TR200201072T2 - 4-Triflorometilsulfinilpirazol türevi hazırlama süreci - Google Patents

4-Triflorometilsulfinilpirazol türevi hazırlama süreci

Info

Publication number
TR200201072T2
TR200201072T2 TR2002/01072T TR200201072T TR200201072T2 TR 200201072 T2 TR200201072 T2 TR 200201072T2 TR 2002/01072 T TR2002/01072 T TR 2002/01072T TR 200201072 T TR200201072 T TR 200201072T TR 200201072 T2 TR200201072 T2 TR 200201072T2
Authority
TR
Turkey
Prior art keywords
trifluoromethylsulfinylpyrazole
preparation process
derivative preparation
halogen
haloalkyl
Prior art date
Application number
TR2002/01072T
Other languages
English (en)
Inventor
Clavel Jean-Louis
Pelta Isabella
Le Bars Sylvie
Charreau Philippe
Original Assignee
Aventis Cropscience Sa
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=8167491&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=TR200201072(T2) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Aventis Cropscience Sa filed Critical Aventis Cropscience Sa
Publication of TR200201072T2 publication Critical patent/TR200201072T2/tr

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D401/00Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
    • C07D401/02Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings
    • C07D401/04Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings directly linked by a ring-member-to-ring-member bond
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D231/00Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/44Oxygen and nitrogen or sulfur and nitrogen atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

Formül (I) bilesiginin hazirlanisi için bir bulus, R halojeni, haloalkili, haloalkoksiyi, R4S(O)n- veya -SF5'i;, R hidrojen veya halojeni; R halojeni; R4 alkil veya haloalkili; ve n 0,1 veya 2'yi temsil eder; bu bulus formül (II) bilesiginin okside edilmesini içerir; burada asinma önleyici önündeki trifloroperasetik asitle bereaber R ,R ve W yukarida tanimlandigi gibidir.
TR2002/01072T 1999-10-22 1999-10-22 4-Triflorometilsulfinilpirazol türevi hazırlama süreci TR200201072T2 (tr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/EP1999/008687 WO2001030760A1 (en) 1999-10-22 1999-10-22 Process for preparing 4-trifluoromethylsulphinylpyrazole derivative

Publications (1)

Publication Number Publication Date
TR200201072T2 true TR200201072T2 (tr) 2002-07-22

Family

ID=8167491

Family Applications (2)

Application Number Title Priority Date Filing Date
TR2002/01072T TR200201072T2 (tr) 1999-10-22 1999-10-22 4-Triflorometilsulfinilpirazol türevi hazırlama süreci
TR2002/02806T TR200202806T2 (tr) 1999-10-22 1999-10-22 4-Triflorometilsulfinilpirazol türevi hazırlama süreci

Family Applications After (1)

Application Number Title Priority Date Filing Date
TR2002/02806T TR200202806T2 (tr) 1999-10-22 1999-10-22 4-Triflorometilsulfinilpirazol türevi hazırlama süreci

Country Status (30)

Country Link
US (2) US6620943B1 (tr)
EP (1) EP1222173B1 (tr)
JP (1) JP4666863B2 (tr)
KR (2) KR100665598B1 (tr)
CN (3) CN101445483B (tr)
AT (1) ATE273961T1 (tr)
AU (1) AU783139B2 (tr)
BG (1) BG65483B1 (tr)
BR (1) BR9917518B1 (tr)
CA (1) CA2384283C (tr)
CZ (1) CZ299822B6 (tr)
DE (1) DE69919599T2 (tr)
DK (1) DK1222173T3 (tr)
EA (1) EA005077B1 (tr)
ES (1) ES2222743T3 (tr)
HR (1) HRP20020438B1 (tr)
HU (1) HU229393B1 (tr)
IL (2) IL149152A0 (tr)
IN (2) IN2005MU00818A (tr)
ME (1) MEP7808A (tr)
MX (1) MX229662B (tr)
NZ (2) NZ517770A (tr)
PL (1) PL206482B1 (tr)
PT (1) PT1222173E (tr)
RO (1) RO121209B1 (tr)
TR (2) TR200201072T2 (tr)
TW (1) TW553936B (tr)
UA (1) UA73752C2 (tr)
WO (1) WO2001030760A1 (tr)
ZA (1) ZA200201961B (tr)

