EP3060522A4 - Procédés de préparation de carbonate de lithium - Google Patents

Procédés de préparation de carbonate de lithium

Info

Publication number
EP3060522A4
EP3060522A4 EP14854916.5A EP14854916A EP3060522A4 EP 3060522 A4 EP3060522 A4 EP 3060522A4 EP 14854916 A EP14854916 A EP 14854916A EP 3060522 A4 EP3060522 A4 EP 3060522A4
Authority
EP
European Patent Office
Prior art keywords
processes
lithium carbonate
preparing lithium
preparing
carbonate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP14854916.5A
Other languages
German (de)
English (en)
Other versions
EP3060522A1 (fr
EP3060522B1 (fr
Inventor
Guy Bourassa
Gary Pearse
Stephen Charles Mackie
Mykolas Gladkovas
Peter Symons
J David Genders
Jean-François Magnan
Geneviève Clayton
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nemaska Lithium Inc
Original Assignee
Nemaska Lithium Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nemaska Lithium Inc filed Critical Nemaska Lithium Inc
Publication of EP3060522A1 publication Critical patent/EP3060522A1/fr
Publication of EP3060522A4 publication Critical patent/EP3060522A4/fr
Application granted granted Critical
Publication of EP3060522B1 publication Critical patent/EP3060522B1/fr
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00—Lithium compounds
    • C01D15/08—Carbonates; Bicarbonates
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B26/00—Obtaining alkali, alkaline earth metals or magnesium
    • C22B26/10—Obtaining alkali metals
    • C22B26/12—Obtaining lithium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/42—Electrodialysis; Electro-osmosis ; Electro-ultrafiltration; Membrane capacitive deionization
    • B01D61/422—Electrodialysis
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/42—Electrodialysis; Electro-osmosis ; Electro-ultrafiltration; Membrane capacitive deionization
    • B01D61/44—Ion-selective electrodialysis
    • B01D61/445—Ion-selective electrodialysis with bipolar membranes; Water splitting
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D7/00—Carbonates of sodium, potassium or alkali metals in general
    • C01D7/07—Preparation from the hydroxides
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/44—Treatment or purification of solutions, e.g. obtained by leaching by chemical processes
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B4/00—Electrothermal treatment of ores or metallurgical products for obtaining metals or alloys
    • C22B4/02—Light metals
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B1/00—Electrolytic production of inorganic compounds or non-metals
    • C25B1/01—Products
    • C25B1/02—Hydrogen or oxygen
    • C25B1/04—Hydrogen or oxygen by electrolysis of water
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B1/00—Electrolytic production of inorganic compounds or non-metals
    • C25B1/01—Products
    • C25B1/14—Alkali metal compounds
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B1/00—Electrolytic production of inorganic compounds or non-metals
    • C25B1/01—Products
    • C25B1/14—Alkali metal compounds
    • C25B1/16—Hydroxides
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B13/00—Diaphragms; Spacing elements
    • C25B13/04—Diaphragms; Spacing elements characterised by the material
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B15/00—Operating or servicing cells
    • C25B15/02—Process control or regulation
    • C25B15/023—Measuring, analysing or testing during electrolytic production
    • C25B15/025—Measuring, analysing or testing during electrolytic production of electrolyte parameters
    • C25B15/027—Temperature
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B15/00—Operating or servicing cells
    • C25B15/02—Process control or regulation
    • C25B15/023—Measuring, analysing or testing during electrolytic production
    • C25B15/025—Measuring, analysing or testing during electrolytic production of electrolyte parameters
    • C25B15/029—Concentration
    • C25B15/031—Concentration pH
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B15/00—Operating or servicing cells
    • C25B15/08—Supplying or removing reactants or electrolytes; Regeneration of electrolytes
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B9/00—Cells or assemblies of cells; Constructional parts of cells; Assemblies of constructional parts, e.g. electrode-diaphragm assemblies; Process-related cell features
    • C25B9/17—Cells comprising dimensionally-stable non-movable electrodes; Assemblies of constructional parts thereof
    • C25B9/19—Cells comprising dimensionally-stable non-movable electrodes; Assemblies of constructional parts thereof with diaphragms
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B9/00—Cells or assemblies of cells; Constructional parts of cells; Assemblies of constructional parts, e.g. electrode-diaphragm assemblies; Process-related cell features
    • C25B9/17—Cells comprising dimensionally-stable non-movable electrodes; Assemblies of constructional parts thereof
    • C25B9/19—Cells comprising dimensionally-stable non-movable electrodes; Assemblies of constructional parts thereof with diaphragms
    • C25B9/21—Cells comprising dimensionally-stable non-movable electrodes; Assemblies of constructional parts thereof with diaphragms two or more diaphragms
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B9/00—Cells or assemblies of cells; Constructional parts of cells; Assemblies of constructional parts, e.g. electrode-diaphragm assemblies; Process-related cell features
    • C25B9/70—Assemblies comprising two or more cells
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2311/00—Details relating to membrane separation process operations and control
    • B01D2311/26—Further operations combined with membrane separation processes
    • B01D2311/2684—Electrochemical processes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02—Processes for making hydrogen or synthesis gas
    • C01B2203/0283—Processes for making hydrogen or synthesis gas containing a CO-shift step, i.e. a water gas shift step
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30—Hydrogen technology
    • Y02E60/36—Hydrogen production from non-carbon containing sources, e.g. by water electrolysis
EP14854916.5A 2013-10-23 2014-10-23 Procédés de préparation de carbonate de lithium Active EP3060522B1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US201361894655P 2013-10-23 2013-10-23
PCT/CA2014/000768 WO2015058287A1 (fr) 2013-10-23 2014-10-23 Procédés de préparation de carbonate de lithium

