DK2139639T3 - Et lodningsstykke, en fremgangsmåde til fremstilling af et lodningsstykke, og en fremgangsmåde til lodning og komponenter fremstillet af nævnte lodningsstykke - Google Patents
Et lodningsstykke, en fremgangsmåde til fremstilling af et lodningsstykke, og en fremgangsmåde til lodning og komponenter fremstillet af nævnte lodningsstykke Download PDFInfo
- Publication number
- DK2139639T3 DK2139639T3 DK08718725.8T DK08718725T DK2139639T3 DK 2139639 T3 DK2139639 T3 DK 2139639T3 DK 08718725 T DK08718725 T DK 08718725T DK 2139639 T3 DK2139639 T3 DK 2139639T3
- Authority
- DK
- Denmark
- Prior art keywords
- inorganic salt
- piece
- alloy
- salt
- metal
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 47
- 238000004519 manufacturing process Methods 0.000 title claims description 15
- 239000000126 substance Substances 0.000 title description 4
- 229910017053 inorganic salt Inorganic materials 0.000 claims description 93
- 230000004907 flux Effects 0.000 claims description 88
- 239000002131 composite material Substances 0.000 claims description 84
- 238000005219 brazing Methods 0.000 claims description 83
- 150000003839 salts Chemical class 0.000 claims description 83
- 239000000463 material Substances 0.000 claims description 65
- 229910052751 metal Inorganic materials 0.000 claims description 62
- 239000002184 metal Substances 0.000 claims description 62
- 239000000956 alloy Substances 0.000 claims description 53
- 239000002245 particle Substances 0.000 claims description 52
- 239000007921 spray Substances 0.000 claims description 50
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 45
- 229910052782 aluminium Inorganic materials 0.000 claims description 45
- 238000002844 melting Methods 0.000 claims description 41
- 230000008018 melting Effects 0.000 claims description 41
- 229910045601 alloy Inorganic materials 0.000 claims description 40
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 28
- 239000001301 oxygen Substances 0.000 claims description 28
- 229910052760 oxygen Inorganic materials 0.000 claims description 28
- 229910000838 Al alloy Inorganic materials 0.000 claims description 26
- 239000011159 matrix material Substances 0.000 claims description 26
- 229910001092 metal group alloy Inorganic materials 0.000 claims description 20
- 230000008569 process Effects 0.000 claims description 16
- 229910052710 silicon Inorganic materials 0.000 claims description 16
- 239000011856 silicon-based particle Substances 0.000 claims description 16
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 14
- 239000013078 crystal Substances 0.000 claims description 13
- 239000010703 silicon Substances 0.000 claims description 12
- 238000010438 heat treatment Methods 0.000 claims description 11
- 239000012298 atmosphere Substances 0.000 claims description 10
- 229910000679 solder Inorganic materials 0.000 claims description 10
- 230000015572 biosynthetic process Effects 0.000 claims description 9
- 238000005507 spraying Methods 0.000 claims description 9
- 238000005096 rolling process Methods 0.000 claims description 8
- 239000007787 solid Substances 0.000 claims description 8
- 238000007596 consolidation process Methods 0.000 claims description 7
- 238000002347 injection Methods 0.000 claims description 6
- 239000007924 injection Substances 0.000 claims description 6
- 238000005242 forging Methods 0.000 claims description 5
- 238000005097 cold rolling Methods 0.000 claims description 4
- 238000001125 extrusion Methods 0.000 claims description 4
- 239000000446 fuel Substances 0.000 claims description 4
- 238000005098 hot rolling Methods 0.000 claims description 4
- 239000011261 inert gas Substances 0.000 claims description 4
- 239000003921 oil Substances 0.000 claims description 4
- -1 potassium fluorine aluminate Chemical class 0.000 claims description 4
- SKFYTVYMYJCRET-UHFFFAOYSA-J potassium;tetrafluoroalumanuide Chemical compound [F-].[F-].[F-].[F-].[Al+3].[K+] SKFYTVYMYJCRET-UHFFFAOYSA-J 0.000 claims description 4
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 239000000470 constituent Substances 0.000 claims description 3
- 238000000605 extraction Methods 0.000 claims description 3
- 238000000926 separation method Methods 0.000 claims description 3
- 150000001875 compounds Chemical class 0.000 claims 5
- 238000005476 soldering Methods 0.000 claims 5
- 238000000889 atomisation Methods 0.000 claims 3
- 238000001746 injection moulding Methods 0.000 claims 3
- 238000000641 cold extrusion Methods 0.000 claims 2
- 238000010273 cold forging Methods 0.000 claims 2
- 238000005520 cutting process Methods 0.000 claims 2
- CSDREXVUYHZDNP-UHFFFAOYSA-N alumanylidynesilicon Chemical compound [Al].[Si] CSDREXVUYHZDNP-UHFFFAOYSA-N 0.000 claims 1
- 239000000843 powder Substances 0.000 description 51
- 239000004411 aluminium Substances 0.000 description 34
- 239000000523 sample Substances 0.000 description 29
- 229910000789 Aluminium-silicon alloy Inorganic materials 0.000 description 24
- 239000000945 filler Substances 0.000 description 17
- 230000000694 effects Effects 0.000 description 14
- 239000000203 mixture Substances 0.000 description 13
- 239000000047 product Substances 0.000 description 13
