EP1337681A1 - Vorrichtung zur tauchbeschichtung eines metallstreifens - Google Patents

Vorrichtung zur tauchbeschichtung eines metallstreifens

Info

Publication number
EP1337681A1
EP1337681A1 EP01993714A EP01993714A EP1337681A1 EP 1337681 A1 EP1337681 A1 EP 1337681A1 EP 01993714 A EP01993714 A EP 01993714A EP 01993714 A EP01993714 A EP 01993714A EP 1337681 A1 EP1337681 A1 EP 1337681A1
Authority
EP
European Patent Office
Prior art keywords
sheath
strip
metal
bath
installation according
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP01993714A
Other languages
English (en)
French (fr)
Other versions
EP1337681B1 (de
Inventor
Didier Dauchelle
Hugues Baudin
Patrice Lucas
Laurent Gacher
Yves Prigent
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ArcelorMittal France SA
Original Assignee
Sollac SA
Lorraine de Laminage Continu SA SOLLAC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sollac SA, Lorraine de Laminage Continu SA SOLLAC filed Critical Sollac SA
Publication of EP1337681A1 publication Critical patent/EP1337681A1/de
Application granted granted Critical
Publication of EP1337681B1 publication Critical patent/EP1337681B1/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C2/00—Hot-dipping or immersion processes for applying the coating material in the molten state without affecting the shape; Apparatus therefor
    • C23C2/34—Hot-dipping or immersion processes for applying the coating material in the molten state without affecting the shape; Apparatus therefor characterised by the shape of the material to be treated
    • C23C2/36—Elongated material
    • C23C2/40—Plates; Strips
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C2/00—Hot-dipping or immersion processes for applying the coating material in the molten state without affecting the shape; Apparatus therefor
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C2/00—Hot-dipping or immersion processes for applying the coating material in the molten state without affecting the shape; Apparatus therefor
    • C23C2/003—Apparatus
    • C23C2/0034—Details related to elements immersed in bath
    • C23C2/00342—Moving elements, e.g. pumps or mixers
    • C23C2/00344—Means for moving substrates, e.g. immersed rollers or immersed bearings
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C2/00—Hot-dipping or immersion processes for applying the coating material in the molten state without affecting the shape; Apparatus therefor
    • C23C2/04—Hot-dipping or immersion processes for applying the coating material in the molten state without affecting the shape; Apparatus therefor characterised by the coating material
    • C23C2/06—Zinc or cadmium or alloys based thereon
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C2/00—Hot-dipping or immersion processes for applying the coating material in the molten state without affecting the shape; Apparatus therefor
    • C23C2/14—Removing excess of molten coatings; Controlling or regulating the coating thickness
    • C23C2/16—Removing excess of molten coatings; Controlling or regulating the coating thickness using fluids under pressure, e.g. air knives