Publications (3)

Publication Number Publication Date
EP3060522A1 EP3060522A1 (fr) 2016-08-31
EP3060522A4 true EP3060522A4 (fr) 2016-12-28
EP3060522B1 EP3060522B1 (fr) 2019-06-12

Family

ID=52992081

Family Applications (1)

Application Number Title Priority Date Filing Date
EP14854916.5A Active EP3060522B1 (fr) 2013-10-23 2014-10-23 Procédés de préparation de carbonate de lithium

Country Status (10)

Country Link
US (3) US10144990B2 (fr)
EP (1) EP3060522B1 (fr)
JP (4) JP6335316B2 (fr)
KR (4) KR102195934B1 (fr)
CN (2) CN109250733B (fr)
AU (2) AU2014339705B2 (fr)
CA (3) CA2928224C (fr)
CL (1) CL2016000980A1 (fr)
DK (1) DK3060522T3 (fr)
WO (1) WO2015058287A1 (fr)

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CA2871092C (fr) 2012-04-23 2017-05-09 Nemaska Lithium Inc. Procedes de preparation d'hydroxyde de lithium
EP3363930B1 (fr) 2012-05-30 2024-03-13 Nemaska Lithium Inc. Procédés de préparation de carbonate lithium
US9695050B2 (en) 2012-11-02 2017-07-04 Terra Co2 Technologies Ltd. Methods and systems using electrochemical cells for processing metal sulfate compounds from mine waste and sequestering CO2
CA2944759A1 (fr) 2013-03-15 2014-09-18 Nemaska Lithium Inc. Procedes pour la preparation d'hydroxyde de lithium
EP3060699B1 (fr) 2013-10-23 2018-05-02 Nemaska Lithium Inc. Procédés et systèmes permettant de préparer de l'hydroxyde de lithium
CN109250733B (zh) * 2013-10-23 2021-07-16 内玛斯卡锂公司 制备碳酸锂的方法
WO2015123762A1 (fr) 2014-02-24 2015-08-27 Nemaska Lithium Inc. Procédés pour le traitement de matériaux contenant du lithium
EP3341330B1 (fr) 2015-08-27 2020-08-19 Nemaska Lithium Inc. Procédés pour le traitement de matériaux contenant du lithium
CL2015003609A1 (es) * 2015-12-11 2016-07-29 Propipe Maquinarias Ltda Sistema y proceso secuencial electrolitico para aumentar la concentración de litio presente en salmueras que reemplaza pozas o piscinas de evaporación y que evita la perdida de agua por evaporación, recupera una fracción como agua industrial y el resto la incorpora nuevamente a un salar
GB201602259D0 (en) 2016-02-08 2016-03-23 Bateman Advanced Technologies Ltd Integrated Lithium production process
EP3417082B1 (fr) * 2016-02-18 2022-10-26 Li-Technology Pty Ltd. Récupération de lithium à partir de minéraux de phosphate
US11289700B2 (en) 2016-06-28 2022-03-29 The Research Foundation For The State University Of New York KVOPO4 cathode for sodium ion batteries
CA2940509A1 (fr) * 2016-08-26 2018-02-26 Nemaska Lithium Inc. Procede de traitement de compositions aqueuses comprenant du sulfate de lithium et de l'acide sulfurique
CN106315629B (zh) * 2016-08-30 2018-01-30 山东瑞福锂业有限公司 一种利用电池级碳酸锂沉锂母液回收制备高纯碳酸锂的工艺
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KR101888181B1 (ko) * 2016-12-23 2018-08-13 주식회사 포스코 수산화리튬 및 탄산리튬의 제조방법
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CN106976894B (zh) * 2017-05-10 2018-10-23 东北大学 一种氯化锂电转化直接制备碳酸锂的方法