- 238000000151 deposition Methods 0.000 description 12
- 238000009718 spray deposition Methods 0.000 description 12
- 230000008021 deposition Effects 0.000 description 11
- 238000009826 distribution Methods 0.000 description 10
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 9
- KMWBBMXGHHLDKL-UHFFFAOYSA-N [AlH3].[Si] Chemical compound [AlH3].[Si] KMWBBMXGHHLDKL-UHFFFAOYSA-N 0.000 description 9
- 238000002156 mixing Methods 0.000 description 9
- 238000005253 cladding Methods 0.000 description 8
- 238000007254 oxidation reaction Methods 0.000 description 8
- KLZUFWVZNOTSEM-UHFFFAOYSA-K Aluminium flouride Chemical compound F[Al](F)F KLZUFWVZNOTSEM-UHFFFAOYSA-K 0.000 description 7
- 230000009471 action Effects 0.000 description 7
- 238000000113 differential scanning calorimetry Methods 0.000 description 7
- 230000003647 oxidation Effects 0.000 description 7
- 238000012545 processing Methods 0.000 description 7
- 230000005496 eutectics Effects 0.000 description 6
- 229910010272 inorganic material Inorganic materials 0.000 description 6
- 239000011147 inorganic material Substances 0.000 description 6
- 239000000155 melt Substances 0.000 description 6
- 229910001868 water Inorganic materials 0.000 description 5
- 238000009736 wetting Methods 0.000 description 5
- 238000002441 X-ray diffraction Methods 0.000 description 4
- 238000013459 approach Methods 0.000 description 4
- 239000011230 binding agent Substances 0.000 description 4
- 239000011162 core material Substances 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- 239000002244 precipitate Substances 0.000 description 4
- 238000007711 solidification Methods 0.000 description 4
- 230000008023 solidification Effects 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 241000566150 Pandion haliaetus Species 0.000 description 3
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 3
- 239000011248 coating agent Substances 0.000 description 3
- 238000000576 coating method Methods 0.000 description 3
- 230000001747 exhibiting effect Effects 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 238000007731 hot pressing Methods 0.000 description 3
- 239000010954 inorganic particle Substances 0.000 description 3
- 238000001000 micrograph Methods 0.000 description 3
- 229910052700 potassium Inorganic materials 0.000 description 3
- 239000011591 potassium Substances 0.000 description 3
- NROKBHXJSPEDAR-UHFFFAOYSA-M potassium fluoride Chemical compound [F-].[K+] NROKBHXJSPEDAR-UHFFFAOYSA-M 0.000 description 3
- 239000011698 potassium fluoride Substances 0.000 description 3
- 238000007712 rapid solidification Methods 0.000 description 3
- 238000010118 rheocasting Methods 0.000 description 3
- 239000011863 silicon-based powder Substances 0.000 description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 2
- 238000007792 addition Methods 0.000 description 2
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical group [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 2
- 230000002902 bimodal effect Effects 0.000 description 2
- 238000005266 casting Methods 0.000 description 2
- 238000005056 compaction Methods 0.000 description 2
- 238000007872 degassing Methods 0.000 description 2
- 230000018044 dehydration Effects 0.000 description 2
- 238000006297 dehydration reaction Methods 0.000 description 2
- 230000001627 detrimental effect Effects 0.000 description 2
- 238000000724 energy-dispersive X-ray spectrum Methods 0.000 description 2
- 239000006023 eutectic alloy Substances 0.000 description 2
- 239000012467 final product Substances 0.000 description 2
- 238000001513 hot isostatic pressing Methods 0.000 description 2
- 230000036571 hydration Effects 0.000 description 2
- 238000006703 hydration reaction Methods 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 238000011835 investigation Methods 0.000 description 2
- 239000010410 layer Substances 0.000 description 2
- 238000003801 milling Methods 0.000 description 2
- 239000011812 mixed powder Substances 0.000 description 2
- 239000012299 nitrogen atmosphere Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000013074 reference sample Substances 0.000 description 2
- 238000001878 scanning electron micrograph Methods 0.000 description 2
- 239000002002 slurry Substances 0.000 description 2
- 238000003892 spreading Methods 0.000 description 2
- 230000007480 spreading Effects 0.000 description 2
- 239000000758 substrate Substances 0.000 description 2
- 239000002344 surface layer Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 229910000676 Si alloy Inorganic materials 0.000 description 1
- 229910018619 Si-Fe Inorganic materials 0.000 description 1
- 229910008289 Si—Fe Inorganic materials 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- 229910000611 Zinc aluminium Inorganic materials 0.000 description 1
- OADLXVPCCPLTKX-UHFFFAOYSA-J [Sn](F)(F)(F)F.[K] Chemical class [Sn](F)(F)(F)F.[K] OADLXVPCCPLTKX-UHFFFAOYSA-J 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 239000010953 base metal Substances 0.000 description 1
- 229910052792 caesium Inorganic materials 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000001311 chemical methods and process Methods 0.000 description 1