Definitions

  • the present invention relates to an installation for hot-dip and continuous coating of a metal strip, in particular a steel strip.
  • steel sheets are used coated with a protective layer, for example against corrosion, and most often coated with a layer of zinc.
  • This type of sheet metal is used in various industries to produce all kinds of parts and in particular appearance parts.
  • this steel strip Before the steel strip passes through the molten metal bath, this steel strip first circulates in an annealing furnace under a reducing atmosphere in order to recrystallize it after the significant work hardening associated with the operation. cold rolling, and preparing its chemical surface state to promote the chemical reactions necessary for the actual quenching operation.
  • the steel strip is brought to around 650 to 900 ° C. depending on the shade during the time necessary for recrystallization and. to surface preparation. She is in-
  • the steel strip After passing through the annealing furnace, the steel strip passes through a sheath also called “bell descent” or “horn” under a protective atmosphere with respect to steel and is immersed in the bath of molten metal. The lower end of the sheath is immersed in the metal bath to determine, with the surface of said bath and inside this sheath, a liquid seal which is crossed by the steel strip as it travels in said sheath.
  • a sheath also called "bell descent” or “horn” under a protective atmosphere with respect to steel and is immersed in the bath of molten metal.
  • the lower end of the sheath is immersed in the metal bath to determine, with the surface of said bath and inside this sheath, a liquid seal which is crossed by the steel strip as it travels in said sheath.
  • the steel strip is deflected by a roller immersed in the metal bath and it emerges from this metal bath, then passes through wringing means serving to regulate the thickness of the coating of liquid metal on this strip of steel.
  • the surface of the liquid seal inside the sheath is generally covered with zinc oxide, resulting from the reaction between the atmosphere inside this sheath and the zinc of the liquid joint and solid intermetallic or matte compounds from the dissolution reaction of the steel strip.
  • These mattes or other particles in supersaturation in the zinc bath, have a density lower than that of liquid zinc and rise to the surface of the bath and in particular to the surface of the liquid seal.
  • the movement of the steel strip through the surface of the liquid seal causes entrainment of the stagnant particles.
  • These particles entrained by the movement of the liquid seal linked to the speed of the steel strip are not discharged into the volume of the bath and emerge in the zone of extraction of the strip, creating appearance defects.
  • the coated steel strip has appearance defects which are amplified, or even revealed during the zinc wringing operation.
  • a first solution to avoid these drawbacks is to clean the surface of the liquid seal by pumping zinc oxides and mattes from the bath.
  • a second solution consists in reducing the surface of the liquid seal at the point of passage of the steel strip by placing a sheet or ceramic plate at the level of this liquid seal to keep part of the particles away from the strip. on the surface and obtain a self-cleaning of the liquid seal by this strip.
  • this solution only partially treats the liquid seal and does not make it possible to achieve a very low density of defects satisfying the requirements of customers desiring surfaces without appearance defects.
  • a solution is also known which aims to obtain cleanliness of the liquid seal by renewing the molten metal bath.
  • the renewal is carried out by introducing liquid zinc pumped into the bath in the vicinity of the immersion zone of the steel strip.
  • the piping ensuring the renewal of the liquid zinc can cause scratches on the steel strip before its immersion and it is itself a source of defects by accumulation of condensed zinc vapors above the liquid joint.
  • the object of the invention is to propose an installation for continuous galvanizing of a metal strip which makes it possible to avoid the pre- previously mentioned and ' to reach the very low density of the defects satisfied. meeting the requirements of customers who want surfaces without appearance defects.
  • the subject of the invention is an installation for continuously dipping a metal strip, of the type comprising: a tank containing a bath of liquid metal,
  • sheath means for wringing off the coated metal strip, at the outlet from the metal bath, characterized in that the sheath is extended, at its lower part, by at least two internal walls each located on one side of the strip and directed towards the surface of the metal bath in said sheath to form at least two compartments for recovering particles of metal oxide and of intermetallic compounds and in that this sheath has a fixed upper part and a movable lower part connected together by a deformable element and means for positioning the movable lower part of this sheath relative to the metal strip.
  • the deformable element is formed by a bellows made of stainless steel
  • the positioning means comprise an actuating member connected to the movable lower part of the sheath to pivotally move this lower part about a transverse axis to the band and located at the bellows,
  • the positioning means comprise two actuating members connected to the movable lower part of the sheath to move this lower part by pivoting about an axis transverse to the strip and located at level of the bellows and / or in translation parallel to the surface of the liquid metal bath,
  • FIG. 1 is a schematic elevation view of a continuous tempering coating installation according to the invention
  • FIG. 2 is a schematic view on a larger scale of a first embodiment of the means for positioning the sheath of the installation according to the invention
  • FIG. 3 and 4 are two schematic views on a larger scale of a second embodiment of the means for positioning the sheath of the installation according to the invention
  • FIG. 5 and 6 are two schematic views showing two embodiments of the means for guiding the strip inside the sheath of the installation according to the invention.
  • the steel strip 1 passes through an annealing furnace, not shown, under a reducing atmosphere with a view to recrystallizing it " after the significant work hardening associated with rolling cold, and to prepare its surface chemical state in order to favor the chemical reactions necessary for the galvanizing operation.
  • the steel strip is brought to a temperature of, for example, between 650 and 900 ° C.
  • the steel strip 1 passes through a galvanizing installation shown in FIG. 1 and designated by the general reference 10.
