EA200870372A1 - Устройство и способы для производства соединений металлов - Google Patents

Устройство и способы для производства соединений металлов

Info

Publication number
EA200870372A1
EA200870372A1 EA200870372A EA200870372A EA200870372A1 EA 200870372 A1 EA200870372 A1 EA 200870372A1 EA 200870372 A EA200870372 A EA 200870372A EA 200870372 A EA200870372 A EA 200870372A EA 200870372 A1 EA200870372 A1 EA 200870372A1
Authority
EA
Eurasian Patent Office
Prior art keywords
aluminum
titanium
production
mixture
compounds
Prior art date
Application number
EA200870372A
Other languages
English (en)
Other versions
EA014894B1 (ru
Inventor
Джавад Хайдар
Сабаратнасингам Гнарараджан
Джон Бертон Данлоп
Original Assignee
Коммонвелт Сайнтифик Энд Индастриэл Рисерч Организэйшн
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from AU2006901558A external-priority patent/AU2006901558A0/en
Application filed by Коммонвелт Сайнтифик Энд Индастриэл Рисерч Организэйшн filed Critical Коммонвелт Сайнтифик Энд Индастриэл Рисерч Организэйшн
Publication of EA200870372A1 publication Critical patent/EA200870372A1/ru
Publication of EA014894B1 publication Critical patent/EA014894B1/ru

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00—Obtaining refractory metals
    • C22B34/10—Obtaining titanium, zirconium or hafnium
    • C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
    • C22B34/1263—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction
    • C22B34/1268—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams
    • C22B34/1272—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams reduction of titanium halides, e.g. Kroll process
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/16—Making metallic powder or suspensions thereof using chemical processes
    • B22F9/18—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
    • B22F9/28—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from gaseous metal compounds
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00—Obtaining refractory metals
    • C22B34/10—Obtaining titanium, zirconium or hafnium
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00—Obtaining refractory metals
    • C22B34/10—Obtaining titanium, zirconium or hafnium
    • C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00—Obtaining refractory metals
    • C22B34/10—Obtaining titanium, zirconium or hafnium
    • C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
    • C22B34/1263—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction
    • C22B34/1277—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using other metals, e.g. Al, Si, Mn
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B5/00—General methods of reducing to metals
    • C22B5/02—Dry methods smelting of sulfides or formation of mattes
    • C22B5/04—Dry methods smelting of sulfides or formation of mattes by aluminium, other metals or silicon
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B5/00—General methods of reducing to metals
    • C22B5/02—Dry methods smelting of sulfides or formation of mattes
    • C22B5/18—Reducing step-by-step
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C1/00—Making non-ferrous alloys
    • C22C1/04—Making non-ferrous alloys by powder metallurgy
    • C22C1/047—Making non-ferrous alloys by powder metallurgy comprising intermetallic compounds
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C14/00—Alloys based on titanium
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B21/00—Obtaining aluminium
    • C22B21/0038—Obtaining aluminium by other processes
    • C22B21/0046—Obtaining aluminium by other processes from aluminium halides
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B4/00—Electrothermal treatment of ores or metallurgical products for obtaining metals or alloys
    • C22B4/06—Alloys

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)

Abstract

Настоящее изобретение относится к поэтапному способу производства соединений титана-алюминия и некоторых титановых сплавов, а также интерметаллидных соединений и сплавов титана-алюминия. На первом этапе некоторое количество алюминия смешивают с некоторым количеством хлорида алюминия (AlCl), а затем к этой смеси добавляют некоторое количество хлорида титана (TiCl). Смесь нагревают до температуры менее 220°С с образованием продукта TiCl, алюминия и AlCl. На втором этапе, причем при необходимости можно добавить еще алюминий, смесь снова нагревают до температуры выше 900°С с образованием соединений титана-алюминия. Этот способ обеспечивает в результате производство порошковых форм соединений титана-алюминия с контролируемым составом. Также описано подходящее устройство реактора.
EA200870372A 2006-03-27 2007-03-27 Устройство и способ для производства соединений металлов EA014894B1 (ru)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
AU2006901558A AU2006901558A0 (en) 2006-03-27 Apparatus and methods for the production of metal compounds
PCT/AU2007/000385 WO2007109847A1 (en) 2006-03-27 2007-03-27 Apparatus and methods for the production of metal compounds

Publications (2)

Publication Number Publication Date
EA200870372A1 true EA200870372A1 (ru) 2009-02-27
EA014894B1 EA014894B1 (ru) 2011-02-28

Family

ID=38540718

Family Applications (1)

Application Number Title Priority Date Filing Date
EA200870372A EA014894B1 (ru) 2006-03-27 2007-03-27 Устройство и способ для производства соединений металлов