- 238000004581 coalescence Methods 0.000 description 1
- 230000001427 coherent effect Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000012792 core layer Substances 0.000 description 1
- 229910001610 cryolite Inorganic materials 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000000280 densification Methods 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 231100001261 hazardous Toxicity 0.000 description 1
- 231100000206 health hazard Toxicity 0.000 description 1
- 239000008240 homogeneous mixture Substances 0.000 description 1
- 150000004677 hydrates Chemical class 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000010348 incorporation Methods 0.000 description 1
- APFVFJFRJDLVQX-UHFFFAOYSA-N indium atom Chemical compound [In] APFVFJFRJDLVQX-UHFFFAOYSA-N 0.000 description 1
- 239000011872 intimate mixture Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000005499 meniscus Effects 0.000 description 1
- 238000006263 metalation reaction Methods 0.000 description 1
- 238000010310 metallurgical process Methods 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 230000036961 partial effect Effects 0.000 description 1
- 235000003270 potassium fluoride Nutrition 0.000 description 1
- 238000004663 powder metallurgy Methods 0.000 description 1
- 238000011112 process operation Methods 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 238000009877 rendering Methods 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 238000005204 segregation Methods 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 238000005482 strain hardening Methods 0.000 description 1
- 230000003746 surface roughness Effects 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- 230000036967 uncompetitive effect Effects 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- BHHYHSUAOQUXJK-UHFFFAOYSA-L zinc fluoride Chemical class F[Zn]F BHHYHSUAOQUXJK-UHFFFAOYSA-L 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K35/00—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
- B23K35/02—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting characterised by mechanical features, e.g. shape
- B23K35/0222—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting characterised by mechanical features, e.g. shape for use in soldering, brazing
- B23K35/0233—Sheets, foils
- B23K35/0238—Sheets, foils layered
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K35/00—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
- B23K35/02—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting characterised by mechanical features, e.g. shape
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C4/00—Coating by spraying the coating material in the molten state, e.g. by flame, plasma or electric discharge
- C23C4/12—Coating by spraying the coating material in the molten state, e.g. by flame, plasma or electric discharge characterised by the method of spraying
- C23C4/123—Spraying molten metal
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K35/00—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
- B23K35/02—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting characterised by mechanical features, e.g. shape
- B23K35/0222—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting characterised by mechanical features, e.g. shape for use in soldering, brazing
- B23K35/0244—Powders, particles or spheres; Preforms made therefrom
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K35/00—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
- B23K35/22—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting characterised by the composition or nature of the material
- B23K35/24—Selection of soldering or welding materials proper
- B23K35/28—Selection of soldering or welding materials proper with the principal constituent melting at less than 950 degrees C
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K35/00—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
- B23K35/22—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting characterised by the composition or nature of the material
- B23K35/36—Selection of non-metallic compositions, e.g. coatings, fluxes; Selection of soldering or welding materials, conjoint with selection of non-metallic compositions, both selections being of interest
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C1/00—Making non-ferrous alloys
- C22C1/10—Alloys containing non-metals
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C1/00—Making non-ferrous alloys
- C22C1/10—Alloys containing non-metals
- C22C1/1036—Alloys containing non-metals starting from a melt
- C22C1/1042—Alloys containing non-metals starting from a melt by atomising
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C32/00—Non-ferrous alloys containing at least 5% by weight but less than 50% by weight of oxides, carbides, borides, nitrides, silicides or other metal compounds, e.g. oxynitrides, sulfides, whether added as such or formed in situ
- C22C32/0089—Non-ferrous alloys containing at least 5% by weight but less than 50% by weight of oxides, carbides, borides, nitrides, silicides or other metal compounds, e.g. oxynitrides, sulfides, whether added as such or formed in situ with other, not previously mentioned inorganic compounds as the main non-metallic constituent, e.g. sulfides, glass
