EP0510291B2 - Verfahren und Vorrichtung zur Herstellung von Aluminiumdosen mit Gewinde - Google Patents
Verfahren und Vorrichtung zur Herstellung von Aluminiumdosen mit Gewinde Download PDFInfo
- Publication number
- EP0510291B2 EP0510291B2 EP91810599A EP91810599A EP0510291B2 EP 0510291 B2 EP0510291 B2 EP 0510291B2 EP 91810599 A EP91810599 A EP 91810599A EP 91810599 A EP91810599 A EP 91810599A EP 0510291 B2 EP0510291 B2 EP 0510291B2
- Authority
- EP
- European Patent Office
- Prior art keywords
- thread
- neck
- rolling
- tools
- roll
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 title claims abstract description 22
- 229910052782 aluminium Inorganic materials 0.000 title claims abstract description 22
- 239000004411 aluminium Substances 0.000 title claims abstract 4
- 238000000034 method Methods 0.000 title claims description 44
- 238000004519 manufacturing process Methods 0.000 title claims description 9
- 238000005096 rolling process Methods 0.000 claims abstract description 30
- 239000000463 material Substances 0.000 claims abstract description 15
- 239000000314 lubricant Substances 0.000 claims abstract description 6
- 239000003054 catalyst Substances 0.000 claims abstract 2
- 239000000654 additive Substances 0.000 claims description 3
- 238000005520 cutting process Methods 0.000 claims description 3
- 239000002966 varnish Substances 0.000 claims description 2
- 238000010409 ironing Methods 0.000 claims 1
- 238000000576 coating method Methods 0.000 abstract description 3
- 239000004014 plasticizer Substances 0.000 abstract description 2
- 239000011248 coating agent Substances 0.000 abstract 2
- 210000003739 neck Anatomy 0.000 description 60
- 239000003973 paint Substances 0.000 description 15
- 238000003780 insertion Methods 0.000 description 4
- 230000037431 insertion Effects 0.000 description 4
- 238000010422 painting Methods 0.000 description 4
- 238000001125 extrusion Methods 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- 229910000838 Al alloy Inorganic materials 0.000 description 1
- 239000004593 Epoxy Substances 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 239000000443 aerosol Substances 0.000 description 1
- 239000011324 bead Substances 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 239000004922 lacquer Substances 0.000 description 1
- 239000005022 packaging material Substances 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 239000013641 positive control Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21D—WORKING OR PROCESSING OF SHEET METAL OR METAL TUBES, RODS OR PROFILES WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21D51/00—Making hollow objects
- B21D51/16—Making hollow objects characterised by the use of the objects
- B21D51/38—Making inlet or outlet arrangements of cans, tins, baths, bottles, or other vessels; Making can ends; Making closures
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21D—WORKING OR PROCESSING OF SHEET METAL OR METAL TUBES, RODS OR PROFILES WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21D51/00—Making hollow objects
- B21D51/16—Making hollow objects characterised by the use of the objects
- B21D51/24—Making hollow objects characterised by the use of the objects high-pressure containers, e.g. boilers, bottles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21H—MAKING PARTICULAR METAL OBJECTS BY ROLLING, e.g. SCREWS, WHEELS, RINGS, BARRELS, BALLS
- B21H3/00—Making helical bodies or bodies having parts of helical shape
- B21H3/02—Making helical bodies or bodies having parts of helical shape external screw-threads ; Making dies for thread rolling
- B21H3/04—Making by means of profiled-rolls or die rolls
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D1/00—Containers having bodies formed in one piece, e.g. by casting metallic material, by moulding plastics, by blowing vitreous material, by throwing ceramic material, by moulding pulped fibrous material, by deep-drawing operations performed on sheet material
- B65D1/02—Bottles or similar containers with necks or like restricted apertures, designed for pouring contents
- B65D1/0223—Bottles or similar containers with necks or like restricted apertures, designed for pouring contents characterised by shape
- B65D1/023—Neck construction
- B65D1/0246—Closure retaining means, e.g. beads, screw-threads
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D1/00—Containers having bodies formed in one piece, e.g. by casting metallic material, by moulding plastics, by blowing vitreous material, by throwing ceramic material, by moulding pulped fibrous material, by deep-drawing operations performed on sheet material
- B65D1/22—Boxes or like containers with side walls of substantial depth for enclosing contents
- B65D1/26—Thin-walled containers, e.g. formed by deep-drawing operations
Definitions
- the invention relates to a method and a device according to the preambles of the corresponding independent claims for the production of Aluminum cans with threads, especially deep-drawn, deep-drawn and stretched or extruded, aluminum cans painted inside and out with bottle thread.
