HRP20020438B1 - Process for preparing 4-trifluoromethylsulphinylpyrazole derivative - Google Patents

Process for preparing 4-trifluoromethylsulphinylpyrazole derivative

Info

Publication number
HRP20020438B1
HRP20020438B1 HR20020438A HRP20020438A HRP20020438B1 HR P20020438 B1 HRP20020438 B1 HR P20020438B1 HR 20020438 A HR20020438 A HR 20020438A HR P20020438 A HRP20020438 A HR P20020438A HR P20020438 B1 HRP20020438 B1 HR P20020438B1
Authority
HR
Croatia
Prior art keywords
trifluoromethylsulphinylpyrazole
derivative
preparing
halogen
compound
Prior art date
Application number
HR20020438A
Other languages
English (en)
Croatian (hr)
Inventor
Clavel Jean-Louis
Pelta Isabelle
Le Bars Sylvie
Charreau Philippe
Original Assignee
BASF Agro B.V.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=8167491&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=HRP20020438(B1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by BASF Agro B.V. filed Critical BASF Agro B.V.
Priority to HR20020438A priority Critical patent/HRP20020438B1/xx
Publication of HRP20020438A2 publication Critical patent/HRP20020438A2/hr
Publication of HRP20020438B1 publication Critical patent/HRP20020438B1/xx

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D401/00—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
    • C07D401/02—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings
    • C07D401/04—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings directly linked by a ring-member-to-ring-member bond
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/44—Oxygen and nitrogen or sulfur and nitrogen atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
HR20020438A 1999-10-22 2002-05-20 Process for preparing 4-trifluoromethylsulphinylpyrazole derivative HRP20020438B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
HR20020438A HRP20020438B1 (en) 1999-10-22 2002-05-20 Process for preparing 4-trifluoromethylsulphinylpyrazole derivative

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
PCT/EP1999/008687 WO2001030760A1 (en) 1999-10-22 1999-10-22 Process for preparing 4-trifluoromethylsulphinylpyrazole derivative
HR20020438A HRP20020438B1 (en) 1999-10-22 2002-05-20 Process for preparing 4-trifluoromethylsulphinylpyrazole derivative

Publications (2)

Publication Number Publication Date
HRP20020438A2 HRP20020438A2 (en) 2004-08-31
HRP20020438B1 true HRP20020438B1 (en) 2011-01-31

Family

ID=8167491

Family Applications (1)

Application Number Title Priority Date Filing Date
HR20020438A HRP20020438B1 (en) 1999-10-22 2002-05-20 Process for preparing 4-trifluoromethylsulphinylpyrazole derivative

Country Status (30)

Country Link
US (2) US6620943B1 (hu)
EP (1) EP1222173B1 (hu)
JP (1) JP4666863B2 (hu)
KR (2) KR100665598B1 (hu)
CN (3) CN101445483B (hu)
AT (1) ATE273961T1 (hu)
AU (1) AU783139B2 (hu)
BG (1) BG65483B1 (hu)
BR (1) BR9917518B1 (hu)
CA (1) CA2384283C (hu)
CZ (1) CZ299822B6 (hu)
DE (1) DE69919599T2 (hu)
DK (1) DK1222173T3 (hu)
EA (1) EA005077B1 (hu)
ES (1) ES2222743T3 (hu)
HR (1) HRP20020438B1 (hu)
HU (1) HU229393B1 (hu)
IL (2) IL149152A0 (hu)
IN (2) IN2005MU00818A (hu)
ME (1) MEP7808A (hu)
MX (1) MX229662B (hu)
NZ (2) NZ527896A (hu)
PL (1) PL206482B1 (hu)
PT (1) PT1222173E (hu)
RO (1) RO121209B1 (hu)
TR (2) TR200201072T2 (hu)
TW (1) TW553936B (hu)
UA (1) UA73752C2 (hu)
WO (1) WO2001030760A1 (hu)
ZA (1) ZA200201961B (hu)

Families Citing this family (35)