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K35/00—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
- B23K35/22—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting characterised by the composition or nature of the material
- B23K35/24—Selection of soldering or welding materials proper
- B23K35/28—Selection of soldering or welding materials proper with the principal constituent melting at less than 950 degrees C
- B23K35/286—Al as the principal constituent
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K35/00—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
- B23K35/22—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting characterised by the composition or nature of the material
- B23K35/36—Selection of non-metallic compositions, e.g. coatings, fluxes; Selection of soldering or welding materials, conjoint with selection of non-metallic compositions, both selections being of interest
- B23K35/3601—Selection of non-metallic compositions, e.g. coatings, fluxes; Selection of soldering or welding materials, conjoint with selection of non-metallic compositions, both selections being of interest with inorganic compounds as principal constituents
- B23K35/3603—Halide salts
- B23K35/3605—Fluorides
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K35/00—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
- B23K35/22—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting characterised by the composition or nature of the material
- B23K35/36—Selection of non-metallic compositions, e.g. coatings, fluxes; Selection of soldering or welding materials, conjoint with selection of non-metallic compositions, both selections being of interest
- B23K35/3601—Selection of non-metallic compositions, e.g. coatings, fluxes; Selection of soldering or welding materials, conjoint with selection of non-metallic compositions, both selections being of interest with inorganic compounds as principal constituents
- B23K35/361—Alumina or aluminates
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/12—All metal or with adjacent metals
- Y10T428/12014—All metal or with adjacent metals having metal particles
- Y10T428/12028—Composite; i.e., plural, adjacent, spatially distinct metal components [e.g., layers, etc.]
- Y10T428/12049—Nonmetal component
- Y10T428/12056—Entirely inorganic
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/12—All metal or with adjacent metals
- Y10T428/12014—All metal or with adjacent metals having metal particles
- Y10T428/12028—Composite; i.e., plural, adjacent, spatially distinct metal components [e.g., layers, etc.]
- Y10T428/12146—Nonmetal particles in a component
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/12—All metal or with adjacent metals
- Y10T428/12493—Composite; i.e., plural, adjacent, spatially distinct metal components [e.g., layers, joint, etc.]
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/12—All metal or with adjacent metals
- Y10T428/12493—Composite; i.e., plural, adjacent, spatially distinct metal components [e.g., layers, joint, etc.]
- Y10T428/12736—Al-base component
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Claims (31)
1. Selvflussende lodningsstykke, hvilket stykke omfatter et sprøjteformet kompositmateriale omfattende mindst et uorganisk salt fordelt i formen af stivnede partikler i en aluminiumlegeringsmatrix, hvor det uorganiske salt er i alt væsentligt uopløseligt og i alt væsentligt ikkeblandbart i aluminiumlegeringsmaterialet i dets smeltede tilstand, hvor det uorganiske salt eller uorganiske salte danner et flusmiddel under lodning for at fremme dannelsen afen termisk induceret metalbinding, hvor stykket er en sprøjteformet knippel.
2. Stykke ifølge krav 1, hvor stykket er blevet bearbejdet, for eksempel, ved smedning eller valsning eller ekstrudering.
3. Stykke ifølge krav 1 eller krav 2, hvor oxygenindholdet af matrixen er ikke mere end 350 ppm efter vægt, fortrinsvis ikke mere end 250 ppm efter vægt, mere fortrinsvis ikke mere end 100 ppm efter vægt og mest fortrinsvis ikke mere end 50 ppm efter vægt.
4. Stykke ifølge krav 1, 2 eller 3, hvor lodningslegeringen har aluminium og silicium som hovedbestanddele, hvor siliciumindholdet fortrinsvis er 5 til 15 vægtprocent, mere fortrinsvis 6 til 13 vægtprocent, mere fortrinsvis 9 til 13 vægtprocent og siliciumindholdet kan være 10 til 12 vægtprocent, i hvilket stykket kan indeholde siliciumpartikler og siliciumpartiklerne kan have en gennemsnitsdiameter på mindre end 10 mikrometer, fortrinsvis på mindre end 5 mikrometer, mere fortrinsvis mindre end 3 mikrometer.
5. Stykke ifølge et hvilket som helst af de foregående krav, hvor et kalium-aluminium-fluorid-flusmiddel er tilvejebragt som det uorganiske salt eller to eller flere uorganiske salte er tilvejebragt der under lodning danner et kalium-aluminium-fluorid-flusmiddel eller et kalium-fluor-aluminat-flusmiddel er tilvejebragt som det uorganiske salt eller to eller flere uorganiske salte er tilvejebragt der under lodning danner et kalium-fluor-aluminat-flusmiddel.
