FI62538C - Foerfarande foer kontinuerlig framstaellning av alkoxisilaner - Google Patents
Foerfarande foer kontinuerlig framstaellning av alkoxisilaner Download PDFInfo
- Publication number
- FI62538C FI62538C FI751673A FI751673A FI62538C FI 62538 C FI62538 C FI 62538C FI 751673 A FI751673 A FI 751673A FI 751673 A FI751673 A FI 751673A FI 62538 C FI62538 C FI 62538C
- Authority
- FI
- Finland
- Prior art keywords
- column
- hydrogen chloride
- solvent
- ester
- esterification
- Prior art date
Links
- 230000001476 alcoholic effect Effects 0.000 title 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 35
- 229910000041 hydrogen chloride Inorganic materials 0.000 claims description 34
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 claims description 34
- 238000009835 boiling Methods 0.000 claims description 26
- 238000005886 esterification reaction Methods 0.000 claims description 22
- 230000032050 esterification Effects 0.000 claims description 21
- 238000004821 distillation Methods 0.000 claims description 19
- 239000002904 solvent Substances 0.000 claims description 19
- 239000005046 Chlorosilane Substances 0.000 claims description 12
- 238000006243 chemical reaction Methods 0.000 claims description 12
- KOPOQZFJUQMUML-UHFFFAOYSA-N chlorosilane Chemical class Cl[SiH3] KOPOQZFJUQMUML-UHFFFAOYSA-N 0.000 claims description 11
- 239000007788 liquid Substances 0.000 claims description 11
- 150000001298 alcohols Chemical class 0.000 claims description 8
- 239000000376 reactant Substances 0.000 claims description 8
- 150000002148 esters Chemical class 0.000 claims description 6
- 239000001257 hydrogen Substances 0.000 claims description 5
- 229910052739 hydrogen Inorganic materials 0.000 claims description 5
- 229920006395 saturated elastomer Chemical group 0.000 claims description 5
- 125000004432 carbon atom Chemical group C* 0.000 claims description 4
- 238000010924 continuous production Methods 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 239000007791 liquid phase Substances 0.000 claims description 3
- 125000000217 alkyl group Chemical group 0.000 claims description 2
- 125000005842 heteroatom Chemical group 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims description 2
- 125000001931 aliphatic group Chemical group 0.000 claims 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 36
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 34
- 238000000034 method Methods 0.000 description 21
- ZDHXKXAHOVTTAH-UHFFFAOYSA-N trichlorosilane Chemical compound Cl[SiH](Cl)Cl ZDHXKXAHOVTTAH-UHFFFAOYSA-N 0.000 description 15
- 239000005052 trichlorosilane Substances 0.000 description 15
- -1 hydrogen chloride forms chloroalkanes Chemical class 0.000 description 14
- 229910000077 silane Inorganic materials 0.000 description 9
- 230000015572 biosynthetic process Effects 0.000 description 8
- 238000000746 purification Methods 0.000 description 7
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 description 6
- 238000007086 side reaction Methods 0.000 description 6
- 238000003786 synthesis reaction Methods 0.000 description 6
