JP2008505220A

JP2008505220A - 熱可塑性ポリカーボネート組成物、その製造方法及び使用方法

熱可塑性ポリカーボネート組成物、その製造方法及び使用方法 Download PDF

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Publication number: JP2008505220A
Authority: JP; Japan
Prior art keywords: composition; polycarbonate; abs; impact modifier; acrylate
Prior art date: 2004-07-02
Legal status : Withdrawn

Application number

JP2007519387A

Other languages

English (en)

Japanese (ja)

Inventor

デルッダー，ジェームズ・エル

フォルカース，アンドリス・アドリアーン

Current Assignee

General Electric Co

Original Assignee

General Electric Co

Priority date

2004-07-02

Filing date

2005-06-30

Publication date

2008-02-21

2005-06-30 Application filed by General Electric Co filed Critical General Electric Co

2008-02-21 Publication of JP2008505220A publication Critical patent/JP2008505220A/ja

Status Withdrawn legal-status Critical Current

Links

239000000203 mixture Substances 0.000 title claims abstract description 173
229920000515 polycarbonate Polymers 0.000 title claims abstract description 143
239000004417 polycarbonate Substances 0.000 title claims abstract description 143
229920001169 thermoplastic Polymers 0.000 title claims abstract description 51
239000004416 thermosoftening plastic Substances 0.000 title claims abstract description 50
238000004519 manufacturing process Methods 0.000 title claims description 11
239000004609 Impact Modifier Substances 0.000 claims abstract description 88
239000013626 chemical specie Substances 0.000 claims abstract description 27
239000000178 monomer Substances 0.000 claims description 91
-1 alkyl phosphate Chemical compound 0.000 claims description 87
229920001577 copolymer Polymers 0.000 claims description 64
239000004676 acrylonitrile butadiene styrene Substances 0.000 claims description 63
229920000122 acrylonitrile butadiene styrene Polymers 0.000 claims description 62
125000003118 aryl group Chemical group 0.000 claims description 54
PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims description 47
NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 39
KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 claims description 37
238000000034 method Methods 0.000 claims description 37
229920001971 elastomer Polymers 0.000 claims description 36
239000000654 additive Substances 0.000 claims description 34
230000015556 catabolic process Effects 0.000 claims description 31
238000006731 degradation reaction Methods 0.000 claims description 31
125000000217 alkyl group Chemical group 0.000 claims description 20
239000000806 elastomer Substances 0.000 claims description 20
230000007062 hydrolysis Effects 0.000 claims description 20
238000006460 hydrolysis reaction Methods 0.000 claims description 20
230000032683 aging Effects 0.000 claims description 19
230000008859 change Effects 0.000 claims description 19
YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 claims description 18
239000000049 pigment Substances 0.000 claims description 18
NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 claims description 16
125000004435 hydrogen atom Chemical class [H]* 0.000 claims description 16
239000005060 rubber Substances 0.000 claims description 16
239000001257 hydrogen Substances 0.000 claims description 15
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230000008569 process Effects 0.000 claims description 15
125000001246 bromo group Chemical group Br* 0.000 claims description 14
125000001309 chloro group Chemical group Cl* 0.000 claims description 13
238000007720 emulsion polymerization reaction Methods 0.000 claims description 13
239000000945 filler Substances 0.000 claims description 13
230000000996 additive effect Effects 0.000 claims description 12
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125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 10