6. Stykke ifølge et hvilket som helst af de foregående krav, hvor kompositmaterialet har et uorganisk saltindhold på 0,2-10 vægtprocent, og kan have et uorganisk saltindhold på mindst 0,9 vægtprocent, og eventuelt har et uorganisk saltindhold på mindst 1,2 vægtprocent og kan have et uorganisk saltindhold på ikke mere end 5 vægtprocent og eventuelt har et uorganisk saltindhold på ikke mere end 4 vægtprocent og kan have et uorganisk saltindhold på omkring 2-3 vægtprocent.
7. Stykke ifølge et hvilket som helst af de foregående krav, hvor det eller hvert uorganiske salt har et lavere smeltepunkt end aluminiumlegeringen.
8. Stykke ifølge et hvilket som helst af de foregående krav, hvor det uorganiske salt eller salte danner partikler i kompositmaterialet mindre end 1 mikrometer i størrelse.
9. Stykke ifølge et hvilket som helst af de foregående krav, hvor det uorganiske salt eller salte danner partikler i kompositmaterialet på mellem 5 og 200 mikrometer i størrelse.
10. Stykke ifølge et hvilket som helst af de foregående krav, hvor det uorganiske salt eller salte danner partikler i kompositmaterialet og mellempartikelafstanden mellem tilstødende saltpartikler er mindre end 10 mikrometer og kan være mindre end 5 mikrometer.
11. Stykke ifølge et hvilket som helst af de foregående krav, hvor oxygenindholdet af stykket er ikke mere end 1000 ppm, fortrinsvis ikke mere end 500 ppm, mere fortrinsvis ikke mere end 300 ppm, mest fortrinsvis ikke mere end 250 ppm.
12. Stykke ifølge et hvilket som helst af de foregående krav, hvor stykket har en ikke-partikelformig mikrostruktur.
13. Stykke ifølge et hvilket som helst af de foregående krav, hvor det uorganiske salt eller salte er fordelt i formen af ikke-makrosegregerede partikler i aluminiumlegeringsmatrixen, således at mellempartikelafstanden mellem saltkrystaller er mindre end 20 mikrometer.
14. Komponent omfattende mindst et stykke ifølge et hvilket som helst af de foregående krav fastgjort til en metalgenstand, såsom en råblok, knippel eller slab, hvor det eller hvert stykke kan være valsebundet på metalgenstanden og hvor to sådanne stykker kan være fastgjort til metalgenstanden på modstående sider deraf, og hvor komponenten kan bearbejdes for eksempel ved en eller flere af varmvalsning, koldvalsning, ekstrudering og smedning og hvor komponenten kan være en komponent til at blive forbundet ved lodning i en varmeveksler, såsom en bilkøler, kondensator, fordamper, oliekøler, ladeluftkøler eller brændstofkøler, eller en stationær varmeveksler, og komponenten kan være en ribbe, plade eller rør, der skal loddes på plads i en varmeveksler, såsom en bilkøler, kondensator, fordamper, oliekøler, ladeluftkøler eller brændstofkøler, eller en stationær varmeveksler.
15. Fremgangsmåde til fremstilling af stykke ifølge et hvilket som helst af kravene 1 til 13 eller en komponent ifølge krav 14, hvilken fremgangsmåde omfatter trinnene at smelte aluminiumlegering, og, i en inert atmosfære at udsende en strøm af den smeltede aluminiumlodningslegering, at forstøve strømmen af smeltet aluminiumlodningslegering til en spray af dråber under anvendelse af en inertgas, at indføre det eller hvert uorganiske salt i strømmen eller sprayen, og at konsolidere aluminiumlodningslegeringen og det eller hvert salt ved sprøjteforming for at danne et kompositstykke i hvilket det uorganiske salt er fordelt som partikler i en aluminiumlodningslegeringsmatrix.
16. Fremgangsmåde til fremstilling af et selvflussende lodningsstykke, hvilken fremgangsmåde omfatter trinnene at smelte aluminiumlodningslegering, og, i en inert atmosfære at udsende en strøm af den smeltede aluminiumlodningslegering, at forstøve strømmen af smeltet aluminiumlodningslegeringmateriale til en spray af dråber under anvendelse af en inertgas, at indføre i strømmen eller sprayen mindst et uorganisk salt, hvor det eller hvert uorganiske salt er i alt væsentligt ikkeblandbart og i alt væsentligt uopløseligt når i sin smeltede form med aluminiumlodningslegeringen, hvor det uorganiske salt eller uorganiske salte anbringes til at danne et flusmiddel under lodning, og at konsolidere aluminiumlodningslegeringen og det eller hvert salt ved at sprøjteforming for at danne et kompositstykke i hvilket det uorganiske salt er fordelt som partikler i en aluminiumlodningslegeringsmatrix.