- XNWFRZJHXBZDAG-UHFFFAOYSA-N 2-METHOXYETHANOL Chemical compound COCCO XNWFRZJHXBZDAG-UHFFFAOYSA-N 0.000 description 5
- YUYCVXFAYWRXLS-UHFFFAOYSA-N trimethoxysilane Chemical compound CO[SiH](OC)OC YUYCVXFAYWRXLS-UHFFFAOYSA-N 0.000 description 5
- 239000005047 Allyltrichlorosilane Substances 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 238000000926 separation method Methods 0.000 description 4
- 150000004756 silanes Chemical class 0.000 description 4
- FDNAPBUWERUEDA-UHFFFAOYSA-N silicon tetrachloride Chemical compound Cl[Si](Cl)(Cl)Cl FDNAPBUWERUEDA-UHFFFAOYSA-N 0.000 description 4
- 239000007858 starting material Substances 0.000 description 4
- GQIUQDDJKHLHTB-UHFFFAOYSA-N trichloro(ethenyl)silane Chemical compound Cl[Si](Cl)(Cl)C=C GQIUQDDJKHLHTB-UHFFFAOYSA-N 0.000 description 4
- 239000005050 vinyl trichlorosilane Substances 0.000 description 4
- 238000010923 batch production Methods 0.000 description 3
- YSNGQKQKGVZLJO-UHFFFAOYSA-N chloro(dimethoxy)silane Chemical compound CO[SiH](Cl)OC YSNGQKQKGVZLJO-UHFFFAOYSA-N 0.000 description 3
- MLNILYVALGPOBD-UHFFFAOYSA-N chloro-dimethoxy-(2-methylpropyl)silane Chemical compound CO[Si](Cl)(OC)CC(C)C MLNILYVALGPOBD-UHFFFAOYSA-N 0.000 description 3
- LIKFHECYJZWXFJ-UHFFFAOYSA-N dimethyldichlorosilane Chemical compound C[Si](C)(Cl)Cl LIKFHECYJZWXFJ-UHFFFAOYSA-N 0.000 description 3
- YYLGKUPAFFKGRQ-UHFFFAOYSA-N dimethyldiethoxysilane Chemical compound CCO[Si](C)(C)OCC YYLGKUPAFFKGRQ-UHFFFAOYSA-N 0.000 description 3
- FWDBOZPQNFPOLF-UHFFFAOYSA-N ethenyl(triethoxy)silane Chemical compound CCO[Si](OCC)(OCC)C=C FWDBOZPQNFPOLF-UHFFFAOYSA-N 0.000 description 3
- GBXOGFTVYQSOID-UHFFFAOYSA-N trichloro(2-methylpropyl)silane Chemical compound CC(C)C[Si](Cl)(Cl)Cl GBXOGFTVYQSOID-UHFFFAOYSA-N 0.000 description 3
- HKFSBKQQYCMCKO-UHFFFAOYSA-N trichloro(prop-2-enyl)silane Chemical compound Cl[Si](Cl)(Cl)CC=C HKFSBKQQYCMCKO-UHFFFAOYSA-N 0.000 description 3
- KBPLFHHGFOOTCA-UHFFFAOYSA-N 1-Octanol Chemical compound CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- IJOOHPMOJXWVHK-UHFFFAOYSA-N chlorotrimethylsilane Chemical compound C[Si](C)(C)Cl IJOOHPMOJXWVHK-UHFFFAOYSA-N 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000011261 inert gas Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- KFUSEUYYWQURPO-OWOJBTEDSA-N trans-1,2-dichloroethene Chemical group Cl\C=C\Cl KFUSEUYYWQURPO-OWOJBTEDSA-N 0.000 description 2
- CPUDPFPXCZDNGI-UHFFFAOYSA-N triethoxy(methyl)silane Chemical compound CCO[Si](C)(OCC)OCC CPUDPFPXCZDNGI-UHFFFAOYSA-N 0.000 description 2
- QQQSFSZALRVCSZ-UHFFFAOYSA-N triethoxysilane Chemical compound CCO[SiH](OCC)OCC QQQSFSZALRVCSZ-UHFFFAOYSA-N 0.000 description 2
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical group ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 description 1
- DORVBVUZVNOVGH-UHFFFAOYSA-N 1-(2-hydroxyethoxy)-4-methoxybutan-2-ol Chemical compound COCCC(O)COCCO DORVBVUZVNOVGH-UHFFFAOYSA-N 0.000 description 1
- ZNQVEEAIQZEUHB-UHFFFAOYSA-N 2-ethoxyethanol Chemical compound CCOCCO ZNQVEEAIQZEUHB-UHFFFAOYSA-N 0.000 description 1
- 229940093475 2-ethoxyethanol Drugs 0.000 description 1