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WO2005023774A1 (en) * 2003-09-11 2005-03-17 Cheminova A/S Process for the preparation of a trifluoromethylthioether
CN100586934C (zh) * 2003-11-07 2010-02-03 凯米诺瓦有限公司 制备三氟甲基硫醚的方法
DE102004020069C5 (de) 2004-04-24 2013-12-05 Voith Patent Gmbh Verfahren zum Satinieren einer Papierbahn
AU2013203228B2 (en) * 2005-12-14 2015-08-27 Makhteshim Chemical Works Ltd Polymorphs and amorphous forms of 5-amino-1-[2,6- dichloro-4-(trifluoromethyl)phenyl]-4- [(trifluoromethyl)sulfinyl]-1H-pyrazole-3-carbonitrile
CA2630849C (en) 2005-12-14 2013-05-14 Makhteshim Chemical Works Ltd. Polymorphs and amorphous forms of 5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-4-[(trifluoromethyl)sulfinyl]-1h-pyrazole-3-carbonitrile
BRPI0621611B1 (pt) 2006-04-25 2015-08-18 Gharda Chemicals Ltd Processo para a preparação de fipronila, inseticida e pirazóis relacionados
CN101168529B (zh) * 2006-10-24 2011-03-23 温州大学 氟虫腈、乙虫腈及其衍生物的合成方法
CA2667562A1 (en) 2006-11-10 2008-05-15 Basf Se Process for the sulfinylation of a pyrazole derivative
JP5931322B2 (ja) 2006-11-10 2016-06-08 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se フィプロニルの結晶変態
CA2667559A1 (en) 2006-11-10 2008-05-15 Basf Se Process for the sulfinylation of a pyrazole derivative
MX2009004323A (es) * 2006-11-10 2009-05-05 Basf Se Nueva modificacion cristalina.
BRPI0718715B8 (pt) 2006-11-10 2021-03-23 Basf Se modificação cristalina iv de fipronil contendo acetona co-cristalizada, fipronil sólido, processos para preparar as modificações cristalinas iv, v e i, mistura pesticida ou parasiticida e composição pesticida ou parasiticida
UA110598C2 (uk) 2006-11-10 2016-01-25 Басф Се Спосіб одержання кристалічної модифікації фіпронілу
CN101250158B (zh) * 2008-04-02 2011-12-07 湖南化工研究院 一种氟虫腈的制备方法
EP2349987B1 (de) 2008-10-02 2012-11-14 Basf Se Verfahren zur herstellung und aufreinigung von trifluormethansulfinsäure
WO2010049746A1 (en) * 2008-10-27 2010-05-06 Dynamit Nobel Gmbh Explosivstoff-Und Systemtechnic Process for the synthesis of fipronil
EP2493860B1 (en) 2009-10-30 2014-01-15 Basf Se Process for the preparation of 4-sulfinyl-pyrazole derivatives
AU2010100462A4 (en) 2010-03-03 2010-06-17 Keki Hormusji Gharda A process for the synthesis of Fipronil
IT1400666B1 (it) 2010-07-07 2013-06-28 Finchimica Srl Procedimento per la sintesi di 5-amino, 1-fenil, 3-ciano, 4-trifluorometil sulfinil pirazoli.
CA2805227A1 (en) 2010-07-12 2012-01-19 Irvita Plant Protection, A Branch Of Celsius Property B.V. Fipronil production process
CN103313604B (zh) * 2011-01-14 2016-03-02 K·H·伽达 [5-氨基-1-(2,6-二氯-4-三氟甲苯基)-3-腈-4-三氟甲基亚磺酰基吡唑]中的多晶体
EP2714664B1 (en) 2011-05-30 2016-10-19 Keki Hormusji Gharda Process for synthesis of fipronil
CN102633722B (zh) * 2012-03-20 2015-05-06 金坛市凌云动物保健品有限公司 一种非泼罗尼的制备方法
TWI579274B (zh) * 2012-04-20 2017-04-21 龍馬躍公司 製備1-芳基-5-烷基吡唑化合物的改良方法
CN102690232A (zh) * 2012-05-30 2012-09-26 河南中医学院 一种氟虫腈中间体的合成方法
US9049860B2 (en) 2013-04-17 2015-06-09 The Hartz Mountain Corporation Ectoparasiticidal methods
CN105254565A (zh) * 2015-09-30 2016-01-20 乐平市康鑫医药化工有限公司 由氰基吡唑一锅法合成硫醚的工艺方法
CN106977460A (zh) * 2017-04-19 2017-07-25 江苏托球农化股份有限公司 1‑(2,6‑二氯‑4‑三氟甲基)苯基‑3‑氰基‑4‑乙巯基‑5‑氨基吡唑的合成
EP3412659A1 (en) 2017-06-09 2018-12-12 Solvay Sa Processes for the manufacture of sulfur-substituted pyrazole derivatives
EP3412658A1 (en) 2017-06-09 2018-12-12 Solvay Sa Processes for the manufacture of sulfur-substitued pyrazole derivatives
CN112430213A (zh) * 2020-12-03 2021-03-02 江苏优普生物化学科技股份有限公司 一种三氟甲硫基吡唑合成工艺
CN113149909B (zh) * 2021-03-24 2022-04-19 台州达辰药业有限公司 5-氨基-3-氰基-1-(2,6-二氯-4-三氟甲基-苯基)吡唑二硫化物制备方法
CN113480482B (zh) * 2021-07-05 2022-11-18 海正药业南通有限公司 一种非泼罗尼中间体的合成方法
CN114213330A (zh) * 2021-12-29 2022-03-22 天和药业股份有限公司 一种氟虫腈精制母液的处理方法