- aluminum is a good and cheap recyclable packaging material, would be it makes sense and desirable if made from aluminum containers could be on the like on plastic or glass bottles for example screwed on a hand pump with a riser pipe or a screw cap could be.
- the aluminum container could be filled with, for example the screw cap come on the market.
- the consumer the pump, which would be designed for multiple use, could simply be Screw the aluminum container on and off and the container without Recycle or refill foreign material.
- To this Purposes would be aluminum cans with appropriate threads, advantageously standardized threads necessary.
- the task is therefore to demonstrate a method and a device to create with those on the inside and externally painted aluminum cans thread, especially standardized thread, can be attached. It is particularly important that the paint, especially the inner varnish is not injured by attaching the thread will, because in the above-described task of such a can Internal threads are in contact with the contents of the can.
- Procedure and Device are said to be in known production lines for the manufacture of deep-drawn, deep-drawn and ironed or extruded, lacquered Aluminum cans can be integrated, i.e. the thread must be made can be in the same setup in which the other work steps like pulling in the neck, cutting the can to length, etc. in a cycle time of approx.
- the cans should be after the application the thread does not need to be cleaned, that is, process and device must do without the addition of lubricant or that a lubricant is used that does not contain the contents of the can or Appearance of the can impaired.
- the thread is made by a rolling on the outer neck side Tool and a quasi stationary one that supports the can material from the inside Tool created on the inside of the neck.
- the two tools work so positively controlled that there is slippage between the neck and the tool arises. This can largely prevent the neck material dammed up in front of the tools and in the direction of movement of the tools is shifted, which lead to oval threads and the paint in would claim and damage to a great extent.
- Figure 1 shows the basic method steps of the inventive method.
- the process is shown as a process block diagram and below it schematically the shape changes produced by the individual process steps on the can, namely as a top view and as a longitudinal section through the neck part of the can.
- A painted inside and out and possibly printed, as long as it have a cylindrical shape.
- the paints used are, for example Polyester or epoxy phenolic lacquers. You are going for increased flexibility, for increased adhesion and for better sliding properties with one or several additives that the expert as plasticizers, and Lubricants are known.
- the devices used for painting correspond to known such devices with which the Spraying the interior paint, the exterior paint with a corresponding roller is applied. After painting, the paints are dried accordingly and polymerized.
- the cans are placed on a turntable stretched, by gradually turning them into the area of successive Tools are guided, which are mounted on a tool plate are.
- a corresponding device is for example in the CH patent 394'998 / 65 (Lechner) and is assumed to be known.
- each can is drawn in in stages, the two process steps depending on the diameter of the can, depending on the desired can shape and depending on the material, consisting of different numbers of effective drawing-in steps with different tools.
- the first time B is pulled in the can has a narrowing shoulder and a substantially cylindrical first neck piece 10
- the second time it is pulled in C a second, narrower, essentially cylindrical neck piece 20 is connected to the first neck piece 10.
- the outside diameter d 1 of the first neck piece 10 essentially corresponds to the outside diameter of the thread to be created
- the outside diameter d 2 of the second narrower neck piece 20 is slightly smaller than the core diameter d 3 of the thread to be created.
- the shape of the retracted shoulder is for the inventive method Not relevant.
- Procedures and tools for pulling in aluminum cans are the same Known specialist. He can also use it for feeding to the one described Adapt the neck shape so that it is not described here Need to become.
- a thread 30 is rolled up on the first neck piece 10 or on the part of the first neck piece 10 facing the second neck piece 20.
- the thread is produced by a thread roll rolling around the outer circumference of the first neck piece 10, which is pressed against a quasi-stationary thread template in the interior of the neck. The thread is therefore pressed inwards from the outside of the neck so that the outside diameter of the finished rolled thread corresponds to the original neck diameter d 1 .
- Its core diameter d 3 is a little larger than the outer diameter d 2 of the second neck piece 20.
- the thread runs against the second neck piece 20, that is, it extends not to the edge of the neck. This prevents the neck edge deformed by the thread rolling from their exactly circular cylindrical shape becomes.
- the can neck is cut to length, for example immediately above the upper outlet of the thread.