  • This installation 10 comprises a tank 11 containing a bath 12 of liquid zinc which contains chemical elements such as aluminum, iron and possible addition elements such as lead, antimony, in particular.
  • the temperature of this liquid zinc bath is of the order of 460 ° C.
  • the steel strip 1 On leaving the annealing furnace, the steel strip 1 is cooled to a temperature close to that of the bath of liquid zinc using exchangers and is then immersed in the bath 12 of liquid zinc.
  • an Fe-Zn-AI intermetallic alloy is formed on the surface of the steel strip 1 producing a zinc coating, the thickness of which is a function of the residence time of the steel strip 1 in the bath 12 of liquid zinc.
  • the galvanizing installation 10 comprises a sheath 13 inside which the steel strip 1 runs under a protective atmosphere with respect to the steel.
  • This sheath '13 also called “bell down" or
  • “trompe” has, in the embodiment shown in the figures, a rectangular cross section.
  • the lower end of the sheath 13a is immersed in the zinc bath 12 so as to determine with the surface of said bath 12 and inside this sheath 13, a liquid seal 14.
  • the steel strip 1 is deflected by a roller 15 commonly called a bottom roller and placed in the zinc bath 12.
  • a roller 15 commonly called a bottom roller and placed in the zinc bath 12.
  • the coated steel strip 1 passes through wringing means 16 which are for example constituted by nozzles 16a for air projection and which are directed towards each face of the steel strip 1 to regulate the thickness of the coating of liquid zinc.
  • the lower end 13a of the sheath 13 is extended, on the opposite side of the face of the strip 1 situated on the side of the deflecting roller 15, by an internal wall 20 directed towards the surface of the liquid seal 14 and which protects with the sheath 13, a compartment 21 for discharge liquid zinc to collect particles of zinc oxides and intermetallic compounds which float on the surface of the liquid seal 14.
  • the upper edge 20a of the internal wall 20 is positioned below the surface of the liquid seal 14 and the compartment 21 is provided with means, not shown, for maintaining the level of liquid zinc in said compartment at a level below the surface of the liquid seal 14 to produce a natural flow of the liquid zinc from this surface of said seal 14 to this compartment 21.
  • the lower end 13a of the sheath 13 located opposite the face of the strip 1 placed opposite the. deflector roller 15, is extended by an internal wall 22 directed towards the surface of the liquid seal 14 and providing with the sheath 13 a sealed compartment 23 for storing zinc oxide particles.
  • the upper edge 22a of the internal wall 22 is positioned above the surface of the liquid seal 14.
  • this compartment 23 serves as a receptacle for zinc oxides which can come from the inclined lower wall of the sheath and makes it possible to store these oxides in order to protect the steel strip 1.
  • the upper edge 22a of the internal wall 22 can be positioned below the surface of the liquid seal 14 and, in this case, the compartment 23 is a compartment for discharging the liquid zinc, like the compartment 21.
  • the steel strip 1 must penetrate into the liquid zinc seal 14 without risking touching the walls 20 and 22 of the two compartments 21 and 23.
  • the line of passage of the steel strip 1 between the walls 20 and 22 of the two compartments 21 and 23 is determined by the diameter of the deflector roller 15 and by its position.
  • the sheath 13 has two parts, a fixed upper part 30 and a movable lower part 31, connected together by a deformable element 32 so as to be able to modify the position of the movable lower part 31 of the sheath 13.
  • the deformable element 32 is ' constituted by a bellows, for example made of stainless steel and the lower part 31 of the sheath 13 is associated with means 35 for positioning the internal walls 20 and 22 relative to the steel strip 1.
  • the positioning means 35 comprise an actuating member -35a constituted for example by a hydraulic or pneumatic cylinder and connected to the movable lower part 31 of the sheath 13 to pivotally move this lower part 31 around a virtual axis A transverse to the strip 1 and located at the bellows 32.
  • the angle of inclination of this lower part 31 can be modified as a function of the inclination of the strip of steel 1, as shown in dotted lines in FIG. 2.
  • the positioning means 35 comprise two actuating members, respectively 35a and 35b, constituted for example by hydraulic or pneumatic jacks and connected to the lower part 31 of the sheath 13.
  • the movable lower part 31 of the sheath 13 is moved in translation parallel to the surface of the liquid metal bath 12 when the displacement stroke of the actuating rods of said jacks is identical, as shown in Fig. 3.
  • the lower movable part 31 remains parallel to itself.
  • the position of the internal walls 20 and 22 of the compartments 21 and 23 is adjusted so that the steel strip 1 penetrates into the liquid zinc seal 14 determined by said internal walls 20 and 22 without risking touching these walls.
  • the installation comprises means 40 for guiding the steel strip 1 inside the sheath 13.
  • These guide means 40 are formed by a deflecting roller 41 or 42 placed in the sheath 13 to draw the line of passage of the steel strip 1 relative to the roller 15 and more easily adjust the passage of said steel strip 1 between the two walls 20 and 22 of the compartments 21 and 23.
  • the deflector roller 41 is disposed on the face of the strip 1 opposite to that in contact with the roller 15, as shown in Fig. 5, and in the case of a thicker steel strip 1, the deflector roller 42 is arranged on the face of the strip 1 in contact with the drive roller 15, as shown in FIG. 6.
  • the deflector roller 42 makes it possible to compensate for the bending of the steel strip 1 in the transverse direction which is linked to the deformation gradient of the fibers of the steel strip, in its thickness, on the rollers of the furnace. upstream of the galvanizing tank.
  • the invention applies to any metallic coating by dipping.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Coating With Molten Metal (AREA)
  • Coating Apparatus (AREA)
  • Laminated Bodies (AREA)
  • Electroplating Methods And Accessories (AREA)
  • Chemical Treatment Of Metals (AREA)
EP01993714A 2000-11-10 2001-11-07 Vorrichtung zur tauchbeschichtung eines metallstreifens Expired - Lifetime EP1337681B1 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR0014482 2000-11-10
FR0014482A FR2816637B1 (fr) 2000-11-10 2000-11-10 Installation de revetement au trempe d'une bande metallique
PCT/FR2001/003454 WO2002038823A1 (fr) 2000-11-10 2001-11-07 Installation de revetement au trempe d'une bande metallique

