DE69636206T2 - Verfahren zur Herstellung eines Katalysators - Google Patents

Verfahren zur Herstellung eines Katalysators Download PDF

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Publication number
DE69636206T2
DE69636206T2 DE69636206T DE69636206T DE69636206T2 DE 69636206 T2 DE69636206 T2 DE 69636206T2 DE 69636206 T DE69636206 T DE 69636206T DE 69636206 T DE69636206 T DE 69636206T DE 69636206 T2 DE69636206 T2 DE 69636206T2
Authority
DE
Germany
Prior art keywords
catalyst
catalytically active
parts
active ingredient
powder
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69636206T
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German (de)
English (en)
Other versions
DE69636206D1 (de
Inventor
Hideki Sugi
Fumio Sakai
Koichi Yamato-shi Wada
Kazuo Annaka-shi SHIRAISHI
Toshitake Sawa-gun KOJIMA
Atsushi Sawa-gun UMEJIMA
Yoshimasa Asa-gun SEO
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Kayaku Co Ltd
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Nippon Kayaku Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nippon Kayaku Co Ltd filed Critical Nippon Kayaku Co Ltd
Application granted granted Critical
Publication of DE69636206D1 publication Critical patent/DE69636206D1/de
Publication of DE69636206T2 publication Critical patent/DE69636206T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0027—Powdering
    • B01J37/0045—Drying a slurry, e.g. spray drying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/15—X-ray diffraction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/002—Mixed oxides other than spinels, e.g. perovskite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B01J23/88—Molybdenum
    • B01J23/887—Molybdenum containing in addition other metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/8877—Vanadium, tantalum, niobium or polonium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
    • B01J35/34—Mechanical properties
    • B01J35/38—Abrasion or attrition resistance
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/612—Surface area less than 10 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/66—Pore distribution
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C07C51/252—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
    • B01J35/34—Mechanical properties
    • B01J35/36—Mechanical strength
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0236—Drying, e.g. preparing a suspension, adding a soluble salt and drying

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DE69636206T 1995-03-03 1996-03-01 Verfahren zur Herstellung eines Katalysators Expired - Lifetime DE69636206T2 (de)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
JP6895195 1995-03-03
JP6895195 1995-03-03
JP6394796 1996-02-27
JP06394796A JP3786297B2 (ja) 1995-03-03 1996-02-27 触媒の製造方法
PCT/JP1996/000506 WO1996027437A1 (en) 1995-03-03 1996-03-01 Catalyst and process for producing the same

Publications (2)

Publication Number Publication Date
DE69636206D1 DE69636206D1 (de) 2006-07-20
DE69636206T2 true DE69636206T2 (de) 2006-10-05

Family

ID=26405078

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69636206T Expired - Lifetime DE69636206T2 (de) 1995-03-03 1996-03-01 Verfahren zur Herstellung eines Katalysators

Country Status (9)

Country Link
US (1) US5959143A (enrdf_load_stackoverflow)
EP (2) EP1375466A1 (enrdf_load_stackoverflow)
JP (1) JP3786297B2 (enrdf_load_stackoverflow)
CN (1) CN1087658C (enrdf_load_stackoverflow)
BR (1) BR9605919A (enrdf_load_stackoverflow)
DE (1) DE69636206T2 (enrdf_load_stackoverflow)
MY (1) MY113436A (enrdf_load_stackoverflow)
TW (1) TW372888B (enrdf_load_stackoverflow)
WO (1) WO1996027437A1 (enrdf_load_stackoverflow)