- the connection between the neck edge and the pump connection must be tight.
- the type of seal used can be advantageous to the face of the can neck straight or slightly crooked. Methods and devices to cut can necks are known and must therefore not be described here.
- Figures 2a and b now show a top view in detail of the method and the tools that are used to roll the thread.
- Figure 2a shows the tools before the thread rolling process, Figure 2b during the thread rolling process.
- annular end face 21 of the second neck piece 20 with the outside diameter d 2 and the first neck piece 10 with the outside diameter d 1 are shown.
- an essentially cylindrical or slightly frustoconical thread template 40 is inserted into the doser neck.
- the largest diameter of the template is such that it can be inserted through the second neck piece 20 without difficulty.
- the template On its side surface, the template carries a slightly distorted, negative image 41 of the thread to be rolled, which is indicated by dashed lines in this top view.
- the can neck and the template are arranged coaxially, that is, their axes of rotation S and T coincide.
- a thread form formed as spiral around the roll pulling bead 51
- Thread roll spaced from the neck so that it does not touch it.
- the template 40 and the Thread roll 50 by shifting their axes T and U against each other moves that the template 40 where the thread roll 50 outside is positioned, touches the inner surface of the first neck piece and the Thread form 51 of the thread roll 50 around the thread depth of the roll Thread is pressed into the neck material.
- the thread roll 50 rolled on the neck and thus coordinates the axis of rotation the template rotated about the axis of rotation of the can so that the template always rests against the neck and supports the neck material where the thread roll just rolls.
- the two tools are at least moved once around the can neck and created the thread.
- the template 40 and thread roll 50 brought back into the position described for the insertion (Fig. 2a) and axially away from the can.
- the thread roll 50 When the thread rolls, the thread roll 50 is positively controlled in this way unrolled that the circumferential distance rolled on the roll is greater than that circumferential stretch rolled on the neck. Between thread roll and neck This creates a slip, so that the thread roll is in one Direction rolls over the neck circumference, but always in the opposite direction Direction slips on the neck surface. Through this Slip through which a force counteracts the direction of movement of the thread roll 50 arises on the neck material, the role is prevented Neck material in front of it and shifted in the unwinding direction.
- FIGS. 3a and 3b show, corresponding to FIGS . 2a and 2b, the tools used for the thread rolling process before (FIG. 3a) and during (FIG. 3b) the thread rolling process, namely as a section along the axis of rotation of the can, with only one side of the can neck is shown.
- the threads 41 of the thread template need only correspond to the shape of the finished thread in depth and pitch, but should not have any sharp edges where they come into contact with the deformed inner surface.
- the thread shape 51 of the thread roll 50 must correspond in shape to the shape of the thread to be created.
- the thread template 40 is advantageously designed such that it not only supports the inner surface of the first neck piece 10, but also at least partially the inner surface of the second neck piece 20, although no thread is rolled thereon.
- FIG. 4 schematically shows the parts of a device for thread rolling on cans relevant to the invention in an exemplary embodiment.
- the figure is a section along the axis of rotation S of the can.
- the two neck pieces 10 and 20 are visible from the can.
- the thread template 40 and the thread roller 50 are in a position which corresponds to their position in FIGS. 2b and 3b.
- the axis T of the template 40 is not on the axis of rotation S of the can, the thread roller 50 presses into the neck material.
- the means 60 are shown, by means of which the slip between the thread roll 50 and the can neck is produced. These are around a ring gear 61 which is attached to the shaft 42 of the template 40, and a second ring gear 62 running in this ring gear 61, which the thread roll 50 is attached. Now the axis U of the thread roll 50 moves about the axis T of the template 40, the thread roll rolls by the toothed drive 60 from the can neck under positive control. Since the Rolling radius r of the thread roll 50 on the can neck is smaller than that Rolling radius R of the ring gear 61 arises between the thread roll 50 and Can slip in such a way that the thread roll 50 on the Neck material slips against its direction of drainage.
- the drives for the axial movement of the are not shown in the figure Device parts before and after the effective thread rolling process and for the rotational movement of the thread roll 50 around the can neck and with it coupled circular movement of the axis T.
- the axial movement advantageously the clocked movement of the tool plate, on the too the tools for the other process steps are assembled, used.
- the circular movement of the thread roll is, for example, with a belt drive driven.