17. Fremgangsmåde ifølge krav 15 eller krav 16, hvor det eller hvert uorganiske salt smeltes og forstøves til at blive sprøjteformet eller hvor det uorganiske salt indføres som faste partikler, der kan være af en gennemsnitsdiameter på 10 mikrometer eller mindre.
18. Fremgangsmåde ifølge et hvilket som helst af kravene 15, 16 og 17, hvor aluminiumlegeringsmaterialet forstøves til dråber med en gennemsnitsdiameter i området 50 til 150 mikrometer.
19. Fremgangsmåde ifølge et hvilket som helst af kravene 15 til 18, hvor det eller hvert uorganiske salt har et lavere smeltepunkt end aluminiumlegeringsmaterialet.
20. Fremgangsmåde ifølge et hvilket som helst af kravene 15 til 19, hvor det uorganiske salt forårsages til mindst delvist at smelte, når det indføres eller når det sprøjtes og kan være i alt væsentligt fuldkommen smeltet, når sprøjt aflejres på en samleroverflade med aluminiumlegeringsmaterialet.
21. Fremgangsmåde ifølge et hvilket som helst af kravene 15 til 20, hvor det uorganiske salt eller salte danner partikler i kompositmaterialet og mellempartikelafstanden mellem tilstødende partikler er mindre end diameteren af aluminium-siliciumdråberne fra hvilke det sprøjteformede kompositstykke er dannet, hvor fortrinsvis mellempartikelafstanden mellem tilstødende partikler er mindre end 10 mikrometer, mere fortrinsvis mindre end 5 mikrometer.
22. Fremgangsmåde ifølge et hvilket som helst af kravene 15 til 21, hvor varmeekstrahering fra dråberne af materialerne styres under sprøjtning for at forhindre separation af det uorganiske salt fra aluminiumlegeringen.
23. Fremgangsmåde ifølge et hvilket som helst af kravene 15 til 22, hvor oxygenindholdet af stykket er ikke mere end 500 ppm højere end det kombinerede oxygenindhold af den smeltede aluminiumlegering og det uorganiske salt eller uorganiske salte forud for forstøvning og sprøjtning, fortrinsvis ikke mere end 250 ppm højere end det kombinerede oxygenindhold af den smeltede aluminiumlegering og det uorganiske salt eller uorganiske salte forud for forstøvning og sprøjtning og mere fortrinsvis ikke mere end 100 ppm højere end det kombinerede oxygenindhold af den smeltede aluminiumlegering og det uorganiske salt eller uorganiske salte forud for forstøvning og sprøjtning.
24. Fremgangsmåde ifølge et hvilket som helst af kravene 15 til 23, hvor sprayet rammer en samleroverflade og opbygges til en knippel, og fremgangsmåden inkluderer trinnet at fjerne kniplen fra samleroverfladen.
25. Fremgangsmåde ifølge et hvilket som helst af kravene 15 til 24, hvor stykket bearbejdes, for eksempel ved smedning eller valsning eller ekstrudering.
26. Fremgangsmåde ifølge et hvilket som helst af kravene 15 til 25, hvor kompositmaterialet er fastgjort til en metalgenstand såsom en råblok, knippel eller slab og hvor to stykker af kompositmateriale kan fastgøres til metalgenstanden på modstående sider deraf og kompositmaterialet kan fastgøres ved varm- eller koldvalsningsbinding på metalgenstanden eller kompositmaterialet kan fastgøres til metalgenstanden under konsolideringen af aluminiumlegeringen og salt ved sprøjteformning ved at materialerne sprøjteformes på en metalgenstand for at binde dertil og fortrinsvis kompositmaterialet og metalgenstand bearbejdes for eksempel af en eller flere af varmvalsning, koldvalsning, ekstrudering og smedning.
27. Fremgangsmåde til fremstilling afen lodningsforbindelse, hvilken fremgangsmåde omfatter at placere et stykke ifølge et hvilket som helst af kravene 1 til 13, eller at placere kompositmaterialedelen af en komponent ifølge krav 14, eller at udføre fremgangsmåden ifølge et hvilket som helst af kravene 15 til 26, og at placere kompositmaterialet i direkte kontakt med et andet metaleller metallegeringstykke og at opvarme forbindelsen i fraværet af tilsat flusmiddel.
28. Fremgangsmåde ifølge krav 27, hvor kompositstykket bearbejdes efter fremstilling og før placering i kontakt med det andet metal- eller metallegeringstykke, for eksempel ved en eller flere af varmvalsning, koldvalsning, ekstrudering og smedning.
29. Lodningsforbindelse mellem to stykker eller dele, hvilken lodningsforbindelse er dannet ved at placere et lodningsstykke ifølge et hvilket som helst af kravene 1 til 13, eller ved at placere kompositmaterialedelen afen komponent ifølge krav 14 i direkte kontakt med et andet metal- eller metallegeringstykke og at opvarme forbindelsen i fraværet af tilsat flusmiddel.