* Cited by examiner, † Cited by third party
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MXPA01013211A (es) 1999-06-29 2002-08-12 Mitsubishi Chem Corp Derivados de pirazol y procedimiento para producir los mismos, pesticidas que contienen los mismos como el ingrediente activo.
WO2005023774A1 (en) * 2003-09-11 2005-03-17 Cheminova A/S Process for the preparation of a trifluoromethylthioether
CN100586934C (zh) * 2003-11-07 2010-02-03 凯米诺瓦有限公司 制备三氟甲基硫醚的方法
DE102004020069C5 (de) 2004-04-24 2013-12-05 Voith Patent Gmbh Verfahren zum Satinieren einer Papierbahn
AU2013203226B2 (en) * 2005-12-14 2015-08-27 Makhteshim Chemical Works Ltd Polymorphs and amorphous forms of 5-amino-1-[2,6- dichloro-4-(trifluoromethyl)phenyl]-4- [(trifluoromethyl)sulfinyl]-1H-pyrazole-3-carbonitrile
EP1968578A4 (en) 2005-12-14 2011-02-23 Makhteshim Chem Works Ltd POLYMORPHIC AND AMORPHOUS FORMS OF 5-AMINO-L- [2,6-DICHLORO-4- (TRIFLUOROMETHYL) PHENYL] -4- [(TRIFLUOROMETHYL) SULFINYL] -IH-PYRAZOLE-3-CARBONITRIL
US7777052B2 (en) 2006-04-25 2010-08-17 Gharda Chemicals Limited Process for the preparation of Fipronil, an insecticide, and related pyrazoles
CN101168529B (zh) * 2006-10-24 2011-03-23 温州大学 氟虫腈、乙虫腈及其衍生物的合成方法
PT2083629E (pt) * 2006-11-10 2011-09-01 Basf Se Modificação cristalina de fipronil
CA2667562A1 (en) 2006-11-10 2008-05-15 Basf Se Process for the sulfinylation of a pyrazole derivative
UA110598C2 (uk) * 2006-11-10 2016-01-25 Басф Се Спосіб одержання кристалічної модифікації фіпронілу
BRPI0718720A2 (pt) * 2006-11-10 2013-12-03 Basf Se Fipronil sólido, processo para preparar a modificação cristalina v, mistura pesticida ou parasiticida sinergística, composição pesticida ou parasiticida, uso do fipronil sólido ou da mistura ou da composição, métodos para controlar pragas, para proteger uma planta da infestação e ataque por pragas e para protefer semente e para tratar, controlar, previnir ou proteger animais contra infestação ou infecção por parasitas, semente, e, processo para preparar uma composição para tratar, controlar, prevenir ou proteger animais contra infestação ou infecção por parasitas.
EP2081908B1 (en) 2006-11-10 2013-04-24 BASF Agro B.V., Arnhem (NL), Zürich Branch Process for the sulfinylation of a pyrazole derivative
WO2008055882A1 (en) 2006-11-10 2008-05-15 Basf Se Crystalline modification of fipronil
CN101250158B (zh) * 2008-04-02 2011-12-07 湖南化工研究院 一种氟虫腈的制备方法
DK2349987T3 (da) 2008-10-02 2013-03-11 Basf Se Fremgangsmåde til fremstilling og oprensning af trifluormethansulfinsyre
WO2010049746A1 (en) * 2008-10-27 2010-05-06 Dynamit Nobel Gmbh Explosivstoff-Und Systemtechnic Process for the synthesis of fipronil
DK2493860T3 (da) 2009-10-30 2014-04-07 Basf Se Fremgangsmåde til fremstilling af 4-sulfinylpyrazolderivater
AU2010100462A4 (en) 2010-03-03 2010-06-17 Keki Hormusji Gharda A process for the synthesis of Fipronil
IT1400666B1 (it) 2010-07-07 2013-06-28 Finchimica Srl Procedimento per la sintesi di 5-amino, 1-fenil, 3-ciano, 4-trifluorometil sulfinil pirazoli.
CN103153961A (zh) 2010-07-12 2013-06-12 塞尔休斯物业公司埃尔维塔植物保护分公司 氟虫腈制备方法
CN103313604B (zh) * 2011-01-14 2016-03-02 K·H·伽达 [5-氨基-1-(2,6-二氯-4-三氟甲苯基)-3-腈-4-三氟甲基亚磺酰基吡唑]中的多晶体
CN103547572B (zh) 2011-05-30 2016-03-30 K·H·伽达 一种合成氟虫腈的工艺
CN102633722B (zh) * 2012-03-20 2015-05-06 金坛市凌云动物保健品有限公司 一种非泼罗尼的制备方法
TWI579274B (zh) 2012-04-20 2017-04-21 龍馬躍公司 製備１－芳基－５－烷基吡唑化合物的改良方法
CN102690232A (zh) * 2012-05-30 2012-09-26 河南中医学院 一种氟虫腈中间体的合成方法
US9049860B2 (en) 2013-04-17 2015-06-09 The Hartz Mountain Corporation Ectoparasiticidal methods
CN105254565A (zh) * 2015-09-30 2016-01-20 乐平市康鑫医药化工有限公司 由氰基吡唑一锅法合成硫醚的工艺方法
CN106977460A (zh) * 2017-04-19 2017-07-25 江苏托球农化股份有限公司 1‑(2,6‑二氯‑4‑三氟甲基)苯基‑3‑氰基‑4‑乙巯基‑5‑氨基吡唑的合成
EP3412659A1 (en) 2017-06-09 2018-12-12 Solvay Sa Processes for the manufacture of sulfur-substituted pyrazole derivatives
EP3412658A1 (en) 2017-06-09 2018-12-12 Solvay Sa Processes for the manufacture of sulfur-substitued pyrazole derivatives
CN112430213A (zh) * 2020-12-03 2021-03-02 江苏优普生物化学科技股份有限公司 一种三氟甲硫基吡唑合成工艺
CN113149909B (zh) * 2021-03-24 2022-04-19 台州达辰药业有限公司 5-氨基-3-氰基-1-(2,6-二氯-4-三氟甲基-苯基)吡唑二硫化物制备方法
CN113480482B (zh) * 2021-07-05 2022-11-18 海正药业南通有限公司 一种非泼罗尼中间体的合成方法
CN114213330A (zh) * 2021-12-29 2022-03-22 天和药业股份有限公司 一种氟虫腈精制母液的处理方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0295117A1 (en) * 1987-06-12 1988-12-14 Rhone-Poulenc Agriculture Limited Derivatives of N-phenylpyrazoles
EP0374061A1 (fr) * 1988-12-13 1990-06-20 Rhone-Poulenc Agrochimie Procédé de préparation de perhalogénoalkylthioéthers
EP0668269A1 (fr) * 1994-02-22 1995-08-23 Rhone-Poulenc Agrochimie Procédé de sulfinylation de composés hétérocycliques

