JP2002513045A - カプセル化された活性物質 - Google Patents
カプセル化された活性物質Info
- Publication number
- JP2002513045A JP2002513045A JP2000545641A JP2000545641A JP2002513045A JP 2002513045 A JP2002513045 A JP 2002513045A JP 2000545641 A JP2000545641 A JP 2000545641A JP 2000545641 A JP2000545641 A JP 2000545641A JP 2002513045 A JP2002513045 A JP 2002513045A
- Authority
- JP
- Japan
- Prior art keywords
- active agent
- particles
- polymer
- encapsulated
- activator
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
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- 239000002245 particle Substances 0.000 claims abstract description 135
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- 238000002844 melting Methods 0.000 claims description 11
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- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 description 3
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- GYCMBHHDWRMZGG-UHFFFAOYSA-N Methylacrylonitrile Chemical compound CC(=C)C#N GYCMBHHDWRMZGG-UHFFFAOYSA-N 0.000 description 1
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- 239000013504 Triton X-100 Substances 0.000 description 1
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- GPDWNEFHGANACG-UHFFFAOYSA-L [dibutyl(2-ethylhexanoyloxy)stannyl] 2-ethylhexanoate Chemical compound CCCCC(CC)C(=O)O[Sn](CCCC)(CCCC)OC(=O)C(CC)CCCC GPDWNEFHGANACG-UHFFFAOYSA-L 0.000 description 1
- YRKCREAYFQTBPV-UHFFFAOYSA-N acetylacetone Chemical compound CC(=O)CC(C)=O YRKCREAYFQTBPV-UHFFFAOYSA-N 0.000 description 1
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- 125000001931 aliphatic group Chemical group 0.000 description 1
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- 125000005192 alkyl ethylene group Chemical group 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
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- 125000003118 aryl group Chemical group 0.000 description 1
- 239000012867 bioactive agent Substances 0.000 description 1
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- YHWCPXVTRSHPNY-UHFFFAOYSA-N butan-1-olate;titanium(4+) Chemical compound [Ti+4].CCCC[O-].CCCC[O-].CCCC[O-].CCCC[O-] YHWCPXVTRSHPNY-UHFFFAOYSA-N 0.000 description 1
- CQEYYJKEWSMYFG-UHFFFAOYSA-N butyl acrylate Chemical compound CCCCOC(=O)C=C CQEYYJKEWSMYFG-UHFFFAOYSA-N 0.000 description 1
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- 238000012937 correction Methods 0.000 description 1
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- AYOHIQLKSOJJQH-UHFFFAOYSA-N dibutyltin Chemical compound CCCC[Sn]CCCC AYOHIQLKSOJJQH-UHFFFAOYSA-N 0.000 description 1
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- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 125000003187 heptyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 230000002363 herbicidal effect Effects 0.000 description 1
- RRAMGCGOFNQTLD-UHFFFAOYSA-N hexamethylene diisocyanate Chemical compound O=C=NCCCCCCN=C=O RRAMGCGOFNQTLD-UHFFFAOYSA-N 0.000 description 1
- 125000004051 hexyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
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- 125000002768 hydroxyalkyl group Chemical group 0.000 description 1
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- 125000001905 inorganic group Chemical group 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 150000002513 isocyanates Chemical class 0.000 description 1
- 125000004491 isohexyl group Chemical group C(CCC(C)C)* 0.000 description 1
