JP2009286127A - 多層遮熱コーティング - Google Patents
多層遮熱コーティング Download PDFInfo
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- JP2009286127A JP2009286127A JP2009128586A JP2009128586A JP2009286127A JP 2009286127 A JP2009286127 A JP 2009286127A JP 2009128586 A JP2009128586 A JP 2009128586A JP 2009128586 A JP2009128586 A JP 2009128586A JP 2009286127 A JP2009286127 A JP 2009286127A
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- C23C28/04—Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D only coatings of inorganic non-metallic material
- C23C28/042—Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D only coatings of inorganic non-metallic material including a refractory ceramic layer, e.g. refractory metal oxides, ZrO2, rare earth oxides
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- C—CHEMISTRY; METALLURGY
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- C23C28/00—Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D
- C23C28/04—Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D only coatings of inorganic non-metallic material
- C23C28/048—Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D only coatings of inorganic non-metallic material with layers graded in composition or physical properties
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F01—MACHINES OR ENGINES IN GENERAL; ENGINE PLANTS IN GENERAL; STEAM ENGINES
- F01D—NON-POSITIVE DISPLACEMENT MACHINES OR ENGINES, e.g. STEAM TURBINES
- F01D5/00—Blades; Blade-carrying members; Heating, heat-insulating, cooling or antivibration means on the blades or the members
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- F01D5/28—Selecting particular materials; Particular measures relating thereto; Measures against erosion or corrosion
- F01D5/288—Protective coatings for blades
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F05—INDEXING SCHEMES RELATING TO ENGINES OR PUMPS IN VARIOUS SUBCLASSES OF CLASSES F01-F04
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- F05D2230/00—Manufacture
- F05D2230/90—Coating; Surface treatment
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F05—INDEXING SCHEMES RELATING TO ENGINES OR PUMPS IN VARIOUS SUBCLASSES OF CLASSES F01-F04
- F05D—INDEXING SCHEME FOR ASPECTS RELATING TO NON-POSITIVE-DISPLACEMENT MACHINES OR ENGINES, GAS-TURBINES OR JET-PROPULSION PLANTS
- F05D2300/00—Materials; Properties thereof
- F05D2300/60—Properties or characteristics given to material by treatment or manufacturing
- F05D2300/611—Coating
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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Abstract
【課題】
イットリアベースの遮熱コーティングおよびカルシア-アルミナ-マグネシアケイ酸塩 (CMAS) 攻撃からのそれらの保護の分野を提供する。
【解決手段】
