HUP0203206A2 - Eljárás 4-trifluormetilszulfinilpirazol-származékok előállítására - Google Patents

Eljárás 4-trifluormetilszulfinilpirazol-származékok előállítására

Info

Publication number
HUP0203206A2
HUP0203206A2 HU0203206A HUP0203206A HUP0203206A2 HU P0203206 A2 HUP0203206 A2 HU P0203206A2 HU 0203206 A HU0203206 A HU 0203206A HU P0203206 A HUP0203206 A HU P0203206A HU P0203206 A2 HUP0203206 A2 HU P0203206A2
Authority
HU
Hungary
Prior art keywords
trifluoromethylsulphinylpyrazole
derivative
preparing
compound
general formula
Prior art date
Application number
HU0203206A
Other languages
English (en)
Inventor
Sylvie Bars
Philippe Charreau
Jean-Louis Clavel
Isabelle Pelta
Original Assignee
Aventis Cropscience S.A.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=8167491&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=HUP0203206(A2) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Aventis Cropscience S.A. filed Critical Aventis Cropscience S.A.
Publication of HUP0203206A2 publication Critical patent/HUP0203206A2/hu
Publication of HUP0203206A3 publication Critical patent/HUP0203206A3/hu
Publication of HU229393B1 publication Critical patent/HU229393B1/hu

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D401/00—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
    • C07D401/02—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings
    • C07D401/04—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings directly linked by a ring-member-to-ring-member bond
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/44—Oxygen and nitrogen or sulfur and nitrogen atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

A találmány (I) általános képletű vegyület - a képletben W jelentésenitrogénatom vagy -CR3; R1 jelentése halogénatom, halogénalkilcsoport,halogénalkoxicsoport, R4S(O)n- vagy -SF5; R2 jelentése hidrogénatomvagy halogénatom; R3 jelentése halogénatom; R4 jelentése alkilcsoportvagy halogénalkilcsoport; és n értéke 0, 1 vagy 2 - előállításáravonatkozik, oly módon, hogy egy (II) általános képletű vegyületet -ahol R1, R2 és W jelentése a fent megadott - trifluorperecetsavvaloxidálnak korróziógátló vegyület jelenlétében. Ó
HU0203206A 1999-10-22 1999-10-22 Process for preparing 4-trifluoromethylsulphinylpyrazole derivatives HU229393B1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/EP1999/008687 WO2001030760A1 (en) 1999-10-22 1999-10-22 Process for preparing 4-trifluoromethylsulphinylpyrazole derivative

Publications (3)

Publication Number Publication Date
HUP0203206A2 true HUP0203206A2 (hu) 2003-03-28
HUP0203206A3 HUP0203206A3 (en) 2005-11-28
HU229393B1 HU229393B1 (en) 2013-11-28

Family

ID=8167491

Family Applications (1)

Application Number Title Priority Date Filing Date
HU0203206A HU229393B1 (en) 1999-10-22 1999-10-22 Process for preparing 4-trifluoromethylsulphinylpyrazole derivatives

Country Status (30)

Country Link
US (2) US6620943B1 (hu)
EP (1) EP1222173B1 (hu)
JP (1) JP4666863B2 (hu)
KR (2) KR100665598B1 (hu)
CN (3) CN1896066B (hu)
AT (1) ATE273961T1 (hu)
AU (1) AU783139B2 (hu)
BG (1) BG65483B1 (hu)
BR (1) BR9917518B1 (hu)
CA (1) CA2384283C (hu)
CZ (1) CZ299822B6 (hu)
DE (1) DE69919599T2 (hu)
DK (1) DK1222173T3 (hu)
EA (1) EA005077B1 (hu)
ES (1) ES2222743T3 (hu)
HR (1) HRP20020438B1 (hu)
HU (1) HU229393B1 (hu)
IL (2) IL149152A0 (hu)
IN (2) IN2005MU00818A (hu)
ME (1) MEP7808A (hu)
MX (1) MX229662B (hu)
NZ (2) NZ517770A (hu)
PL (1) PL206482B1 (hu)
PT (1) PT1222173E (hu)
RO (1) RO121209B1 (hu)
TR (2) TR200202806T2 (hu)
TW (1) TW553936B (hu)
UA (1) UA73752C2 (hu)
WO (1) WO2001030760A1 (hu)
ZA (1) ZA200201961B (hu)