- the coupling of the movement of the thread roll 50 and the axis T of the Template 40 and the control of the relative movement of the two axes T and U before and after the effective thread rolling process can be done by appropriate asymmetrical wedge arrangements can be realized, the relative movement of the two axes by a relative movement in the axial Direction of these wedge arrangements is realized.
- the movement of the axis T about the axis S can be realized in such a way that the axis T describes a cylinder jacket around the axis S, or that the axis T describes a cone about the axis S.
- the template 40 In the event of cylinder movement the template 40 must be cylindrical, in the event of taper movement the template 40 must be frustoconical, with in the Can pointing tapered end be designed.
- FIG. 5 shows a can closed with a hand pump 70, to which a thread was attached using the method according to the invention.
- the thread can correspond to any standard for such threads, for example the Euronorm. It can be seen that threads which are produced by the method according to the invention have an accuracy of approximately ⁇ 0.1 mm, an accuracy which far exceeds the accuracy of corresponding plastic or glass threads. For this reason, it is also not necessary, as shown in FIG. 5, to improve the centering of the screwed-on pump by means of a corresponding recess on the end of the can neck facing the shoulder.
- the shape of the can base is not relevant for the method according to the invention.
- the can shown has, for example, an inwardly curved base.
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Ceramic Engineering (AREA)
- Containers Having Bodies Formed In One Piece (AREA)
- Chemical Treatment Of Metals (AREA)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH1149/91 | 1991-04-17 | ||
CH114991 | 1991-04-17 | ||
CH114991 | 1991-04-17 |
Publications (3)
Publication Number | Publication Date |
---|---|
EP0510291A1 EP0510291A1 (de) | 1992-10-28 |
EP0510291B1 EP0510291B1 (de) | 1995-03-08 |
EP0510291B2 true EP0510291B2 (de) | 2000-04-26 |
Family
ID=4203635
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP91810599A Expired - Lifetime EP0510291B2 (de) | 1991-04-17 | 1991-07-26 | Verfahren und Vorrichtung zur Herstellung von Aluminiumdosen mit Gewinde |
Country Status (6)
Country | Link |
---|---|
US (1) | US5293765A (ja) |
EP (1) | EP0510291B2 (ja) |
JP (1) | JP3375661B2 (ja) |
AT (1) | ATE119441T1 (ja) |
DE (1) | DE59104891D1 (ja) |
ES (1) | ES2073722T5 (ja) |
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FR2729316A1 (fr) * | 1995-01-18 | 1996-07-19 | Metal Box Plc | Procede de conformation d'un corps de boite cylindrique destine a recevoir un couvercle vissant |
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CN104289643A (zh) * | 2013-07-15 | 2015-01-21 | 上海万盛保温容器有限公司 | 保温容器筒身滚压螺纹的制作工艺及设备 |
USD739732S1 (en) | 2013-10-03 | 2015-09-29 | Anheuser-Busch, Llc | Metal beverage bottle |
USD739731S1 (en) | 2013-10-03 | 2015-09-29 | Anheuser-Busch, Llc | Metal beverage bottle |
CA2938867A1 (en) | 2014-02-07 | 2015-08-13 | Ball Corporation | Metallic container with a threaded closure |
FR3019148B1 (fr) * | 2014-03-26 | 2016-03-25 | Ardagh Mp West France | Contenant metallique comportant un goulot adapte a recevoir un element d'obturation du type capsule a vis |
EP3633053A1 (en) | 2014-04-30 | 2020-04-08 | Alcoa USA Corp. | Method of manufacturing an aluminum container made from aluminum sheet |
WO2017007610A1 (en) * | 2015-07-06 | 2017-01-12 | Novelis Inc. | Process to manufacture large format aluminum bottles and aluminium bottle manufactured thereby |