Country Status (11)

Country Link
US (1) US8821612B2 (ru)
EP (1) EP1999285B1 (ru)
JP (2) JP5479886B2 (ru)
KR (1) KR101399803B1 (ru)
CN (1) CN101454467B (ru)
AU (1) AU2007231543B2 (ru)
CA (1) CA2644430C (ru)
EA (1) EA014894B1 (ru)
ES (1) ES2394851T3 (ru)
UA (1) UA91908C2 (ru)
WO (1) WO2007109847A1 (ru)

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EA010932B1 (ru) * 2003-07-04 2008-12-30 Коммонвелт Сайентифик Энд Индастриал Рисерч Организейшн Способ и устройство для получения металлических соединений
UA91908C2 (ru) 2006-03-27 2010-09-10 Коммонвелт Сайентифик Энд Индастриал Рисерч Организейшн Способ и устройство для производства соединений металлов
WO2009129570A1 (en) * 2008-04-21 2009-10-29 Commonwealth Scientific And Industrial Research Organisation Method and apparatus for forming titanium-aluminium based alloys
CA2784196C (en) 2009-12-18 2019-12-10 Jawad Haidar Method for producing low aluminium titanium-aluminium alloys
CA2794425A1 (en) * 2010-02-25 2011-09-01 Csir Titanium powder production process
US10035078B2 (en) * 2010-05-04 2018-07-31 Commonwealth Scientific And Industrial Research Organisation Separation method
WO2013009630A1 (en) * 2011-07-08 2013-01-17 Metal Oxygen Separation Technologies, Inc. Apparatus and method for condensing metal vapor
AT516062B1 (de) * 2015-01-15 2016-02-15 Boehlerit Gmbh & Co Kg Verfahren zum Beschichten eines Gegenstandes und damit hergestellte Beschichtung
CN104625081B (zh) * 2015-01-26 2017-02-01 北京科技大学 一种熔盐法制备钛铝合金粉末的方法
EP3334847A4 (en) 2015-08-14 2018-06-27 Coogee Titanium Pty Ltd Method for production of a composite material using excess oxidant
AU2016309952B2 (en) * 2015-08-14 2022-01-27 Coogee Titanium Pty Ltd Method for recovery of metal-containing material from a composite material
EA037140B9 (ru) * 2015-08-14 2021-03-15 Куги Титаниум Пти Лтд Способы с использованием реакционноспособных частиц с высокой площадью поверхности на единицу объема
WO2017219075A1 (en) * 2016-06-20 2017-12-28 Othrys Technologies Pty Ltd Coating of particulate substrates
EP3472368A4 (en) * 2016-06-20 2020-01-08 D-Block Coating Pty Ltd COATING PROCESS AND COATED MATERIALS
CA3029580C (en) 2016-07-06 2024-01-23 Kinaltek Pty. Ltd. Thermochemical processing of exothermic metallic systems
CN109996896B (zh) * 2016-09-14 2021-10-26 通用金属钛有限责任公司 生产钛-铝-钒合金的方法
CN110198798B (zh) * 2016-10-21 2022-11-29 通用电气公司 通过还原四卤化钛制造钛合金材料
CN110199040B (zh) * 2016-10-21 2022-10-04 通用电气公司 通过还原四氯化钛制造钛合金材料
US11193185B2 (en) 2016-10-21 2021-12-07 General Electric Company Producing titanium alloy materials through reduction of titanium tetrachloride
CN106745217B (zh) * 2017-03-14 2018-02-06 江苏展钛科技有限公司 一种用于铝粉还原四氯化钛制取三氯化钛的方法及反应器
CN107350482B (zh) * 2017-06-19 2019-08-02 西安建筑科技大学 一种V-Ti-Fe储氢合金粉的液相反应制备方法
CN113427016B (zh) * 2021-07-08 2024-02-13 安徽理工大学 一种制备细微钛铝金属间化合物粉末的装置及其生产方法
CN113774235B (zh) * 2021-08-25 2022-06-21 西安交通大学 一种间歇式连续提取皮江法炼镁中的结晶镁的方法及装置
CN114000076B (zh) * 2021-11-04 2022-05-27 四川大学 一种初始凝固相为β相的多取向片层组织TiAl合金及其制备方法和应用