表面上に遮熱コーティング(2-6)を有する部品(1)であって、遮熱コーティングは、化学的に安定化されたジルコニアを含む層 (3) を少なくとも1つ含み、そして化学的に安定化されたジルコニアを含む層 (3)に少なくとも間接的に隣接しおよびそれの表面に面する側に、カルシウムの酸化物を含有する環境汚染物質組成物と反応しておらずかつ化学的に安定化されたジルコニアを含む層(3)の材料と反応していない保護層(4)および/または浸透帯(5)が提供される部品(1)。そのような部品を製造する方法ならびに遮断塗料用保護層を被覆するための特定の系の、CMASを保護するための使用。
【選択図】 図1
Description
これらの検討から、本発明は、CMAS 攻撃を防ぐための解決策を提案する:
1) TBCの外層において、イットリア安定化されたジルコニアの代わりにカルシア安定化されたジルコニアを使用する
2) TBC上の上面上にCaSO4 層をデポジットさせてそれをCMAS 攻撃から保護する
3) TBCの外層において、SrZrO3、CaZrO3、Ca-ドープトSrZrO3、またはSr-ドープト CaZrO3を使用する。
超合金基材、APS (大気圧プラズマスプレー) かまたはHVOF(高速酸素燃料熱スプレー)のいずれかによってデポジットさせるボンドコート、プラズマスプレーによってデポジットさせるイットリア-安定化されたジルコニア遮熱コーティングおよび下記の方法の内の一つによってデポジットさせるCaSO4 環境障壁塗料:
1) スラリーコーティング
2) 熱スプレー
3) PVD (物理蒸着)
4) CVD (化学蒸着)
5) CaOをデポジットさせそしてSO2含有雰囲気中でそれを反応させる
可能な部品およびコーティング、CaZrO3、または被覆されるCa-安定化されたジルコニアの記述:
本発明に従う環境障壁塗料を被覆する可能な部分は、下記にすることができる: 燃焼室タイル; 羽根; 翼等。
実験の項:
遮熱コーティング層 (YSZ)上に硫酸カルシウム保護層を形成する上述した手順を使用して、標準のガスタービン部品YSZ遮熱コーティング層3に、硫酸カルシウム保護層4を被覆しそして次いで、試験条件を施した。
CMASは、かなりの量の CaO (CaSO4! ではない)を含有し、それの含有率は、35重量%までおよび更にそれ以上になることができる。CaOは、YSZの中に拡散することができ、そしてYSZ構造内の安定用元素の含有量を増大するに至り、YSZの相組成をキュービックジルコニアの方へ変更するに至る。直接CMASに接した使用前の試料において、キュービックジルコニア含有量の増大は、X 線回折によって観測され、TBCが、デポジットされたままのTBCにおけるのに比べて安定用元素を一層高い含有率で含有することをはっきりと示し、立ち代わって、TBC層における残留応力の増大ならびにTBC層の不安定化およびそれの破砕に至る。
2 ボンドコート層
3 遮熱コーティング層
4 硫酸カルシウム 層
5 浸透帯
6 追加の層
7 CMAS デポジット層
8 反応層
Claims (15)
- 表面上に遮熱コーティング(2-6)を有する部品(1)であって、遮熱コーティングは、化学的に安定化されたジルコニアを含む層 (3) を少なくとも1つ含み、そして化学的に安定化されたジルコニアを含む層 (3)に少なくとも間接的に隣接しおよびそれの表面に面する側に、カルシウムの酸化物を含有する環境汚染物質組成物と反応しておらずかつ化学的に安定化されたジルコニアを含む層(3)の材料と反応していない保護層(4)および/または浸透帯(5)が提供される部品(1)。
- 保護層 (4) が、下記: 硫酸カルシウム, カルシウム-ドープトSrZrO3、ストロンチウム-ドープトCaZrO3の群より選択されるカルシウム系を含む、請求項1記載の部品(1)。
- 保護層(4) が、本質的に硫酸カルシウムからなる、請求項1記載の部品(1)。
- 保護層(4) が、化学的に安定化されたジルコニアを含む層(3)に直接隣接する、請求項1〜3のいずれか一に記載の部品(1)。
- 化学的に安定化されたジルコニアを含む層 (3)が、下記: イットリア-安定化されたジルコニア、酸化スカンジウム-安定化されたジルコニア、およびカルシア-安定化されたジルコニアまたはこれらの組合せからなる群より選択される、請求項1〜4のいずれか一に記載の部品(1)。
- 化学的に安定化されたジルコニアを含む層 (3)が、本質的にイットリア-安定化されたジルコニアからなる、請求項1〜4のいずれか一に記載の部品(1)。
- 保護層(4)に面する化学的に安定化されたジルコニアを含む層(3)の側に、保護層(4)の材料が化学的に安定化されたジルコニアを含む層(3)の細孔に浸透する浸透帯(5)がある、請求項1〜6のいずれか一に記載の部品(1)。
- 浸透帯(5)が、10-100 マイクロメーターの範囲の厚さである、請求項7記載の部品(1)。
- 保護層(4) が、透過性でありおよび犠牲的でない、請求項1〜8のいずれか一に記載の部品(1)。
- 保護層(4)の表面に面する側に、部品の実際の最後の表面層を形成する、請求項1〜9のいずれか一に記載の部品(1)。
- 部品(1) が、圧縮/燃焼空気流に暴露される、下記: ハウジング/案内要素/燃焼室タイルまたはこれらの部分もしくは部品、翼またはこれの部分もしくは部品、羽根またはこれの部分もしくは部品の群より選択されるガスタービン部品である、請求項1〜10のいずれか一に記載の部品(1)。
- 化学的に安定化されたジルコニアを含む層(3)を少なくとも1つ備えた部品(1)に、下記: スラリーコーティング; 熱スプレーコーティング; 物理蒸着; 化学蒸着から選択するコーティングプロセスを使用してCaSO4またはCaSO4-2H2Oをデポジットさせ;そしてそれを炉内で10 Pa〜1000 PaのSO2、および 100 Pa〜25 kPaのO2を含有する管理された雰囲気と温度300°C〜800°Cの範囲で反応させることによって保護層(4)を被覆する、請求項1〜11のいずれか一に記載の部品(1) を製造する方法。
- 化学的に安定化されたジルコニアを含む層(3)を、超合金でできている部品(1)を、グリットブラストし、大気圧プラズマスプレーまたは高速酸素燃料熱スプレーによってボンドコートデポジットさせそして続いてジルコニア、イットリア-安定化されたジルコニア遮熱コートを、プラズマスプレーすることによってデポジットさせることで造る、請求項12記載の方法。