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FR2760009A1 (fr) * 1997-02-27 1998-08-28 Atochem Elf Sa Procede de fabrication d'acide acrylique a partir de l'acroleine par reaction redox et l'utilisation d'une composition solide d'oxydes mixtes comme systeme redox dans ladite reaction
DE19815278A1 (de) * 1998-04-06 1999-10-07 Basf Ag Multimetalloxidmassen
DE19815281A1 (de) 1998-04-06 1999-10-07 Basf Ag Multimetalloxidmassen
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KR100373895B1 (ko) * 1998-08-28 2003-02-26 아사히 가세이 가부시키가이샤 프로판 또는 이소부탄으로부터 아크릴로니트릴 또는메트아크릴로니트릴을 제조하는데 사용하기 위한 산화물촉매의 제조 방법
JP4247565B2 (ja) 1999-03-10 2009-04-02 東亞合成株式会社 アクリル酸製造用の触媒およびそれを用いたアクリル酸の製造方法
US6762148B2 (en) 1999-09-17 2004-07-13 Nippon Kayaku Kabushiki Kaisha Catalyst process of making
JP3883755B2 (ja) * 1999-09-17 2007-02-21 日本化薬株式会社 触媒の製造方法
US6531631B1 (en) 2000-04-28 2003-03-11 Saudi Basic Industries Corporation Oxidation of ethane to acetic acid and ethylene using molybdenum and vanadium based catalysts
US6444845B1 (en) 2000-04-28 2002-09-03 Saudia Basic Industries Corporation Process for the oxidation of unsaturated aldehydes to produce carboxylic acids using Mo-V based catalysts
DE10046928A1 (de) * 2000-09-21 2002-04-11 Basf Ag Verfahren zur Herstellung von Multimetalloxidmassen
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JP4295521B2 (ja) 2003-02-13 2009-07-15 株式会社日本触媒 アクリル酸製造用触媒およびアクリル酸の製造方法
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JP4442317B2 (ja) * 2004-05-21 2010-03-31 三菱化学株式会社 複合酸化物触媒の製造方法
JP4783249B2 (ja) * 2006-09-15 2011-09-28 日本化薬株式会社 複合金属酸化物触媒及び複合金属酸化物触媒の製造方法
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CN104437527A (zh) * 2013-09-24 2015-03-25 中国石油化工股份有限公司 丙烯酸成型催化剂及其制备方法
WO2015053269A1 (ja) * 2013-10-10 2015-04-16 日本化薬株式会社 不飽和カルボン酸の製造方法、及び担持触媒
CN105664960A (zh) * 2014-11-20 2016-06-15 中国石油化工股份有限公司 丙烯酸成型催化剂
CN104772104B (zh) * 2015-03-19 2017-01-04 中国工程物理研究院材料研究所 一种用于制备固定床反应器填料的方法
JP6447327B2 (ja) * 2015-04-02 2019-01-09 三菱ケミカル株式会社 複合酸化物触媒、それを用いたアクロレイン及びアクリル酸の製造方法
JP6799581B2 (ja) 2015-08-24 2020-12-16 ローム アンド ハース カンパニーＲｏｈｍ Ａｎｄ Ｈａａｓ Ｃｏｍｐａｎｙ モノマー生成で使用するための材料の不活性度を決定する方法
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JP6452169B2 (ja) 2016-09-14 2019-01-16 日本化薬株式会社 アクリル酸製造用触媒ならびにアクリル酸の製造方法
JP6668207B2 (ja) * 2016-09-15 2020-03-18 日本化薬株式会社 アクリル酸製造用触媒
KR20220004141A (ko) 2019-05-02 2022-01-11 다우 글로벌 테크놀로지스 엘엘씨 아크릴산 제조에서 고활성 및 고선택성 촉매를 사용한 알데히드 부산물의 저감 공정
JP7459589B2 (ja) * 2020-03-18 2024-04-02 三菱ケミカル株式会社 アクリル酸合成用触媒の製造方法
JP7347282B2 (ja) * 2020-03-18 2023-09-20 三菱ケミカル株式会社 不飽和カルボン酸合成用触媒の製造方法
KR20230002897A (ko) * 2020-04-21 2023-01-05 바스프 에스이 원소 Mo, W, V 및 Cu를 함유하는 촉매 활성 다원소 산화물의 제조 방법
CN116033968B (zh) 2020-09-03 2024-10-01 株式会社日本触媒 丙烯酸制造用催化剂及其制造方法、以及丙烯酸的制造方法
CN118119448A (zh) * 2021-10-14 2024-05-31 日本化药株式会社 不饱和羧酸制造用催化剂及其制造方法以及不饱和羧酸的制造方法
WO2024120861A1 (de) 2022-12-07 2024-06-13 Basf Se Verfahren zur herstellung eines die elemente mo, w, v, cu und sb enthaltenden katalytisch aktiven multielementoxids
JP7649426B2 (ja) 2022-12-20 2025-03-19 日本化薬株式会社 触媒及びそれを用いた化合物の製造方法
JP7667381B1 (ja) * 2023-09-15 2025-04-22 日本化薬株式会社 不飽和カルボン酸製造用触媒および不飽和カルボン酸の製造方法
WO2025125092A1 (de) 2023-12-14 2025-06-19 Basf Se Verfahren zur herstellung eines die elemente mo, w, v, cu und sb enthaltenden katalytisch aktiven multielementoxids

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MX9605309A (es) 1998-07-31
DE69636206D1 (de) 2006-07-20
JP3786297B2 (ja) 2006-06-14
MY113436A (en) 2002-02-28
EP0758562A1 (en) 1997-02-19
JPH08299797A (ja) 1996-11-19
EP1375466A1 (en) 2004-01-02
US5959143A (en) 1999-09-28
MX198952B (enrdf_load_stackoverflow) 2000-10-06
EP0758562B1 (en) 2006-06-07
WO1996027437A1 (en) 1996-09-12
TW372888B (enrdf_load_stackoverflow) 1999-11-01
EP0758562A4 (en) 1997-11-05
BR9605919A (pt) 1997-11-18
CN1087658C (zh) 2002-07-17

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