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CA2377236C (en) 1999-06-29 2010-08-17 Mitsubishi Chemical Corporation Pyrazole derivative, production process thereof, and pest control agent containing the same as active ingredient
WO2005023774A1 (en) * 2003-09-11 2005-03-17 Cheminova A/S Process for the preparation of a trifluoromethylthioether
CN100586934C (zh) * 2003-11-07 2010-02-03 凯米诺瓦有限公司 制备三氟甲基硫醚的方法
DE102004020069C5 (de) 2004-04-24 2013-12-05 Voith Patent Gmbh Verfahren zum Satinieren einer Papierbahn
CA2630849C (en) 2005-12-14 2013-05-14 Makhteshim Chemical Works Ltd. Polymorphs and amorphous forms of 5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-4-[(trifluoromethyl)sulfinyl]-1h-pyrazole-3-carbonitrile
AU2013203232B2 (en) * 2005-12-14 2015-08-27 Makhteshim Chemical Works Ltd Polymorphs and amorphous forms of 5-amino-1-[2,6- dichloro-4-(trifluoromethyl)phenyl]-4- [(trifluoromethyl)sulfinyl]-1H-pyrazole-3-carbonitrile
NZ568025A (en) 2006-04-25 2011-02-25 Gharda Chemicals Ltd Process for the preparation of fipronil, an insecticide, and related pyrazoles
CN101168529B (zh) * 2006-10-24 2011-03-23 温州大学 氟虫腈、乙虫腈及其衍生物的合成方法
CN101562980B (zh) * 2006-11-10 2014-04-16 巴斯夫欧洲公司 锐劲特的晶型
NZ576593A (en) 2006-11-10 2011-12-22 Basf Se Process for the sulfinylation of a pyrazole derivative
AU2007316639B2 (en) 2006-11-10 2012-12-20 Basf Se Crystalline modification of fipronil
UA110598C2 (uk) * 2006-11-10 2016-01-25 Басф Се Спосіб одержання кристалічної модифікації фіпронілу
EP2083628A1 (en) 2006-11-10 2009-08-05 Basf Se Crystalline modification of fipronil
ES2422296T3 (es) 2006-11-10 2013-09-10 Basf Se Proceso para la sulfinilación de un derivado pirazol
CN101250158B (zh) * 2008-04-02 2011-12-07 湖南化工研究院 一种氟虫腈的制备方法
AU2009299905B2 (en) 2008-10-02 2013-10-10 Boehringer Ingelheim Animal Health USA Inc. Method for producing and purifying trifluoromethanesulfinic acid
WO2010049746A1 (en) * 2008-10-27 2010-05-06 Dynamit Nobel Gmbh Explosivstoff-Und Systemtechnic Process for the synthesis of fipronil
EP2493860B1 (en) 2009-10-30 2014-01-15 Basf Se Process for the preparation of 4-sulfinyl-pyrazole derivatives
AU2010100462A4 (en) 2010-03-03 2010-06-17 Keki Hormusji Gharda A process for the synthesis of Fipronil
IT1400666B1 (it) * 2010-07-07 2013-06-28 Finchimica Srl Procedimento per la sintesi di 5-amino, 1-fenil, 3-ciano, 4-trifluorometil sulfinil pirazoli.
EP2593436A1 (en) 2010-07-12 2013-05-22 Irvita Plant Protection, A Branch of Celsius Property B.V. Fipronil production process
US9198421B2 (en) * 2011-01-14 2015-12-01 Keki Hormusji Gharda Polymorphism in 5-amino-1-(2,6-dichloro-4-trifluoromethylphenyl)-3-cyano-4-trifluoro methyl sulfinyl pyrazole
WO2012164571A1 (en) 2011-05-30 2012-12-06 Keki Hormusji Gharda Process for synthesis of fipronil
CN102633722B (zh) * 2012-03-20 2015-05-06 金坛市凌云动物保健品有限公司 一种非泼罗尼的制备方法
TWI579274B (zh) * 2012-04-20 2017-04-21 龍馬躍公司 製備１－芳基－５－烷基吡唑化合物的改良方法
CN102690232A (zh) * 2012-05-30 2012-09-26 河南中医学院 一种氟虫腈中间体的合成方法
US8993613B2 (en) 2013-04-17 2015-03-31 The Hartz Mountain Corporation Ectoparasiticidal formulations
CN105254565A (zh) * 2015-09-30 2016-01-20 乐平市康鑫医药化工有限公司 由氰基吡唑一锅法合成硫醚的工艺方法
CN106977460A (zh) * 2017-04-19 2017-07-25 江苏托球农化股份有限公司 1‑(2,6‑二氯‑4‑三氟甲基)苯基‑3‑氰基‑4‑乙巯基‑5‑氨基吡唑的合成
EP3412659A1 (en) 2017-06-09 2018-12-12 Solvay Sa Processes for the manufacture of sulfur-substituted pyrazole derivatives
EP3412658A1 (en) 2017-06-09 2018-12-12 Solvay Sa Processes for the manufacture of sulfur-substitued pyrazole derivatives
CN112430213A (zh) * 2020-12-03 2021-03-02 江苏优普生物化学科技股份有限公司 一种三氟甲硫基吡唑合成工艺
CN113149909B (zh) * 2021-03-24 2022-04-19 台州达辰药业有限公司 5-氨基-3-氰基-1-(2,6-二氯-4-三氟甲基-苯基)吡唑二硫化物制备方法
CN113480482B (zh) * 2021-07-05 2022-11-18 海正药业南通有限公司 一种非泼罗尼中间体的合成方法
CN114213330A (zh) * 2021-12-29 2022-03-22 天和药业股份有限公司 一种氟虫腈精制母液的处理方法