- 239000011133 lead Substances 0.000 description 1
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- 238000011068 loading method Methods 0.000 description 1
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- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- LVHBHZANLOWSRM-UHFFFAOYSA-N methylenebutanedioic acid Natural products OC(=O)CC(=C)C(O)=O LVHBHZANLOWSRM-UHFFFAOYSA-N 0.000 description 1
- 238000013008 moisture curing Methods 0.000 description 1
- BMLIZLVNXIYGCK-UHFFFAOYSA-N monuron Chemical compound CN(C)C(=O)NC1=CC=C(Cl)C=C1 BMLIZLVNXIYGCK-UHFFFAOYSA-N 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- QOHMWDJIBGVPIF-UHFFFAOYSA-N n',n'-diethylpropane-1,3-diamine Chemical compound CCN(CC)CCCN QOHMWDJIBGVPIF-UHFFFAOYSA-N 0.000 description 1
- TXXWBTOATXBWDR-UHFFFAOYSA-N n,n,n',n'-tetramethylhexane-1,6-diamine Chemical compound CN(C)CCCCCCN(C)C TXXWBTOATXBWDR-UHFFFAOYSA-N 0.000 description 1
- 125000005609 naphthenate group Chemical group 0.000 description 1
- IOQPZZOEVPZRBK-UHFFFAOYSA-N octan-1-amine Chemical compound CCCCCCCCN IOQPZZOEVPZRBK-UHFFFAOYSA-N 0.000 description 1
- UKODFQOELJFMII-UHFFFAOYSA-N pentamethyldiethylenetriamine Chemical compound CN(C)CCN(C)CCN(C)C UKODFQOELJFMII-UHFFFAOYSA-N 0.000 description 1
- 125000001147 pentyl group Chemical group C(CCCC)* 0.000 description 1
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- XNGIFLGASWRNHJ-UHFFFAOYSA-L phthalate(2-) Chemical compound [O-]C(=O)C1=CC=CC=C1C([O-])=O XNGIFLGASWRNHJ-UHFFFAOYSA-L 0.000 description 1
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- 239000000843 powder Substances 0.000 description 1
- 150000003141 primary amines Chemical class 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- SCUZVMOVTVSBLE-UHFFFAOYSA-N prop-2-enenitrile;styrene Chemical compound C=CC#N.C=CC1=CC=CC=C1 SCUZVMOVTVSBLE-UHFFFAOYSA-N 0.000 description 1
- HKJYVRJHDIPMQB-UHFFFAOYSA-N propan-1-olate;titanium(4+) Chemical compound CCCO[Ti](OCCC)(OCCC)OCCC HKJYVRJHDIPMQB-UHFFFAOYSA-N 0.000 description 1
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- ADRDEXBBJTUCND-UHFFFAOYSA-N pyrrolizidine Chemical compound C1CCN2CCCC21 ADRDEXBBJTUCND-UHFFFAOYSA-N 0.000 description 1
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- RWSOTUBLDIXVET-UHFFFAOYSA-O sulfonium Chemical compound [SH3+] RWSOTUBLDIXVET-UHFFFAOYSA-O 0.000 description 1
- ISXSCDLOGDJUNJ-UHFFFAOYSA-N tert-butyl prop-2-enoate Chemical compound CC(C)(C)OC(=O)C=C ISXSCDLOGDJUNJ-UHFFFAOYSA-N 0.000 description 1
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- 229920005992 thermoplastic resin Polymers 0.000 description 1
- 150000003606 tin compounds Chemical class 0.000 description 1
- IUTCEZPPWBHGIX-UHFFFAOYSA-N tin(2+) Chemical class [Sn+2] IUTCEZPPWBHGIX-UHFFFAOYSA-N 0.000 description 1
- KSBAEPSJVUENNK-UHFFFAOYSA-L tin(ii) 2-ethylhexanoate Chemical compound [Sn+2].CCCCC(CC)C([O-])=O.CCCCC(CC)C([O-])=O KSBAEPSJVUENNK-UHFFFAOYSA-L 0.000 description 1
- YJGJRYWNNHUESM-UHFFFAOYSA-J triacetyloxystannyl acetate Chemical compound [Sn+4].CC([O-])=O.CC([O-])=O.CC([O-])=O.CC([O-])=O YJGJRYWNNHUESM-UHFFFAOYSA-J 0.000 description 1
- IMFACGCPASFAPR-UHFFFAOYSA-N tributylamine Chemical compound CCCCN(CCCC)CCCC IMFACGCPASFAPR-UHFFFAOYSA-N 0.000 description 1
- 239000012498 ultrapure water Substances 0.000 description 1
- 238000002604 ultrasonography Methods 0.000 description 1
- 150000003672 ureas Chemical class 0.000 description 1