NAWXUBYGYWOOIX-SFHVURJKSA-N (2s)-2-[[4-[2-(2,4-diaminoquinazolin-6-yl)ethyl]benzoyl]amino]-4-methylidenepentanedioic acid Chemical compound C1=CC2=NC(N)=NC(N)=C2C=C1CCC1=CC=C(C(=O)N[C@@H](CC(=C)C(O)=O)C(O)=O)C=C1 NAWXUBYGYWOOIX-SFHVURJKSA-N 0.000 claims description 9
238000005227 gel permeation chromatography Methods 0.000 claims description 9
239000000155 melt Substances 0.000 claims description 9
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125000003710 aryl alkyl group Chemical group 0.000 claims description 7
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239000004094 surface-active agent Substances 0.000 claims description 7
NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 6
GYCMBHHDWRMZGG-UHFFFAOYSA-N Methylacrylonitrile Chemical compound CC(=C)C#N GYCMBHHDWRMZGG-UHFFFAOYSA-N 0.000 claims description 6
239000004793 Polystyrene Substances 0.000 claims description 6
125000004104 aryloxy group Chemical group 0.000 claims description 6
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238000012360 testing method Methods 0.000 claims description 6
TVONJMOVBKMLOM-UHFFFAOYSA-N 2-methylidenebutanenitrile Chemical compound CCC(=C)C#N TVONJMOVBKMLOM-UHFFFAOYSA-N 0.000 claims description 5
239000005062 Polybutadiene Substances 0.000 claims description 5
125000000753 cycloalkyl group Chemical group 0.000 claims description 5
125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 claims description 5
238000002156 mixing Methods 0.000 claims description 5
239000010452 phosphate Substances 0.000 claims description 5
229920002857 polybutadiene Polymers 0.000 claims description 5
CYLVUSZHVURAOY-UHFFFAOYSA-N 2,2-dibromoethenylbenzene Chemical compound BrC(Br)=CC1=CC=CC=C1 CYLVUSZHVURAOY-UHFFFAOYSA-N 0.000 claims description 4
CMPIGRYBIGUGTH-UHFFFAOYSA-N 2-bromoprop-2-enenitrile Chemical compound BrC(=C)C#N CMPIGRYBIGUGTH-UHFFFAOYSA-N 0.000 claims description 4
OYUNTGBISCIYPW-UHFFFAOYSA-N 2-chloroprop-2-enenitrile Chemical compound ClC(=C)C#N OYUNTGBISCIYPW-UHFFFAOYSA-N 0.000 claims description 4
DKFAYHWIVQDPCC-UHFFFAOYSA-N 3-chloroprop-2-enenitrile Chemical compound ClC=CC#N DKFAYHWIVQDPCC-UHFFFAOYSA-N 0.000 claims description 4
125000004453 alkoxycarbonyl group Chemical group 0.000 claims description 4
150000008052 alkyl sulfonates Chemical class 0.000 claims description 4
125000000000 cycloalkoxy group Chemical group 0.000 claims description 4
238000001125 extrusion Methods 0.000 claims description 4
125000004123 n-propyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])* 0.000 claims description 4
238000007493 shaping process Methods 0.000 claims description 4
SNOOUWRIMMFWNE-UHFFFAOYSA-M sodium;6-[(3,4,5-trimethoxybenzoyl)amino]hexanoate Chemical compound [Na+].COC1=CC(C(=O)NCCCCCC([O-])=O)=CC(OC)=C1OC SNOOUWRIMMFWNE-UHFFFAOYSA-M 0.000 claims description 4
SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 3
229920002943 EPDM rubber Polymers 0.000 claims description 3
125000005161 aryl oxy carbonyl group Chemical group 0.000 claims description 3
238000000576 coating method Methods 0.000 claims description 3
238000007334 copolymerization reaction Methods 0.000 claims description 3
125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims description 3
ORTFAQDWJHRMNX-UHFFFAOYSA-N hydroxidooxidocarbon(.) Chemical group O[C]=O ORTFAQDWJHRMNX-UHFFFAOYSA-N 0.000 claims description 3
238000000465 moulding Methods 0.000 claims description 3
150000004760 silicates Chemical class 0.000 claims description 3
125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 claims description 3
125000004642 (C1-C12) alkoxy group Chemical group 0.000 claims description 2
WAEOXIOXMKNFLQ-UHFFFAOYSA-N 1-methyl-4-prop-2-enylbenzene Chemical group CC1=CC=C(CC=C)C=C1 WAEOXIOXMKNFLQ-UHFFFAOYSA-N 0.000 claims description 2
CTHJQRHPNQEPAB-UHFFFAOYSA-N 2-methoxyethenylbenzene Chemical compound COC=CC1=CC=CC=C1 CTHJQRHPNQEPAB-UHFFFAOYSA-N 0.000 claims description 2
