素微粒子、フッ化金属結晶微粒子、及び窒化ホウ素微粒子からなる群から選択される少なくとも1種である、
請求項1乃至請求項3のいずれか1項に記載の放熱性粉体塗料組成物。 - 前記(B)成分の平均一次粒子径が、0.1μm以上50μm以下である、
請求項1乃至請求項4のいずれか1項に記載の放熱性粉体塗料組成物。 - さらに、着色顔料(C)を含有する、
請求項1乃至請求項5のいずれか1項に記載の放熱性粉体塗料組成物。 - 前記(C)成分が、酸化チタン粉末、カーボンブラック粉末、及び酸化鉄粉末からなる群から選択される少なくとも1種である、
請求項1乃至請求項6のいずれか1項に記載の放熱性粉体塗料組成物。 - 前記(C)成分の含有量が、0.5質量%以上30質量%以下である、
請求項1乃請求項7のいずれか1項に記載の放熱性粉体塗料組成物。 - 請求項1乃至請求項8のいずれか1項に記載の放熱性粉体塗料組成物から得られる、
放熱性塗膜。 - 請求項9に記載の放熱性塗膜によって覆われた
被塗装物。
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KR20190033876A (ko) * | 2017-09-22 | 2019-04-01 | 주식회사 엘지화학 | 필름의 제조 방법 |
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Also Published As
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WO2014136615A1 (ja) | 2014-09-12 |
TWI592474B (zh) | 2017-07-21 |
TW201446955A (zh) | 2014-12-16 |
JP6359841B2 (ja) | 2018-07-18 |
US20160024366A1 (en) | 2016-01-28 |
CN105073918A (zh) | 2015-11-18 |
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