- 229910052720 vanadium Inorganic materials 0.000 description 1
- GPPXJZIENCGNKB-UHFFFAOYSA-N vanadium Chemical compound [V]#[V] GPPXJZIENCGNKB-UHFFFAOYSA-N 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
- 229910052845 zircon Inorganic materials 0.000 description 1
- GFQYVLUOOAAOGM-UHFFFAOYSA-N zirconium(iv) silicate Chemical compound [Zr+4].[O-][Si]([O-])([O-])[O-] GFQYVLUOOAAOGM-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
- B01J13/04—Making microcapsules or microballoons by physical processes, e.g. drying, spraying
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
- B01J13/20—After-treatment of capsule walls, e.g. hardening
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
- B01J13/20—After-treatment of capsule walls, e.g. hardening
- B01J13/206—Hardening; drying
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
- Y10T428/2984—Microcapsule with fluid core [includes liposome]
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
- Y10T428/2984—Microcapsule with fluid core [includes liposome]
- Y10T428/2985—Solid-walled microcapsule from synthetic polymer
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
- Y10T428/2984—Microcapsule with fluid core [includes liposome]
- Y10T428/2985—Solid-walled microcapsule from synthetic polymer
- Y10T428/2987—Addition polymer from unsaturated monomers only
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
- Y10T428/2989—Microcapsule with solid core [includes liposome]
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Manufacturing Of Micro-Capsules (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Medicinal Preparation (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Catalysts (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US8312798P | 1998-04-27 | 1998-04-27 | |
| US60/083,127 | 1998-04-27 | ||
| PCT/US1999/009105 WO1999055454A1 (en) | 1998-04-27 | 1999-04-27 | Encapsulated active materials |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2010262560A Division JP5351131B2 (ja) | 1998-04-27 | 2010-11-25 | カプセル化された活性物質を含む粒子とその製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2002513045A true JP2002513045A (ja) | 2002-05-08 |
| JP2002513045A5 JP2002513045A5 (enExample) | 2006-05-25 |
Family
ID=22176365
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2000545641A Withdrawn JP2002513045A (ja) | 1998-04-27 | 1999-04-27 | カプセル化された活性物質 |
| JP2010262560A Expired - Fee Related JP5351131B2 (ja) | 1998-04-27 | 2010-11-25 | カプセル化された活性物質を含む粒子とその製造方法 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2010262560A Expired - Fee Related JP5351131B2 (ja) | 1998-04-27 | 2010-11-25 | カプセル化された活性物質を含む粒子とその製造方法 |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US6224793B1 (enExample) |
| EP (1) | EP1077763B1 (enExample) |
| JP (2) | JP2002513045A (enExample) |
| KR (1) | KR100577629B1 (enExample) |
| CN (1) | CN1207090C (enExample) |
| AT (1) | ATE259257T1 (enExample) |
| AU (1) | AU3666799A (enExample) |
| BR (1) | BR9910337B1 (enExample) |
| CA (1) | CA2330472C (enExample) |
| DE (1) | DE69914739T2 (enExample) |
| ES (1) | ES2212552T3 (enExample) |
| WO (1) | WO1999055454A1 (enExample) |
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2000044636A (ja) * | 1998-05-27 | 2000-02-15 | Hitachi Chem Co Ltd | 熱硬化性樹脂組成物及びこれを用いたコイルの製造法 |
| JP2000273323A (ja) * | 1999-03-24 | 2000-10-03 | Hitachi Chem Co Ltd | 硬化剤組成物、熱硬化性樹脂組成物、これを用いた管ライニング材及び管ライニング工法 |