150000008055 alkyl aryl sulfonates Chemical class 0.000 claims description 2
150000008051 alkyl sulfates Chemical class 0.000 claims description 2
238000006388 chemical passivation reaction Methods 0.000 claims description 2
239000011248 coating agent Substances 0.000 claims description 2
239000003086 colorant Substances 0.000 claims description 2
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KETWBQOXTBGBBN-UHFFFAOYSA-N hex-1-enylbenzene Chemical compound CCCCC=CC1=CC=CC=C1 KETWBQOXTBGBBN-UHFFFAOYSA-N 0.000 claims description 2
229920012128 methyl methacrylate acrylonitrile butadiene styrene Polymers 0.000 claims description 2
229920001200 poly(ethylene-vinyl acetate) Polymers 0.000 claims description 2
HJWLCRVIBGQPNF-UHFFFAOYSA-N prop-2-enylbenzene Chemical compound C=CCC1=CC=CC=C1 HJWLCRVIBGQPNF-UHFFFAOYSA-N 0.000 claims description 2
239000012779 reinforcing material Substances 0.000 claims description 2
229920000181 Ethylene propylene rubber Polymers 0.000 claims 1
125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims 1
229920003049 isoprene rubber Polymers 0.000 claims 1
FUGYGGDSWSUORM-UHFFFAOYSA-N para-hydroxystyrene Natural products OC1=CC=C(C=C)C=C1 FUGYGGDSWSUORM-UHFFFAOYSA-N 0.000 claims 1
150000003440 styrenes Chemical class 0.000 claims 1
125000003011 styrenyl group Chemical group [H]\C(*)=C(/[H])C1=C([H])C([H])=C([H])C([H])=C1[H] 0.000 claims 1
230000003301 hydrolyzing effect Effects 0.000 abstract description 14
XECAHXYUAAWDEL-UHFFFAOYSA-N acrylonitrile butadiene styrene Chemical compound C=CC=C.C=CC#N.C=CC1=CC=CC=C1 XECAHXYUAAWDEL-UHFFFAOYSA-N 0.000 description 42
239000012071 phase Substances 0.000 description 41
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IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical class C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 21
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238000006116 polymerization reaction Methods 0.000 description 10
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125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 5
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MZHULIWXRDLGRR-UHFFFAOYSA-N tridecyl 3-(3-oxo-3-tridecoxypropyl)sulfanylpropanoate Chemical compound CCCCCCCCCCCCCOC(=O)CCSCCC(=O)OCCCCCCCCCCCCC MZHULIWXRDLGRR-UHFFFAOYSA-N 0.000 description 1
150000004684 trihydrates Chemical class 0.000 description 1
SRPWOOOHEPICQU-UHFFFAOYSA-N trimellitic anhydride Chemical compound OC(=O)C1=CC=C2C(=O)OC(=O)C2=C1 SRPWOOOHEPICQU-UHFFFAOYSA-N 0.000 description 1
NJMOHBDCGXJLNJ-UHFFFAOYSA-N trimellitic anhydride chloride Chemical compound ClC(=O)C1=CC=C2C(=O)OC(=O)C2=C1 NJMOHBDCGXJLNJ-UHFFFAOYSA-N 0.000 description 1
OOZBTDPWFHJVEK-UHFFFAOYSA-N tris(2-nonylphenyl) phosphate Chemical compound CCCCCCCCCC1=CC=CC=C1OP(=O)(OC=1C(=CC=CC=1)CCCCCCCCC)OC1=CC=CC=C1CCCCCCCCC OOZBTDPWFHJVEK-UHFFFAOYSA-N 0.000 description 1
PLCFYBDYBCOLSP-UHFFFAOYSA-N tris(prop-2-enyl) 2-hydroxypropane-1,2,3-tricarboxylate Chemical compound C=CCOC(=O)CC(O)(CC(=O)OCC=C)C(=O)OCC=C PLCFYBDYBCOLSP-UHFFFAOYSA-N 0.000 description 1
235000013799 ultramarine blue Nutrition 0.000 description 1
229920006032 ungrafted co-polymer Polymers 0.000 description 1
238000009849 vacuum degassing Methods 0.000 description 1
229920002554 vinyl polymer Polymers 0.000 description 1
239000001993 wax Substances 0.000 description 1
239000000080 wetting agent Substances 0.000 description 1
239000001018 xanthene dye Substances 0.000 description 1
125000005023 xylyl group Chemical group 0.000 description 1
229910052725 zinc Inorganic materials 0.000 description 1
239000011701 zinc Substances 0.000 description 1
WGEATSXPYVGFCC-UHFFFAOYSA-N zinc ferrite Chemical compound O=[Zn].O=[Fe]O[Fe]=O WGEATSXPYVGFCC-UHFFFAOYSA-N 0.000 description 1
GFQYVLUOOAAOGM-UHFFFAOYSA-N zirconium(iv) silicate Chemical compound [Zr+4].[O-][Si]([O-])([O-])[O-] GFQYVLUOOAAOGM-UHFFFAOYSA-N 0.000 description 1