Family Cites Families (40)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2005443A (en) * 1934-03-14 1935-06-18 Walter R Steele Harmonica
US2745735A (en) 1953-04-28 1956-05-15 Kaiser Aluminium Chem Corp Method of producing titanium
GB757873A (en) 1954-12-08 1956-09-26 Kaiser Aluminium Chem Corp Production of titanium
US3004848A (en) 1958-10-02 1961-10-17 Nat Distillers Chem Corp Method of making titanium and zirconium alloys
US3252823A (en) 1961-10-17 1966-05-24 Du Pont Process for aluminum reduction of metal halides in preparing alloys and coatings
BE645733A (ru) 1963-04-23
FR1471183A (fr) 1965-12-31 1967-03-03 Kuhlmann Ets Procédé pour l'obtention de poudres métalliques ou composites par réduction directe des halogénures correspondants
US3455678A (en) 1967-01-16 1969-07-15 Ethyl Corp Process for the concurrent production of aif3 and a metallic titanium product
US3684264A (en) 1971-01-06 1972-08-15 Vasily Ivanovich Petrov Apparatus for reduction of titanium halides and subsequent vacuum separation of reduction products
US3900312A (en) * 1972-10-16 1975-08-19 Toth Aluminum Corp Reduction of aluminum chloride by manganese
NL7607838A (nl) 1975-09-08 1977-03-10 Stauffer Chemical Co Werkwijze voor de bereiding van een katalysa- torcomponent en het met deze werkwijze verkre- gen produkt.
JPS5278608A (en) 1975-12-25 1977-07-02 Arita Kenkyusho Kk Dechloridizing titanium group meta chloride
JPS5350099A (en) 1976-10-20 1978-05-08 Toyo Soda Mfg Co Ltd Production of titanium carbide
GB1566363A (en) 1978-03-21 1980-04-30 G Ni I Pi Redkometallich Promy Magnesium-thermic reduction of chlorides
FR2505364A1 (fr) * 1981-05-06 1982-11-12 Rhone Poulenc Spec Chim Procede de fabrication d'alliages de titane et d'aluminium
CA1202183A (en) 1982-05-31 1986-03-25 Hiroshi Ishizuka Apparatus and method for producing purified refractory metal from a chloride thereof
US4447045A (en) 1982-07-21 1984-05-08 Mitsubishi Kinzoku Kabushiki Kaisha Apparatus for preparing high-melting-point high-toughness metals
JPS59226127A (ja) 1983-04-27 1984-12-19 Mitsubishi Metal Corp 高融点高靭性金属の製造装置
EP0134643A3 (en) 1983-07-08 1986-12-30 Solex Research Corporation of Japan Preparing metallic zirconium, hafnium or titanium
BR8402087A (pt) 1984-05-04 1985-12-10 Vale Do Rio Doce Co Processo de obtencao de titanio metalico a partir de um concentrado de anastasio,por aluminotermia e magnesiotermia
JPS6415334A (en) 1987-07-09 1989-01-19 Toho Titanium Co Ltd Production of metal from metal halide
JPS6452031A (en) 1987-08-24 1989-02-28 Toho Titanium Co Ltd Production of titanium alloy
JPH0747787B2 (ja) 1989-05-24 1995-05-24 株式会社エヌ・ケイ・アール チタン粉末またはチタン複合粉末の製造方法
JPH04107234A (ja) 1990-08-27 1992-04-08 Sumitomo Metal Ind Ltd 高強度高靭性チタン合金
US5397375A (en) 1991-02-21 1995-03-14 The University Of Melbourne Process for the production of metallic titanium and intermediates useful in the processing of ilmenite and related minerals
CN1101080A (zh) * 1993-09-28 1995-04-05 峨眉山市汇海经济技术开发公司 一种用铝热法生产高钛铁的方法
US5460642A (en) 1994-03-21 1995-10-24 Teledyne Industries, Inc. Aerosol reduction process for metal halides
RU2082561C1 (ru) 1994-12-15 1997-06-27 Акционерное общество "Российский научно-исследовательский и проектный институт титана и магния" Способ получения интерметаллида титан - алюминий в форме порошка
US5749937A (en) 1995-03-14 1998-05-12 Lockheed Idaho Technologies Company Fast quench reactor and method
US6168173B1 (en) * 1997-11-19 2001-01-02 The Burton Corporation Snowboard boot with binding interface
JP4132526B2 (ja) 1999-12-28 2008-08-13 東邦チタニウム株式会社 粉末状チタンの製造方法
US6699305B2 (en) 2000-03-21 2004-03-02 James J. Myrick Production of metals and their alloys
UA38454A (ru) 2000-07-06 2001-05-15 Державний Науково-Дослідний Та Проектний Інститут Титану Способ получения смешанных кристаллов трихлоридов титана и алюминия
US6902601B2 (en) 2002-09-12 2005-06-07 Millennium Inorganic Chemicals, Inc. Method of making elemental materials and alloys
EA010932B1 (ru) * 2003-07-04 2008-12-30 Коммонвелт Сайентифик Энд Индастриал Рисерч Организейшн Способ и устройство для получения металлических соединений
JP4107234B2 (ja) 2003-12-22 2008-06-25 松下電工株式会社 温水床暖房パネル
JP5232988B2 (ja) 2006-02-27 2013-07-10 国立大学法人名古屋大学 ナノ粒子の製造方法
UA91908C2 (ru) 2006-03-27 2010-09-10 Коммонвелт Сайентифик Энд Индастриал Рисерч Организейшн Способ и устройство для производства соединений металлов
WO2009129570A1 (en) 2008-04-21 2009-10-29 Commonwealth Scientific And Industrial Research Organisation Method and apparatus for forming titanium-aluminium based alloys
UA38454U (en) 2008-08-14 2009-01-12 Вячеслав Андреевич Барабаш Induction heater