Family Cites Families (6)

* Cited by examiner, † Cited by third party
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FR2716453B1 (fr) * 1994-02-22 1996-03-29 Rhone Poulenc Agrochimie Procédé de sulfinylation de composés hétérocycliques.
DE3602728A1 (de) * 1985-05-17 1986-11-20 Bayer Ag, 51373 Leverkusen Schaedlingsbekaempfungsmittel auf basis von pyrazolderivaten
US5232940A (en) 1985-12-20 1993-08-03 Hatton Leslie R Derivatives of N-phenylpyrazoles
GB8713768D0 (en) * 1987-06-12 1987-07-15 May & Baker Ltd Compositions of matter
US5547974A (en) * 1985-12-20 1996-08-20 Rhone-Poulenc Agriculture Ltd. Derivatives of N-phenylpyrazoles
CA2004776C (fr) 1988-12-13 2000-04-25 Claude Wakselman Procede de preparation de perfluoroalkylthioethers

Also Published As

Publication number Publication date
CZ299822B6 (cs) 2008-12-03
HRP20020438B1 (en) 2011-01-31
IN192712B (hu) 2004-05-15
KR100665599B1 (ko) 2007-01-10
EA200200481A1 (ru) 2002-10-31
HRP20020438A2 (en) 2004-08-31
BG106622A (en) 2002-12-29
DK1222173T3 (da) 2004-09-20
CN1163488C (zh) 2004-08-25
AU1270700A (en) 2001-05-08
AU783139B2 (en) 2005-09-29
TR200201072T2 (tr) 2002-07-22
CN101445483A (zh) 2009-06-03
DE69919599D1 (de) 2004-09-23
HU229393B1 (en) 2013-11-28
BG65483B1 (bg) 2008-09-30
EA005077B1 (ru) 2004-10-28
BR9917518B1 (pt) 2009-08-11
ES2222743T3 (es) 2005-02-01
CN101445483B (zh) 2011-03-30
KR100665598B1 (ko) 2007-01-10
IN2002MU00312A (hu) 2007-06-29
IL149152A0 (en) 2002-11-10
CN1332730A (zh) 2002-01-23
KR20060097747A (ko) 2006-09-14
RO121209B1 (ro) 2007-01-30
BR9917518A (pt) 2002-06-18
PL206482B1 (pl) 2010-08-31
MXPA02003944A (es) 2003-10-15
MX229662B (es) 2005-08-04
CZ20021384A3 (cs) 2002-08-14
CA2384283C (en) 2009-02-03
WO2001030760A1 (en) 2001-05-03
PT1222173E (pt) 2004-11-30
EP1222173B1 (en) 2004-08-18
US6620943B1 (en) 2003-09-16
PL354611A1 (en) 2004-02-09
NZ517770A (en) 2003-11-28
NZ527896A (en) 2004-07-30
US6881848B2 (en) 2005-04-19
ZA200201961B (en) 2003-05-28
JP4666863B2 (ja) 2011-04-06
ATE273961T1 (de) 2004-09-15
HUP0203206A3 (en) 2005-11-28
US20040034234A1 (en) 2004-02-19
TR200202806T2 (tr) 2003-03-21
MEP7808A (en) 2010-06-10
DE69919599T2 (de) 2005-08-11
UA73752C2 (en) 2005-09-15
TW553936B (en) 2003-09-21
CN1896066A (zh) 2007-01-17
IN2005MU00818A (hu) 2005-11-11
CA2384283A1 (en) 2001-05-03
IL149152A (en) 2008-08-07
KR20020040899A (ko) 2002-05-30
CN1896066B (zh) 2011-06-15
EP1222173A1 (en) 2002-07-17
JP2003512456A (ja) 2003-04-02

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Legal Events

Date Code Title Description
GB9A Succession in title

Owner name: BASF AGRO B.V., ARNHEM (NL), WAEDENSWIL-BRANCH, CH

Free format text: FORMER OWNER(S): AVENTIS CROPSCIENCE S.A., FR