- カルシア安定化されたジルコニア, CaSO4, SrZrO3, CaZrO3, Ca-ドープト SrZrO3, Sr-ドープト CaZrO3の、部品の化学的に安定化されたジルコニアを含む遮熱コーティング(2)の外側帯 (5) におけるおよび/または化学的に安定化されたジルコニアを含む遮熱コーティング層(2)の中にカルシウムが拡散するのを防ぐための化学的に安定化されたジルコニアを含む遮熱コーティング(2)の保護層(4)としての使用。
- 硫酸カルシウムを、本質的にイットリア-安定化されたジルコニアからなる遮熱コーティング層(2)上だけで本質的に硫酸カルシウムからなる保護層(4)として使用する、請求項14記載の使用。
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EP08104164.2 | 2008-05-29 | ||
EP08104164 | 2008-05-29 |
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JP2009286127A true JP2009286127A (ja) | 2009-12-10 |
JP2009286127A5 JP2009286127A5 (ja) | 2014-01-16 |
JP5478942B2 JP5478942B2 (ja) | 2014-04-23 |
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US (1) | US8216689B2 (ja) |
EP (1) | EP2128299B1 (ja) |
JP (1) | JP5478942B2 (ja) |
CN (1) | CN101612823B (ja) |
Cited By (5)
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US8859052B2 (en) | 2008-12-19 | 2014-10-14 | General Electric Company | Methods for making environmental barrier coatings and ceramic components having CMAS mitigation capability |
JP2015501375A (ja) * | 2011-10-13 | 2015-01-15 | ゼネラル・エレクトリック・カンパニイ | 遮熱コーティング系およびそのための方法 |
US9023486B2 (en) | 2011-10-13 | 2015-05-05 | General Electric Company | Thermal barrier coating systems and processes therefor |
JP2018059465A (ja) * | 2016-10-06 | 2018-04-12 | 三菱重工業株式会社 | 遮熱コーティング膜、タービン部材及び遮熱コーティング方法 |
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US20090186237A1 (en) | 2008-01-18 | 2009-07-23 | Rolls-Royce Corp. | CMAS-Resistant Thermal Barrier Coatings |
US9394608B2 (en) | 2009-04-06 | 2016-07-19 | Asm America, Inc. | Semiconductor processing reactor and components thereof |
US8802201B2 (en) | 2009-08-14 | 2014-08-12 | Asm America, Inc. | Systems and methods for thin-film deposition of metal oxides using excited nitrogen-oxygen species |
JP5561733B2 (ja) * | 2010-12-28 | 2014-07-30 | 株式会社日立製作所 | 遮熱コーティングを有するガスタービン用部品と、それを用いたガスタービン |
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US9017481B1 (en) | 2011-10-28 | 2015-04-28 | Asm America, Inc. | Process feed management for semiconductor substrate processing |
US20130167552A1 (en) * | 2012-01-04 | 2013-07-04 | General Electric Company | Exhaust strut and turbomachine incorprating same |
US9347126B2 (en) | 2012-01-20 | 2016-05-24 | General Electric Company | Process of fabricating thermal barrier coatings |
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Also Published As
Publication number | Publication date |
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CN101612823A (zh) | 2009-12-30 |
US20090324989A1 (en) | 2009-12-31 |
US8216689B2 (en) | 2012-07-10 |
EP2128299B1 (en) | 2016-12-28 |
EP2128299A1 (en) | 2009-12-02 |
JP5478942B2 (ja) | 2014-04-23 |
CN101612823B (zh) | 2014-06-18 |
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