30. Lodningsforbindelse mellem to stykker eller dele, hvilken lodningsforbindelse er dannet ved at udføre fremgangsmåden ifølge et hvilket som helst af kravene 15 til 28, at placere kompositmaterialet i direkte kontakt med et metal- eller metallegeringstykke, og at opvarme forbindelsen i fraværet af tilsat flusmiddel.
31. Genstand omfattende en lodningsforbindelse ifølge krav 29 eller krav 30, hvor genstanden eventuelt er en varmeveksler.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB0704926A GB2447486A (en) | 2007-03-14 | 2007-03-14 | A brazing piece comprising a composite material including an inorganic flux |
| PCT/GB2008/000883 WO2008110808A1 (en) | 2007-03-14 | 2008-03-14 | A brazing piece, a method of making a brazing piece, and a method of brazing and components made from said brazing piece |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DK2139639T3 true DK2139639T3 (da) | 2018-06-06 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DK08718725.8T DK2139639T3 (da) | 2007-03-14 | 2008-03-14 | Et lodningsstykke, en fremgangsmåde til fremstilling af et lodningsstykke, og en fremgangsmåde til lodning og komponenter fremstillet af nævnte lodningsstykke |
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| EP (1) | EP2139639B9 (da) |
| JP (2) | JP6184047B2 (da) |
| KR (1) | KR101532799B1 (da) |
| CN (1) | CN101674915B (da) |
| BR (1) | BRPI0808862B1 (da) |
| CA (1) | CA2681166C (da) |
| DK (1) | DK2139639T3 (da) |
| EA (1) | EA016458B1 (da) |
| ES (1) | ES2670933T3 (da) |
| GB (1) | GB2447486A (da) |
| HK (1) | HK1141260A1 (da) |
| HU (1) | HUE037502T2 (da) |
| MX (1) | MX2009009815A (da) |
| NO (1) | NO2139639T3 (da) |
| PL (1) | PL2139639T3 (da) |
| PT (1) | PT2139639T (da) |
| TR (1) | TR201807160T4 (da) |
| WO (1) | WO2008110808A1 (da) |
| ZA (1) | ZA200907139B (da) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2447486A (en) * | 2007-03-14 | 2008-09-17 | Sandvik Osprey Ltd | A brazing piece comprising a composite material including an inorganic flux |
| US8991480B2 (en) * | 2010-12-15 | 2015-03-31 | Uop Llc | Fabrication method for making brazed heat exchanger with enhanced parting sheets |
| DE102012006121A1 (de) * | 2012-03-26 | 2013-09-26 | Erbslöh Aluminium Gmbh | Lotpulver |
| MX2015001174A (es) * | 2012-07-27 | 2015-11-23 | Gränges Sweden Ab | Material en forma de cinta con excelente resistencia contra la corrosion despues del latonado. |
| JP6090736B2 (ja) * | 2012-10-26 | 2017-03-08 | 株式会社Uacj | アルミニウム合金のろう付方法及びフラックス成分被覆アルミニウム合金部材 |
| CN103740956B (zh) * | 2014-01-08 | 2015-12-30 | 镇江镨利玛新型材料科技有限公司 | 高硅铝合金的制备方法 |
| US20150219405A1 (en) * | 2014-02-05 | 2015-08-06 | Lennox Industries Inc. | Cladded brazed alloy tube for system components |
| EP2907615A1 (de) | 2014-05-28 | 2015-08-19 | AMAG rolling GmbH | Verbundblech |
| JP6472323B2 (ja) * | 2015-05-18 | 2019-02-20 | タツタ電線株式会社 | 成膜方法 |
| BR102015026864A2 (pt) * | 2015-10-22 | 2017-05-02 | Whirlpool Sa | processo de brasagem de tubos e compressor |
| JP6454262B2 (ja) | 2015-12-24 | 2019-01-16 | タツタ電線株式会社 | 半田接続構造、および成膜方法 |
| HUE047293T2 (hu) | 2016-04-12 | 2020-04-28 | Graenges Ab | Forrasztólemez |
| US10730150B2 (en) | 2017-08-07 | 2020-08-04 | Honeywell International Inc. | Flowable brazing compositions and methods of brazing metal articles together using the same |