Also Published As

Publication number Publication date
ES2394851T3 (es) 2013-02-06
EA014894B1 (ru) 2011-02-28
AU2007231543B2 (en) 2011-07-21
JP5886815B2 (ja) 2016-03-16
US20090165597A1 (en) 2009-07-02
CA2644430C (en) 2015-06-30
KR101399803B1 (ko) 2014-05-27
US8821612B2 (en) 2014-09-02
JP5479886B2 (ja) 2014-04-23
WO2007109847A1 (en) 2007-10-04
UA91908C2 (ru) 2010-09-10
AU2007231543A1 (en) 2007-10-04
EP1999285A4 (en) 2010-05-12
CA2644430A1 (en) 2007-10-04
CN101454467B (zh) 2014-01-08
EP1999285B1 (en) 2012-08-01
EP1999285A1 (en) 2008-12-10
KR20080106479A (ko) 2008-12-05
CN101454467A (zh) 2009-06-10
JP2014074232A (ja) 2014-04-24
JP2009531537A (ja) 2009-09-03

Similar Documents

Publication Publication Date Title
EA200870372A1 (ru) Устройство и способы для производства соединений металлов
CA2992502C (en) Method for producing titanium or titanium aluminum alloys through two-stage aluminothermic reduction and obtaining titanium-free cryolite as byproducts
CN103834834B (zh) 一种可阳极氧化的高性能压铸铝合金及其制备方法
EA200700906A1 (ru) Низкотемпературный промышленный процесс
CN105316550B (zh) 一种含长周期结构相高阻尼镁合金及其制备方法
CN107936300A (zh) 高氯酸盐改性分子筛环保稳定剂及其制备方法
ATE530555T1 (de) Verfahren zur herstellung von wasserstoffreichen cyclosiloxanen
Cai et al. Thermodynamic Analysis of Al‐RE Phase Formation in AZ91‐RE (Ce, Y, Gd) Magnesium Alloy
NO20081519L (no) Fremgangsmate og apparatur for fremstilling av Ti
CN105779803A (zh) 一种铝合金用复合变质剂及其制备方法
RU2011122498A (ru) Способ модифицирования доэвтектических алюминиево-кремниевых сплавов
CN104004987B (zh) 海绵钛生产用反应器的渗钛方法
NO20080519L (no) Fremgangsmate for produksjon av hoyrenset silikon
WO2003089676A8 (en) Iterative cycle process for carbon supersaturation of molten metal and solid metals obtained thereby
CN106747513B (zh) 一种超细钛铝酸钙粉体及其制备方法
CN100447265C (zh) 一种消除铝锭中钛偏析的方法
CN108060319A (zh) 一种高效纯净铝合金环保精炼剂及其制造方法
WO2014156783A1 (ja) 香料組成物及びその製造方法
JP2012214427A (ja) １，２−ベンズイソチアゾリン−３−オンを含有する水性組成物の製造方法
FR3095437B1 (fr) Procédé d’obtention de bromure de tétraéthylammonium et de tétrafluoroborate de tétraéthylammonium, produits et utilisations correspondants
CN108130442A (zh) 一种无钠无烟铝合金环保精炼剂及其制造方法
RU2018111183A (ru) Титано-медно-железный сплав и соответствующий способ тиксоформинга
CN104384461B (zh) 一种高锌镁锌锰合金铸锭的半连续铸造方法
CN105481006B (zh) 一种提高铝粉除钒法稳定性的方法
WO2017012710A8 (de) Verfahren zur reduktion von dreiwertigem eisen bei der herstellung von titandioxid im sulfatverfahren

Legal Events

Date Code Title Description
MM4A Lapse of a eurasian patent due to non-payment of renewal fees within the time limit in the following designated state(s)

Designated state(s): AM AZ BY KG MD TJ TM