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FR2716453B1 (fr) * 1994-02-22 1996-03-29 Rhone Poulenc Agrochimie Procédé de sulfinylation de composés hétérocycliques.
DE3602728A1 (de) * 1985-05-17 1986-11-20 Bayer Ag, 51373 Leverkusen Schaedlingsbekaempfungsmittel auf basis von pyrazolderivaten
US5232940A (en) 1985-12-20 1993-08-03 Hatton Leslie R Derivatives of N-phenylpyrazoles
US5547974A (en) * 1985-12-20 1996-08-20 Rhone-Poulenc Agriculture Ltd. Derivatives of N-phenylpyrazoles
GB8713768D0 (en) * 1987-06-12 1987-07-15 May & Baker Ltd Compositions of matter
CA2004776C (fr) * 1988-12-13 2000-04-25 Claude Wakselman Procede de preparation de perfluoroalkylthioethers

Also Published As

Publication number Publication date
CZ299822B6 (cs) 2008-12-03
WO2001030760A1 (en) 2001-05-03
IN2002MU00312A (tr) 2007-06-29
RO121209B1 (ro) 2007-01-30
PL206482B1 (pl) 2010-08-31
IL149152A0 (en) 2002-11-10
HU229393B1 (en) 2013-11-28
HUP0203206A2 (hu) 2003-03-28
JP2003512456A (ja) 2003-04-02
TW553936B (en) 2003-09-21
US6881848B2 (en) 2005-04-19
MX229662B (es) 2005-08-04
IL149152A (en) 2008-08-07
PT1222173E (pt) 2004-11-30
CZ20021384A3 (cs) 2002-08-14
BR9917518A (pt) 2002-06-18
MEP7808A (en) 2010-06-10
EA005077B1 (ru) 2004-10-28
CN1163488C (zh) 2004-08-25
KR100665599B1 (ko) 2007-01-10
KR20020040899A (ko) 2002-05-30
JP4666863B2 (ja) 2011-04-06
CA2384283A1 (en) 2001-05-03
ES2222743T3 (es) 2005-02-01
CN101445483A (zh) 2009-06-03
NZ527896A (en) 2004-07-30
UA73752C2 (en) 2005-09-15
AU1270700A (en) 2001-05-08
PL354611A1 (en) 2004-02-09
IN2005MU00818A (tr) 2005-11-11
DK1222173T3 (da) 2004-09-20
CN101445483B (zh) 2011-03-30
BG65483B1 (bg) 2008-09-30
MXPA02003944A (es) 2003-10-15
DE69919599D1 (de) 2004-09-23
HUP0203206A3 (en) 2005-11-28
EP1222173A1 (en) 2002-07-17
US6620943B1 (en) 2003-09-16
BG106622A (en) 2002-12-29
KR100665598B1 (ko) 2007-01-10
CN1896066B (zh) 2011-06-15
ZA200201961B (en) 2003-05-28
HRP20020438B1 (en) 2011-01-31
IN192712B (tr) 2004-05-15
EP1222173B1 (en) 2004-08-18
CN1896066A (zh) 2007-01-17
AU783139B2 (en) 2005-09-29
HRP20020438A2 (en) 2004-08-31
KR20060097747A (ko) 2006-09-14
CA2384283C (en) 2009-02-03
EA200200481A1 (ru) 2002-10-31
DE69919599T2 (de) 2005-08-11
BR9917518B1 (pt) 2009-08-11
US20040034234A1 (en) 2004-02-19
ATE273961T1 (de) 2004-09-15
CN1332730A (zh) 2002-01-23
TR200202806T2 (tr) 2003-03-21
NZ517770A (en) 2003-11-28

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