CN105344896A (zh) * | 2015-12-03 | 2016-02-24 | 绵阳祥泰科技有限责任公司 | 滚压螺纹模具的改进结构 |
CN105363976A (zh) * | 2015-12-03 | 2016-03-02 | 绵阳祥泰科技有限责任公司 | 安装牢固的螺纹模具 |
US20180044155A1 (en) | 2016-08-12 | 2018-02-15 | Ball Corporation | Apparatus and Methods of Capping Metallic Bottles |
CA3177802A1 (en) | 2016-12-30 | 2018-07-05 | Ball Corporation | Aluminum alloy for impact extruded containers and method of making the same |
CA3053478C (en) | 2017-02-16 | 2021-11-09 | Ball Corporation | Apparatus and methods of forming and applying roll-on pilfer proof closures on the threaded neck of metal containers |
DE202017103121U1 (de) * | 2017-05-23 | 2017-06-22 | Constantia Teich Gmbh | Tiefgezogene Schale, insbesondere Aluminiumschale |
JP7046163B2 (ja) | 2017-09-15 | 2022-04-01 | ボール コーポレイション | ネジ付き容器用の金属栓を形成する装置及び方法 |
JP7048361B2 (ja) | 2018-03-12 | 2022-04-05 | 大和製罐株式会社 | ネジ付きボトル型缶およびその製造方法 |
MX2021005230A (es) | 2018-11-05 | 2021-06-18 | Ball Corp | Recipiente metalico con una tapa roscada. |
CA3143701A1 (en) | 2019-06-26 | 2020-12-30 | Ball Corporation | A method and apparatus for sealing a metallic container with a metallic end closure |
US11767152B2 (en) | 2021-06-29 | 2023-09-26 | Iv Thought Products And Design Corp. | Re-sealing vacuum package receptacle |
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US2145587A (en) * | 1937-12-27 | 1939-01-31 | Draper Mfg Co | Thread swaging apparatus |
DE1189044B (de) * | 1961-01-12 | 1965-03-18 | Rudolf Lechner K G Tubenfabrik | Verfahren zur Herstellung nahtloser Metallflaschen |
US3832962A (en) * | 1971-08-23 | 1974-09-03 | Aluminum Co Of America | Precoating of aluminum can sheet |
BE795322A (fr) * | 1972-02-21 | 1973-05-29 | Vyzk Ustav Mech | Machine multi-operation a mouvement circulaire |
GB1445758A (en) * | 1973-11-29 | 1976-08-11 | Hutogepgyar | Method of and apparatus for thread rolling |
JPS56172533U (ja) * | 1980-05-23 | 1981-12-19 | ||
JPS5790877U (ja) * | 1980-11-26 | 1982-06-04 | ||
JPS57190740A (en) * | 1981-05-18 | 1982-11-24 | Sakura Kankougiyou Kk | Manufacture of can end plate |
DD204046A1 (de) * | 1982-03-26 | 1983-11-16 | Manfred Huettig | Vorrichtung zum stirnseitigen umformen von duennwandigen gesickten zylindrischen werkstuecken |
JPS61217353A (ja) * | 1985-03-14 | 1986-09-26 | 東洋製罐株式会社 | 耐ブリスタ−性に優れた加熱殺菌用内面塗装エアゾ−ル缶 |
JPH0117375Y2 (ja) * | 1986-11-26 | 1989-05-19 | ||
JPH0822636B2 (ja) * | 1987-06-12 | 1996-03-06 | 武内プレス工業株式会社 | フェルトペンの胴体及びその製造方法 |
JPH01210136A (ja) * | 1988-02-17 | 1989-08-23 | Terumo Corp | アルミニウム缶の製造方法 |
JPH01228567A (ja) * | 1988-03-09 | 1989-09-12 | Toyo Seikan Kaisha Ltd | エアゾール缶及びエアゾール缶用天地蓋 |
FR2649359B1 (fr) * | 1989-07-06 | 1993-02-12 | Cebal | Bande ou portion de bande pour emboutissage ou emboutissage-etirage, et son utilisation |
-
1991
- 1991-07-26 EP EP91810599A patent/EP0510291B2/de not_active Expired - Lifetime
- 1991-07-26 DE DE59104891T patent/DE59104891D1/de not_active Expired - Fee Related
- 1991-07-26 AT AT91810599T patent/ATE119441T1/de not_active IP Right Cessation
- 1991-07-26 ES ES91810599T patent/ES2073722T5/es not_active Expired - Lifetime
-
1992
- 1992-04-16 US US07/869,296 patent/US5293765A/en not_active Expired - Fee Related
- 1992-04-17 JP JP12558592A patent/JP3375661B2/ja not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
EP0510291A1 (de) | 1992-10-28 |
DE59104891D1 (de) | 1995-04-13 |
EP0510291B1 (de) | 1995-03-08 |
JPH05229545A (ja) | 1993-09-07 |
US5293765A (en) | 1994-03-15 |
JP3375661B2 (ja) | 2003-02-10 |
ES2073722T3 (es) | 1995-08-16 |
ATE119441T1 (de) | 1995-03-15 |
ES2073722T5 (es) | 2000-11-01 |
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