Publications (2)

Publication Number Publication Date
EP1337681A1 true EP1337681A1 (de) 2003-08-27
EP1337681B1 EP1337681B1 (de) 2008-01-02

Family

ID=8856313

Family Applications (1)

Application Number Title Priority Date Filing Date
EP01993714A Expired - Lifetime EP1337681B1 (de) 2000-11-10 2001-11-07 Vorrichtung zur tauchbeschichtung eines metallstreifens

Country Status (32)

Country Link
US (1) US6923864B2 (de)
EP (1) EP1337681B1 (de)
JP (1) JP3779272B2 (de)
KR (1) KR101144757B1 (de)
CN (1) CN1220787C (de)
AR (1) AR034182A1 (de)
AT (1) ATE382719T1 (de)
AU (2) AU2377602A (de)
BG (1) BG65317B1 (de)
BR (1) BR0100007B1 (de)
CA (1) CA2428486C (de)
CZ (1) CZ298884B6 (de)
DE (1) DE60132240T2 (de)
DK (1) DK1337681T5 (de)
EA (1) EA004334B1 (de)
EC (1) ECSP034592A (de)
EE (1) EE04821B1 (de)
ES (1) ES2296830T3 (de)
FR (1) FR2816637B1 (de)
HR (1) HRP20030364B1 (de)
HU (1) HUP0303550A2 (de)
MA (1) MA25854A1 (de)
ME (1) ME00793B (de)
MX (1) MXPA03004075A (de)
NO (1) NO20032088L (de)
PL (1) PL201515B1 (de)
PT (1) PT1337681E (de)
SK (1) SK286934B6 (de)
TW (1) TW554072B (de)
UA (1) UA74225C2 (de)
WO (1) WO2002038823A1 (de)
ZA (1) ZA200303501B (de)