JP2020522621A (ja) * 2017-06-08 2020-07-30 アーバン マイニング プロプライエタリー リミテッド リチウムを回収する方法
CN107473242B (zh) * 2017-09-19 2019-03-05 江西赣锋锂业股份有限公司 一种利用碳酸锂制备高纯氧化锂的方法
CN107540005B (zh) * 2017-10-13 2019-03-22 山东鲁北企业集团总公司 一种连续沉锂槽及电池级碳酸锂连续沉锂工艺
EP3700866A4 (fr) * 2017-10-26 2021-05-19 International Battery Metals, Ltd. Appareil d'extraction modulaire
CN107640779A (zh) * 2017-11-15 2018-01-30 天元锂电材料河北有限公司 锂辉石制取碳酸锂工艺
CA3155660A1 (fr) 2017-11-22 2019-05-31 Nemaska Lithium Inc. Procedes de preparation d'hydroxydes et d'oxydes de divers metaux et leurs derives
DE102018005586A1 (de) 2018-07-17 2020-01-23 Manfred Koch Ein neuer integrierter Prozess für die Herstellung von Kathodenmaterial für Batterien
CN110451534A (zh) * 2018-08-06 2019-11-15 南方科技大学 一种锂盐的提纯装置、提纯系统和提纯方法
CN110817904B (zh) * 2018-08-14 2021-07-20 比亚迪股份有限公司 单水合氢氧化锂及其制备方法和用途以及锂离子电池正极材料和锂离子电池
CN109411742A (zh) * 2018-10-24 2019-03-01 浙江晨阳新材料有限公司 制备锂电池材料的方法
JP6533859B1 (ja) * 2018-10-29 2019-06-19 株式会社アサカ理研 炭酸リチウムの製造装置
CN115057569A (zh) * 2018-12-21 2022-09-16 曼格夫水科技有限公司 Li回收方法和现场生产用于Li回收方法的化学品
CN109650414B (zh) * 2019-01-18 2020-01-14 成都开飞高能化学工业有限公司 高杂质锂源制备电池级、高纯级的氢氧化锂和碳酸锂的方法及系统
WO2020159868A1 (fr) * 2019-01-28 2020-08-06 Richardson Robert George Séquestration chimique de co2, de nox et de so2
JP7051242B2 (ja) 2019-02-06 2022-04-11 株式会社タチエス 車両用ヘッドレスト
CN109761415A (zh) * 2019-02-19 2019-05-17 北京中科康仑环境科技研究院有限公司 一种碳酸氢铵沉钴废水的资源化处理工艺
CN109680295B (zh) * 2019-02-22 2019-11-22 北京廷润膜技术开发股份有限公司 一种工业级碳酸锂固体制备氢氧化锂的方法
EP3972937A4 (fr) * 2019-05-22 2023-07-26 Nemaska Lithium Inc. Procédés de préparation d'hydroxydes et d'oxydes de divers métaux et de leurs dérivés
CN110436679B (zh) * 2019-07-31 2023-12-29 杭州蓝然环境技术股份有限公司 碳酸锂洗水资源化综合利用的装置及其方法
KR102182845B1 (ko) * 2019-08-23 2020-11-25 부경대학교 산학협력단 황산리튬으로부터 탄산리튬 제조방법
CN110482763A (zh) * 2019-09-11 2019-11-22 北京中科瑞升资源环境技术有限公司 含盐废水的资源化耦合集成系统和资源化方法
CN112575339B (zh) * 2019-09-27 2022-04-15 天齐锂业（江苏）有限公司 锂辉石制备氢氧化锂的方法及去除钠钾的方法
KR102059858B1 (ko) * 2019-11-01 2019-12-27 한국지질자원연구원 염수로부터 리튬을 회수하는 방법
WO2021178748A1 (fr) * 2020-03-06 2021-09-10 The Board Of Regents Of The Nevada System Of Higher Education On Behalf Of The University Of Nevada, Las Vegas Récupération de lithium à partir de sels de lithium dissous dans des liquides ioniques
CN113694733B (zh) * 2020-05-20 2022-11-25 国家能源投资集团有限责任公司 一种基于双极膜电渗析装置的锂分离方法
KR102242686B1 (ko) 2020-12-14 2021-04-21 한국지질자원연구원 리튬농축액 제조방법 및 이로부터 제조된 리튬농축액을 이용한 리튬화합물 제조방법
WO2022133458A1 (fr) * 2020-12-16 2022-06-23 Battelle Energy Alliance, Llc Procédés de récupération de lithium à partir d'un matèriau contenant du lithium, et systèmes associés
CN113636578B (zh) * 2021-09-10 2023-05-26 宜春银锂新能源有限责任公司 一种锂云母制备碳酸锂提高品质的工艺
FR3139563A1 (fr) * 2022-09-08 2024-03-15 Eurodia Industrie Procédé de préparation d’hydroxyde de lithium, et installation pour la mise en œuvre du procédé
CN116837229B (zh) * 2023-08-31 2023-11-28 中国科学院过程工程研究所 一种基于流动电极电化学选择性提锂的系统及方法和应用

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