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 1
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 1
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 1
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical group ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 239000001089 [(2R)-oxolan-2-yl]methanol Substances 0.000 description 1
- 125000003545 alkoxy group Chemical group 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 229950005499 carbon tetrachloride Drugs 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 229960001701 chloroform Drugs 0.000 description 1
- NEHMKBQYUWJMIP-UHFFFAOYSA-N chloromethane Chemical compound ClC NEHMKBQYUWJMIP-UHFFFAOYSA-N 0.000 description 1
- SLLGVCUQYRMELA-UHFFFAOYSA-N chlorosilicon Chemical compound Cl[Si] SLLGVCUQYRMELA-UHFFFAOYSA-N 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000011437 continuous method Methods 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000006735 deficit Effects 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- ZPYQWYVXIIGOOH-UHFFFAOYSA-N dichloro(methoxy)silane Chemical compound CO[SiH](Cl)Cl ZPYQWYVXIIGOOH-UHFFFAOYSA-N 0.000 description 1
- KTQYJQFGNYHXMB-UHFFFAOYSA-N dichloro(methyl)silicon Chemical compound C[Si](Cl)Cl KTQYJQFGNYHXMB-UHFFFAOYSA-N 0.000 description 1
- REJXSKJCSSLMJA-UHFFFAOYSA-N dichloro-methoxy-(2-methylpropyl)silane Chemical compound CO[Si](Cl)(Cl)CC(C)C REJXSKJCSSLMJA-UHFFFAOYSA-N 0.000 description 1
- GAURFLBIDLSLQU-UHFFFAOYSA-N diethoxy(methyl)silicon Chemical compound CCO[Si](C)OCC GAURFLBIDLSLQU-UHFFFAOYSA-N 0.000 description 1
- PKTOVQRKCNPVKY-UHFFFAOYSA-N dimethoxy(methyl)silicon Chemical compound CO[Si](C)OC PKTOVQRKCNPVKY-UHFFFAOYSA-N 0.000 description 1
- 230000008034 disappearance Effects 0.000 description 1
- 125000004185 ester group Chemical group 0.000 description 1
- MBGQQKKTDDNCSG-UHFFFAOYSA-N ethenyl-diethoxy-methylsilane Chemical compound CCO[Si](C)(C=C)OCC MBGQQKKTDDNCSG-UHFFFAOYSA-N 0.000 description 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 1
- ITAHRPSKCCPKOK-UHFFFAOYSA-N ethyl trimethyl silicate Chemical compound CCO[Si](OC)(OC)OC ITAHRPSKCCPKOK-UHFFFAOYSA-N 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000011552 falling film Substances 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000005055 methyl trichlorosilane Substances 0.000 description 1
- 239000005048 methyldichlorosilane Substances 0.000 description 1
- JLUFWMXJHAVVNN-UHFFFAOYSA-N methyltrichlorosilane Chemical compound C[Si](Cl)(Cl)Cl JLUFWMXJHAVVNN-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 150000002905 orthoesters Chemical class 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 229910052573 porcelain Inorganic materials 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 1
- BSYVTEYKTMYBMK-UHFFFAOYSA-N tetrahydrofurfuryl alcohol Chemical compound OCC1CCCO1 BSYVTEYKTMYBMK-UHFFFAOYSA-N 0.000 description 1
- LFQCEHFDDXELDD-UHFFFAOYSA-N tetramethyl orthosilicate Chemical compound CO[Si](OC)(OC)OC LFQCEHFDDXELDD-UHFFFAOYSA-N 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- ZOYFEXPFPVDYIS-UHFFFAOYSA-N trichloro(ethyl)silane Chemical compound CC[Si](Cl)(Cl)Cl ZOYFEXPFPVDYIS-UHFFFAOYSA-N 0.000 description 1