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US20070036908A1 (en) * 2003-02-27 2007-02-15 Holger Behrens Method and device for melt dip coating metal strips, especially steel strips
KR100695948B1 (ko) * 2006-02-03 2007-03-16 문일호 구이용 팬
KR101353197B1 (ko) * 2011-10-25 2014-01-17 주식회사 포스코 강판 도금라인의 스나우트 장치
DE102013101131A1 (de) * 2013-02-05 2014-08-07 Thyssenkrupp Steel Europe Ag Vorrichtung zum Schmelztauchbeschichten von Metallband
DE102013104267B3 (de) 2013-04-26 2014-02-27 Thyssenkrupp Steel Europe Ag Vorrichtung zum kontinuierlichen Schmelztauchbeschichten von Metallband
KR101533212B1 (ko) * 2015-03-17 2015-07-01 최경철 스나우트의 댐 레벨 유지장치
WO2017187226A1 (fr) * 2016-04-26 2017-11-02 Arcelormittal Installation de revêtement au trempé à chaud et en continu d'une bande métallique et procédé associé
WO2017187225A1 (fr) * 2016-04-26 2017-11-02 Arcelormittal Installation de revêtement au trempé à chaud et en continu d'une bande métallique et procédé associé
WO2018228661A1 (de) * 2017-06-12 2018-12-20 Thyssenkrupp Steel Europe Ag Rüssel für eine schmelztauchbeschichtungsanlage sowie verfahren für dessen betrieb
KR101999029B1 (ko) * 2017-12-26 2019-07-10 주식회사 포스코 도금 스나우트
WO2019224584A1 (en) * 2018-05-25 2019-11-28 Arcelormittal Method for dip-coating a metal strip
FR3105796B1 (fr) * 2019-12-26 2022-06-10 Fives Stein Dispositif pour l’evacuation de mattes de la surface d’un bain de metal liquide a l’interieur d’une descente de cloche d’une ligne de revetement en continu d’une bande metallique
US11898251B2 (en) * 2020-05-22 2024-02-13 Cleveland-Cliffs Steel Properties Inc. Snout for use in a hot dip coating line
MX2022014521A (es) 2020-05-22 2022-12-13 Cleveland Cliffs Steel Properties Inc Pico de vertido para usarse en una linea de inmersion en caliente.
CN114107863B (zh) * 2021-11-19 2023-08-18 武汉钢铁有限公司 一种能减少锌液挂渣的炉鼻子装置
CN118321091B (zh) * 2024-06-17 2024-09-17 江苏荣明不锈钢有限公司 一种钢丝浸涂机

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Also Published As

Publication number Publication date
DK1337681T5 (da) 2008-05-13
ZA200303501B (en) 2003-11-13
ME00793B (me) 2012-03-20
US6923864B2 (en) 2005-08-02
BR0100007A (pt) 2002-07-09
EE200300210A (et) 2003-08-15
TW554072B (en) 2003-09-21
CZ20031292A3 (cs) 2004-01-14
JP2004513237A (ja) 2004-04-30
EA200300551A1 (ru) 2003-10-30
HRP20030364A2 (en) 2003-06-30
KR20030048121A (ko) 2003-06-18
MA25854A1 (fr) 2003-07-01
SK286934B6 (sk) 2009-07-06
AU2002223776B2 (en) 2006-01-05
ATE382719T1 (de) 2008-01-15
BR0100007B1 (pt) 2012-10-02
CA2428486C (fr) 2009-04-07
US20040028832A1 (en) 2004-02-12
MXPA03004075A (es) 2004-04-20
CN1220787C (zh) 2005-09-28
BG65317B1 (bg) 2008-01-31
WO2002038823A1 (fr) 2002-05-16
EA004334B1 (ru) 2004-04-29
CN1473205A (zh) 2004-02-04
SK5102003A3 (en) 2003-12-02
PL362471A1 (en) 2004-11-02
NO20032088L (no) 2003-07-08
DE60132240T2 (de) 2009-04-16
CZ298884B6 (cs) 2008-03-05
UA74225C2 (uk) 2005-11-15
BG107777A (en) 2004-01-30
FR2816637A1 (fr) 2002-05-17
ECSP034592A (es) 2003-09-24
CA2428486A1 (fr) 2002-05-16
PL201515B1 (pl) 2009-04-30
HUP0303550A2 (en) 2004-03-01
JP3779272B2 (ja) 2006-05-24
DE60132240D1 (de) 2008-02-14
AU2377602A (en) 2002-05-21
HRP20030364B1 (en) 2008-11-30
ES2296830T3 (es) 2008-05-01
EE04821B1 (et) 2007-04-16
EP1337681B1 (de) 2008-01-02
KR101144757B1 (ko) 2012-05-21
DK1337681T3 (da) 2008-03-17
AR034182A1 (es) 2004-02-04
FR2816637B1 (fr) 2003-10-24
NO20032088D0 (no) 2003-05-09
PT1337681E (pt) 2008-02-21

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