| JP2001200021A (ja) * | 2000-01-19 | 2001-07-24 | Hitachi Chem Co Ltd | 樹脂組成物 |
| WO2006109747A1 (ja) * | 2005-04-07 | 2006-10-19 | Mitsui Chemicals, Inc. | オレフィン系重合体からなるカプセル状の微粒子 |
| JP2007063405A (ja) * | 2005-08-31 | 2007-03-15 | Casio Electronics Co Ltd | 超音波破壊用マイクロカプセル及びその製造方法 |
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- 1999-04-27 KR KR1020007011990A patent/KR100577629B1/ko not_active Expired - Fee Related
- 1999-04-27 CN CNB998055018A patent/CN1207090C/zh not_active Expired - Fee Related
- 1999-04-27 JP JP2000545641A patent/JP2002513045A/ja not_active Withdrawn
- 1999-04-27 WO PCT/US1999/009105 patent/WO1999055454A1/en not_active Ceased
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| JP2000044636A (ja) * | 1998-05-27 | 2000-02-15 | Hitachi Chem Co Ltd | 熱硬化性樹脂組成物及びこれを用いたコイルの製造法 |
| JP2000273323A (ja) * | 1999-03-24 | 2000-10-03 | Hitachi Chem Co Ltd | 硬化剤組成物、熱硬化性樹脂組成物、これを用いた管ライニング材及び管ライニング工法 |
| JP2001200021A (ja) * | 2000-01-19 | 2001-07-24 | Hitachi Chem Co Ltd | 樹脂組成物 |
| JP2008511736A (ja) * | 2004-09-01 | 2008-04-17 | アップルトン ペーパーズ インコーポレイテッド | カプセル化された硬化系 |
| WO2006109747A1 (ja) * | 2005-04-07 | 2006-10-19 | Mitsui Chemicals, Inc. | オレフィン系重合体からなるカプセル状の微粒子 |
| KR100973381B1 (ko) | 2005-04-07 | 2010-08-02 | 미쓰이 가가쿠 가부시키가이샤 | 올레핀계 중합체로 이루어지는 캡슐형상의 미립자 |
| US8349451B2 (en) | 2005-04-07 | 2013-01-08 | Mitsui Chemicals, Inc. | Capsular fine particle comprising olefinic polymer |
| JP5252915B2 (ja) * | 2005-04-07 | 2013-07-31 | 三井化学株式会社 | オレフィン系重合体からなるカプセル状の微粒子 |
| JP2007063405A (ja) * | 2005-08-31 | 2007-03-15 | Casio Electronics Co Ltd | 超音波破壊用マイクロカプセル及びその製造方法 |
| JP2010511713A (ja) * | 2006-12-05 | 2010-04-15 | ランデック コーポレイション | 薬物送達 |
| JP2015507050A (ja) * | 2012-02-02 | 2015-03-05 | アーケマ・インコーポレイテッド | 活性成分のカプセル化による、ハロゲン化オレフィンを含むポリオールブレンド物の改良された貯蔵寿命 |
| JP2014024986A (ja) * | 2012-07-27 | 2014-02-06 | Dow Corning Toray Co Ltd | 微粒子及びそれを含む硬化性オルガノポリシロキサン組成物 |
| JP2014141552A (ja) * | 2013-01-22 | 2014-08-07 | Sumitomo Bakelite Co Ltd | 樹脂組成物、注入剤および充填方法 |
| JP2020509930A (ja) * | 2017-03-09 | 2020-04-02 | コンストラクション リサーチ アンド テクノロジー ゲーエムベーハーＣｏｎｓｔｒｕｃｔｉｏｎ Ｒｅｓｅａｒｃｈ ＆ Ｔｅｃｈｎｏｌｏｇｙ ＧｍｂＨ | マイクロカプセル化された重付加触媒 |
| JP2023071777A (ja) * | 2017-03-09 | 2023-05-23 | コンストラクション リサーチ アンド テクノロジー ゲーエムベーハー | マイクロカプセル化された重付加触媒 |
| JP7587613B2 (ja) | 2017-03-09 | 2024-11-20 | シーカ テクノロジー アクチェンゲゼルシャフト | マイクロカプセル化された重付加触媒 |
| JP2020059836A (ja) * | 2018-03-29 | 2020-04-16 | 東ソー株式会社 | 触媒内包ポリビニル樹脂微粒子、該微粒子組成物、触媒内包ポリビニル樹脂微粒子及び該微粒子組成物の製造方法 |
| JP7318250B2 (ja) | 2018-03-29 | 2023-08-01 | 東ソー株式会社 | 触媒内包ポリビニル樹脂微粒子、該微粒子組成物、触媒内包ポリビニル樹脂微粒子及び該微粒子組成物の製造方法 |
| JP2021194565A (ja) * | 2020-06-10 | 2021-12-27 | 東ソー株式会社 | 脂質微粒子 |
| JP7501130B2 (ja) | 2020-06-10 | 2024-06-18 | 東ソー株式会社 | 脂質微粒子 |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1207090C (zh) | 2005-06-22 |
| CA2330472A1 (en) | 1999-11-04 |
| CA2330472C (en) | 2007-09-04 |
| DE69914739D1 (de) | 2004-03-18 |
| ATE259257T1 (de) | 2004-02-15 |
| JP5351131B2 (ja) | 2013-11-27 |
| ES2212552T3 (es) | 2004-07-16 |
| EP1077763A1 (en) | 2001-02-28 |
| WO1999055454A1 (en) | 1999-11-04 |
| DE69914739T2 (de) | 2004-09-30 |
| BR9910337B1 (pt) | 2010-08-24 |
| KR20010043104A (ko) | 2001-05-25 |
| AU3666799A (en) | 1999-11-16 |
| KR100577629B1 (ko) | 2006-05-10 |
| EP1077763B1 (en) | 2004-02-11 |
| CN1298321A (zh) | 2001-06-06 |
| US6224793B1 (en) | 2001-05-01 |
| JP2011072999A (ja) | 2011-04-14 |
| BR9910337A (pt) | 2001-01-09 |
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