- GPWLZOISJZHVHX-UHFFFAOYSA-N trichloro(propan-2-yl)silane Chemical compound CC(C)[Si](Cl)(Cl)Cl GPWLZOISJZHVHX-UHFFFAOYSA-N 0.000 description 1
- XYJRNCYWTVGEEG-UHFFFAOYSA-N trimethoxy(2-methylpropyl)silane Chemical compound CO[Si](OC)(OC)CC(C)C XYJRNCYWTVGEEG-UHFFFAOYSA-N 0.000 description 1
- 239000005051 trimethylchlorosilane Substances 0.000 description 1
- 238000005292 vacuum distillation Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/025—Silicon compounds without C-silicon linkages
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
- C07F7/1804—Compounds having Si-O-C linkages
- C07F7/1872—Preparation; Treatments not provided for in C07F7/20
- C07F7/188—Preparation; Treatments not provided for in C07F7/20 by reactions involving the formation of Si-O linkages
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19742427085 DE2427085C3 (de) | 1974-06-05 | Kontinuierliches Verfahren zur Herstellung von Alkoxisllanen | |
| DE2427085 | 1974-06-05 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| FI751673A FI751673A (de) | 1975-12-06 |
| FI62538B FI62538B (fi) | 1982-09-30 |
| FI62538C true FI62538C (fi) | 1983-01-10 |
Family
ID=5917349
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FI751673A FI62538C (fi) | 1974-06-05 | 1975-06-05 | Foerfarande foer kontinuerlig framstaellning av alkoxisilaner |
Country Status (17)
| Country | Link |
|---|---|
| US (1) | US4039567A (de) |
| JP (1) | JPS6035351B2 (de) |
| AT (1) | AT334915B (de) |
| BE (1) | BE829853A (de) |
| CA (1) | CA1051014A (de) |
| CH (1) | CH615684A5 (de) |
| DD (1) | DD120024A5 (de) |
| DK (1) | DK142237C (de) |
| ES (1) | ES438214A1 (de) |
| FI (1) | FI62538C (de) |
| FR (1) | FR2273812A1 (de) |
| GB (1) | GB1514197A (de) |
| IT (1) | IT1035922B (de) |
| NL (1) | NL181926C (de) |
| NO (1) | NO145075C (de) |
| SE (1) | SE415181B (de) |
| SU (1) | SU619108A3 (de) |
Families Citing this family (28)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5087845A (de) * | 1973-12-13 | 1975-07-15 | ||
| JPS564687Y2 (de) * | 1976-06-16 | 1981-02-02 | ||
| JPS5459461U (de) * | 1977-10-04 | 1979-04-24 | ||
| JPS5490482U (de) * | 1977-12-09 | 1979-06-26 | ||
| LU80112A1 (de) * | 1978-08-16 | 1979-01-19 | ||
| LU82173A1 (fr) * | 1980-02-15 | 1980-05-07 | Wurth Sa O | Dispositif de chargement pour fours a cuve |
| LU83280A1 (fr) * | 1981-04-03 | 1983-03-24 | Wurth Paul Sa | Procede pour actionner une goulotte oscillante dans une enceinte sous pression,dispositif pour la mise en oeuvre de ce procede et installation de chargement d'un four a cuve equipe d'un tel dispositif |
| US4609751A (en) * | 1981-12-14 | 1986-09-02 | General Electric Company | Method of hydrolyzing chlorosilanes |
| US4421926A (en) * | 1982-06-28 | 1983-12-20 | General Electric Company | Process for co-alkoxylation of halosilanes and separation of the resulting products |
| DE3236628C2 (de) * | 1982-10-04 | 1986-09-11 | Dynamit Nobel Ag, 5210 Troisdorf | Verfahren zur kontinuierlichen Herstellung von Alkoxysilanen |