| CN111432972B (zh) * | 2018-06-14 | 2022-05-03 | 日本轻金属株式会社 | 多层包覆件的制造方法 |
| CN114845830B (zh) * | 2019-12-27 | 2024-03-01 | 哈利玛化成株式会社 | 钎焊材料的涂布方法和钎焊用金属构件的制造方法 |
| CN111843280A (zh) * | 2020-05-25 | 2020-10-30 | 上海萨新东台热传输材料有限公司 | 一种自钎焊铝合金层状复合材料、制备方法及应用 |
| CN112792478A (zh) * | 2021-01-06 | 2021-05-14 | 李珮豪 | 一种自钎剂铝钎料板材及其制作方法 |
| CN113210608A (zh) * | 2021-03-31 | 2021-08-06 | 银邦金属复合材料股份有限公司 | 预埋钎剂铝合金复合材料及其制备方法和应用 |
| CN113232381A (zh) * | 2021-05-19 | 2021-08-10 | 飞荣达科技(江苏)有限公司 | 一种自带无腐蚀钎焊剂的铝合金复合板及其制备方法 |
| CN114473385B (zh) * | 2022-02-17 | 2023-05-26 | 上海华峰铝业股份有限公司 | 一种预埋钎剂复合板及其制备方法和用途 |
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2007
- 2007-03-14 GB GB0704926A patent/GB2447486A/en not_active Withdrawn
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2008
- 2008-03-14 DK DK08718725.8T patent/DK2139639T3/da active
- 2008-03-14 EP EP08718725.8A patent/EP2139639B9/en active Active
- 2008-03-14 MX MX2009009815A patent/MX2009009815A/es active IP Right Grant
- 2008-03-14 BR BRPI0808862A patent/BRPI0808862B1/pt not_active IP Right Cessation
- 2008-03-14 EA EA200970855A patent/EA016458B1/ru unknown
- 2008-03-14 TR TR2018/07160T patent/TR201807160T4/tr unknown
- 2008-03-14 NO NO08718725A patent/NO2139639T3/no unknown
- 2008-03-14 KR KR1020097021482A patent/KR101532799B1/ko active IP Right Grant
- 2008-03-14 CA CA2681166A patent/CA2681166C/en active Active
- 2008-03-14 JP JP2009553209A patent/JP6184047B2/ja not_active Expired - Fee Related
- 2008-03-14 PT PT87187258T patent/PT2139639T/pt unknown
- 2008-03-14 ES ES08718725.8T patent/ES2670933T3/es active Active
- 2008-03-14 US US12/595,942 patent/US8871356B2/en active Active
- 2008-03-14 WO PCT/GB2008/000883 patent/WO2008110808A1/en active Application Filing
- 2008-03-14 CN CN200880008343.5A patent/CN101674915B/zh active Active
- 2008-03-14 HU HUE08718725A patent/HUE037502T2/hu unknown
- 2008-03-14 PL PL08718725T patent/PL2139639T3/pl unknown
-
2009
- 2009-10-13 ZA ZA200907139A patent/ZA200907139B/xx unknown
-
2010
- 2010-08-17 HK HK10107840.5A patent/HK1141260A1/xx not_active IP Right Cessation
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2015
- 2015-06-09 JP JP2015116512A patent/JP6080901B2/ja not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| TR201807160T4 (tr) | 2018-06-21 |
| ES2670933T3 (es) | 2018-06-04 |
| CA2681166A1 (en) | 2008-09-18 |
| ZA200907139B (en) | 2010-06-30 |
| HK1141260A1 (en) | 2010-11-05 |
| EP2139639B9 (en) | 2019-03-06 |
| GB2447486A (en) | 2008-09-17 |
| JP2015213962A (ja) | 2015-12-03 |
| JP6080901B2 (ja) | 2017-02-15 |
| US20100206529A1 (en) | 2010-08-19 |
| CA2681166C (en) | 2018-03-27 |
| KR101532799B1 (ko) | 2015-06-30 |
| PT2139639T (pt) | 2018-06-01 |
| EA200970855A1 (ru) | 2010-04-30 |
| WO2008110808A1 (en) | 2008-09-18 |
| GB0704926D0 (en) | 2007-04-25 |
| BRPI0808862B1 (pt) | 2017-05-23 |
| CN101674915A (zh) | 2010-03-17 |
| US8871356B2 (en) | 2014-10-28 |
| KR20090127929A (ko) | 2009-12-14 |
| EA016458B1 (ru) | 2012-05-30 |
| JP6184047B2 (ja) | 2017-08-23 |
| MX2009009815A (es) | 2009-12-02 |
| CN101674915B (zh) | 2014-03-12 |
| EP2139639A1 (en) | 2010-01-06 |
| JP2010521308A (ja) | 2010-06-24 |
| NO2139639T3 (da) | 2018-09-29 |
| BRPI0808862A2 (pt) | 2014-09-23 |
| HUE037502T2 (hu) | 2018-08-28 |
| EP2139639B1 (en) | 2018-05-02 |
| PL2139639T3 (pl) | 2018-08-31 |
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