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3602728A1 (de) * 1985-05-17 1986-11-20 Bayer Ag, 51373 Leverkusen Schaedlingsbekaempfungsmittel auf basis von pyrazolderivaten
US5232940A (en) 1985-12-20 1993-08-03 Hatton Leslie R Derivatives of N-phenylpyrazoles
US5547974A (en) * 1985-12-20 1996-08-20 Rhone-Poulenc Agriculture Ltd. Derivatives of N-phenylpyrazoles

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0295117A1 (en) * 1987-06-12 1988-12-14 Rhone-Poulenc Agriculture Limited Derivatives of N-phenylpyrazoles
EP0374061A1 (fr) * 1988-12-13 1990-06-20 Rhone-Poulenc Agrochimie Procédé de préparation de perhalogénoalkylthioéthers
EP0668269A1 (fr) * 1994-02-22 1995-08-23 Rhone-Poulenc Agrochimie Procédé de sulfinylation de composés hétérocycliques

Also Published As

Publication number Publication date
DK1222173T3 (da) 2004-09-20
KR100665598B1 (ko) 2007-01-10
BG106622A (en) 2002-12-29
PL206482B1 (pl) 2010-08-31
IN192712B (hu) 2004-05-15
KR20020040899A (ko) 2002-05-30
BR9917518B1 (pt) 2009-08-11
EA200200481A1 (ru) 2002-10-31
CA2384283C (en) 2009-02-03
KR20060097747A (ko) 2006-09-14
EP1222173A1 (en) 2002-07-17
WO2001030760A1 (en) 2001-05-03
TW553936B (en) 2003-09-21
NZ527896A (en) 2004-07-30
EP1222173B1 (en) 2004-08-18
US6620943B1 (en) 2003-09-16
MX229662B (es) 2005-08-04
JP2003512456A (ja) 2003-04-02
CN101445483A (zh) 2009-06-03
IL149152A0 (en) 2002-11-10
CN1163488C (zh) 2004-08-25
CN1332730A (zh) 2002-01-23
HU229393B1 (en) 2013-11-28
IN2002MU00312A (hu) 2007-06-29
CN101445483B (zh) 2011-03-30
ZA200201961B (en) 2003-05-28
CZ20021384A3 (cs) 2002-08-14
KR100665599B1 (ko) 2007-01-10
IL149152A (en) 2008-08-07
PT1222173E (pt) 2004-11-30
CZ299822B6 (cs) 2008-12-03
HUP0203206A3 (en) 2005-11-28
CN1896066B (zh) 2011-06-15
CN1896066A (zh) 2007-01-17
ATE273961T1 (de) 2004-09-15
EA005077B1 (ru) 2004-10-28
DE69919599T2 (de) 2005-08-11
US6881848B2 (en) 2005-04-19
AU783139B2 (en) 2005-09-29
BR9917518A (pt) 2002-06-18
AU1270700A (en) 2001-05-08
NZ517770A (en) 2003-11-28
MXPA02003944A (es) 2003-10-15
ES2222743T3 (es) 2005-02-01
IN2005MU00818A (hu) 2005-11-11
MEP7808A (en) 2010-06-10
US20040034234A1 (en) 2004-02-19
PL354611A1 (en) 2004-02-09
DE69919599D1 (de) 2004-09-23
RO121209B1 (ro) 2007-01-30
JP4666863B2 (ja) 2011-04-06
UA73752C2 (en) 2005-09-15
CA2384283A1 (en) 2001-05-03
TR200201072T2 (tr) 2002-07-22
TR200202806T2 (tr) 2003-03-21
BG65483B1 (bg) 2008-09-30
HRP20020438A2 (en) 2004-08-31
HUP0203206A2 (hu) 2003-03-28

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Legal Events

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A1OB Publication of a patent application
ARAI Request for the grant of a patent on the basis of the submitted results of a substantive examination of a patent application
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Owner name: BASF AGRO B.V., CH

B1PR Patent granted
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Payment date: 20181019

Year of fee payment: 20

PB20 Patent expired after termination of 20 years

Effective date: 20191022