| JPS60258189A (ja) * | 1984-06-02 | 1985-12-20 | Agency Of Ind Science & Technol | アルキルクロロシランの加水分解法 |
| DE3431839A1 (de) * | 1984-08-30 | 1986-03-06 | Dynamit Nobel Ag, 5210 Troisdorf | Verfahren zur herstellung von trialkylorganoxysilanen |
| DE3522904A1 (de) * | 1985-06-27 | 1987-01-08 | Dynamit Nobel Ag | Verfahren zur herstellung von orthoestern des titans, zirkons oder hafniums |
| US4855473A (en) * | 1986-05-27 | 1989-08-08 | Bayer Aktiengesellschaft | Process for the preparation of organooxychlorosilanes |
| JPS63102055U (de) * | 1986-12-19 | 1988-07-02 | ||
| NL8700819A (nl) * | 1987-04-08 | 1988-11-01 | Philips Nv | Inrichting voor het registreren van informatie op of het uitlezen van informatie uit een informatieplaat. |
| JPH02128245U (de) * | 1989-03-30 | 1990-10-23 | ||
| JPH02140656U (de) * | 1989-04-21 | 1990-11-26 | ||
| US4924022A (en) * | 1989-10-04 | 1990-05-08 | Dow Corning Corporation | Method for preparation of organoalkoxysilanes |
| US5559264A (en) * | 1994-02-24 | 1996-09-24 | Osi Specialities, Inc. | Process for making chloroorganosilicon compounds |
| US5374761A (en) | 1994-04-29 | 1994-12-20 | Corning Corporation | Process for preparation of organooxysilanes |
| ATE311396T1 (de) * | 2001-08-06 | 2005-12-15 | Degussa | Organosiliciumverbindungen |
| CN102070663B (zh) * | 2010-12-27 | 2013-01-09 | 蓝星化工新材料股份有限公司江西星火有机硅厂 | 二甲基二乙氧基硅烷制备工艺 |
| CN102532181B (zh) * | 2011-12-07 | 2014-05-28 | 江西晨光新材料有限公司 | 一种三甲氧基氢硅醇解工艺 |
| JP5978940B2 (ja) * | 2012-11-16 | 2016-08-24 | 信越化学工業株式会社 | オルガノキシシラン中の残留ハロゲン化物の低減方法 |
| CN103288865B (zh) * | 2013-05-31 | 2016-03-30 | 合盛硅业股份有限公司 | 一种利用有机硅共沸物生产正硅酸乙酯的方法 |
| CN109517006B (zh) * | 2018-11-13 | 2021-03-16 | 江西宏柏新材料股份有限公司 | 塔式有机法连续生产3-辛酰基硫代丙基三乙氧基硅烷的方法 |
| CN113150026A (zh) * | 2021-05-06 | 2021-07-23 | 兰州康鹏威耳化工有限公司 | 一种苯基三甲氧基硅烷连续制备方法和系统 |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2061189C3 (de) * | 1970-12-11 | 1974-12-05 | Wacker-Chemie Gmbh, 8000 Muenchen | Verfahren zur kontinuierlichen Herstellung von Alkoxysilanen oder Alkoxypolysiloxanen |
| US3801618A (en) * | 1973-06-06 | 1974-04-02 | Chevron Res | Process for alkyl orthosilicate |
-
1975
- 1975-05-06 DD DD185863A patent/DD120024A5/xx unknown
- 1975-05-22 GB GB22342/75A patent/GB1514197A/en not_active Expired
- 1975-05-26 SU SU752136593A patent/SU619108A3/ru active
- 1975-05-30 CH CH703575A patent/CH615684A5/de not_active IP Right Cessation
- 1975-06-03 JP JP50066986A patent/JPS6035351B2/ja not_active Expired
- 1975-06-03 IT IT49870/75A patent/IT1035922B/it active
- 1975-06-03 FR FR7517298A patent/FR2273812A1/fr active Granted
- 1975-06-03 AT AT419775A patent/AT334915B/de not_active IP Right Cessation
- 1975-06-03 NO NO751944A patent/NO145075C/no unknown
- 1975-06-04 ES ES438214A patent/ES438214A1/es not_active Expired
- 1975-06-04 DK DK251875A patent/DK142237C/da not_active IP Right Cessation
- 1975-06-04 BE BE157019A patent/BE829853A/xx not_active IP Right Cessation
- 1975-06-04 CA CA228,543A patent/CA1051014A/en not_active Expired
- 1975-06-04 SE SE7506387A patent/SE415181B/xx not_active IP Right Cessation
- 1975-06-05 NL NLAANVRAGE7506688,A patent/NL181926C/xx not_active IP Right Cessation
- 1975-06-05 US US05/584,271 patent/US4039567A/en not_active Expired - Lifetime
- 1975-06-05 FI FI751673A patent/FI62538C/fi not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| FI751673A (de) | 1975-12-06 |
| JPS5113725A (de) | 1976-02-03 |
| CA1051014A (en) | 1979-03-20 |
| DK142237C (da) | 1981-02-23 |
| NL181926C (nl) | 1987-12-01 |
| FI62538B (fi) | 1982-09-30 |
| ES438214A1 (es) | 1977-01-16 |
| NO145075B (no) | 1981-09-28 |
| DK251875A (da) | 1975-12-06 |
| NO145075C (no) | 1982-01-20 |
| DE2427085B2 (de) | 1976-07-01 |
| DK142237B (da) | 1980-09-29 |
| SE7506387L (sv) | 1975-12-08 |
| NL181926B (nl) | 1987-07-01 |
| ATA419775A (de) | 1976-06-15 |
| DE2427085A1 (de) | 1975-12-11 |
| NO751944L (de) | 1975-12-08 |
| AT334915B (de) | 1977-02-10 |
| GB1514197A (en) | 1978-06-14 |
| IT1035922B (it) | 1979-10-20 |
| CH615684A5 (de) | 1980-02-15 |
| NL7506688A (nl) | 1975-12-09 |
| AU8131075A (en) | 1976-11-25 |
| DD120024A5 (de) | 1976-05-20 |
| JPS6035351B2 (ja) | 1985-08-14 |
| FR2273812A1 (fr) | 1976-01-02 |
| SU619108A3 (ru) | 1978-08-05 |
| US4039567A (en) | 1977-08-02 |
| SE415181B (sv) | 1980-09-15 |
| FR2273812B1 (de) | 1978-10-13 |
| BE829853A (fr) | 1975-10-01 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| FI62538C (fi) | Foerfarande foer kontinuerlig framstaellning av alkoxisilaner | |
| US7507850B2 (en) | Preparation of organosilane esters | |
| JPH0549675B2 (de) | ||
| JP3616161B2 (ja) | オルガノオキシシランの製造方法 | |
| CN110799458B (zh) | 用于制备锗-硅-层的三苯基甲锗烷基甲硅烷和三氯甲硅烷基-三氯甲锗烷及其制备方法 | |
| US4228092A (en) | Process for the preparation of organoalkoxysilanes | |
| JPS62918B2 (de) | ||
| US6084116A (en) | Process for preparing acetoxysilanes | |
| EP1368359B1 (de) | Kontinuierliche umesterung von alkoxysilanen | |
| US4730074A (en) | Vapor phase alcoholysis of aminosilanes and carbamatosilanes | |
| US4173576A (en) | Process for the esterification of chlorosilanes | |
| US4958040A (en) | Process for the preparation of diorganohalogenosilanes | |
| US4824982A (en) | Method for the cleavage of organic siloxanes, and products and applications thereof | |
| US4417067A (en) | Method of cleaving organosiloxanes | |
| JP6906424B2 (ja) | アミノシラン類の製造方法 | |
| US5187291A (en) | Process for the simultaneous and continuous preparation of acyloxysilanes and carboxylic acid chlorides | |
| US4762938A (en) | Process for the preparation of alkoxysilanes | |
| US4421926A (en) | Process for co-alkoxylation of halosilanes and separation of the resulting products | |
| JP2797881B2 (ja) | ３−［ｎ−（２−アミノエチル）］アミノプロピルアルコキシシランの連続的製造方法及びその製造装置 | |
| RU2299213C1 (ru) | Способ получения алкоксисиланов | |
| JP2713676B2 (ja) | ３−［ｎ−（２−アミノエチル）］アミノプロピルアルコキシシランの製造方法とその製造装置 | |
| JPS5949228B2 (ja) | ハロゲンシランのエステル化法 | |
| AU2003217799A1 (en) | Preparation of mixed-halogen halo-silanes | |
| JPH11500131A (ja) | 有機シランの製造方法 | |
| RU2119491C1 (ru) | Способ выделения триметилхлорсилана из смеси с четыреххлористым кремнием |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MM | Patent lapsed |
Owner name: DYNAMIT NOBEL AKTIENGESELLSCHAFT |