DE69636206T2 - Verfahren zur Herstellung eines Katalysators - Google Patents

Verfahren zur Herstellung eines Katalysators Download PDF

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Publication number
DE69636206T2
DE69636206T2 DE69636206T DE69636206T DE69636206T2 DE 69636206 T2 DE69636206 T2 DE 69636206T2 DE 69636206 T DE69636206 T DE 69636206T DE 69636206 T DE69636206 T DE 69636206T DE 69636206 T2 DE69636206 T2 DE 69636206T2
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DE
Germany
Prior art keywords
catalyst
catalytically active
parts
active ingredient
powder
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69636206T
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German (de)
English (en)
Other versions
DE69636206D1 (de
Inventor
Hideki Sugi
Fumio Sakai
Koichi Yamato-shi Wada
Kazuo Annaka-shi SHIRAISHI
Toshitake Sawa-gun KOJIMA
Atsushi Sawa-gun UMEJIMA
Yoshimasa Asa-gun SEO
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Nippon Kayaku Co Ltd
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Nippon Kayaku Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
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Publication of DE69636206D1 publication Critical patent/DE69636206D1/de
Application granted granted Critical
Publication of DE69636206T2 publication Critical patent/DE69636206T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0027—Powdering
    • B01J37/0045—Drying a slurry, e.g. spray drying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/002—Mixed oxides other than spinels, e.g. perovskite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B01J23/88—Molybdenum
    • B01J23/887—Molybdenum containing in addition other metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/8877—Vanadium, tantalum, niobium or polonium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
    • B01J35/34—Mechanical properties
    • B01J35/38—Abrasion or attrition resistance
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/612—Surface area less than 10 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/66—Pore distribution
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C07C51/252—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/15—X-ray diffraction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
    • B01J35/34—Mechanical properties
    • B01J35/36—Mechanical strength
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0236—Drying, e.g. preparing a suspension, adding a soluble salt and drying

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DE69636206T 1995-03-03 1996-03-01 Verfahren zur Herstellung eines Katalysators Expired - Lifetime DE69636206T2 (de)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
JP6895195 1995-03-03
JP6895195 1995-03-03
JP6394796 1996-02-27
JP06394796A JP3786297B2 (ja) 1995-03-03 1996-02-27 触媒の製造方法
PCT/JP1996/000506 WO1996027437A1 (en) 1995-03-03 1996-03-01 Catalyst and process for producing the same

Publications (2)

Publication Number Publication Date
DE69636206D1 DE69636206D1 (de) 2006-07-20
DE69636206T2 true DE69636206T2 (de) 2006-10-05

Family

ID=26405078

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69636206T Expired - Lifetime DE69636206T2 (de) 1995-03-03 1996-03-01 Verfahren zur Herstellung eines Katalysators

Country Status (9)

Country Link
US (1) US5959143A (cg-RX-API-DMAC7.html)
EP (2) EP0758562B1 (cg-RX-API-DMAC7.html)
JP (1) JP3786297B2 (cg-RX-API-DMAC7.html)
CN (1) CN1087658C (cg-RX-API-DMAC7.html)
BR (1) BR9605919A (cg-RX-API-DMAC7.html)
DE (1) DE69636206T2 (cg-RX-API-DMAC7.html)
MY (1) MY113436A (cg-RX-API-DMAC7.html)
TW (1) TW372888B (cg-RX-API-DMAC7.html)
WO (1) WO1996027437A1 (cg-RX-API-DMAC7.html)

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DE19815280A1 (de) * 1998-04-06 1999-10-07 Basf Ag Multimetalloxidmassen
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JP4247565B2 (ja) * 1999-03-10 2009-04-02 東亞合成株式会社 アクリル酸製造用の触媒およびそれを用いたアクリル酸の製造方法
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US6531631B1 (en) 2000-04-28 2003-03-11 Saudi Basic Industries Corporation Oxidation of ethane to acetic acid and ethylene using molybdenum and vanadium based catalysts
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JP5134745B2 (ja) * 2001-09-19 2013-01-30 株式会社日本触媒 アクリル酸の製造方法
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JP4442317B2 (ja) * 2004-05-21 2010-03-31 三菱化学株式会社 複合酸化物触媒の製造方法
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JP6668207B2 (ja) * 2016-09-15 2020-03-18 日本化薬株式会社 アクリル酸製造用触媒
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WO2021152916A1 (ja) * 2020-01-31 2021-08-05 三菱ケミカル株式会社 触媒の製造方法及びアクリル酸の製造方法
JP7347282B2 (ja) * 2020-03-18 2023-09-20 三菱ケミカル株式会社 不飽和カルボン酸合成用触媒の製造方法
JP7459589B2 (ja) * 2020-03-18 2024-04-02 三菱ケミカル株式会社 アクリル酸合成用触媒の製造方法
US12343708B2 (en) * 2020-04-21 2025-07-01 Basf Se Method for producing a catalytically active multi-element oxide containing the elements Mo, W, V and Cu
JP7360557B2 (ja) 2020-09-03 2023-10-12 株式会社日本触媒 アクリル酸製造用触媒とその製造方法およびアクリル酸の製造方法
CN118119448A (zh) * 2021-10-14 2024-05-31 日本化药株式会社 不饱和羧酸制造用催化剂及其制造方法以及不饱和羧酸的制造方法
WO2024120861A1 (de) 2022-12-07 2024-06-13 Basf Se Verfahren zur herstellung eines die elemente mo, w, v, cu und sb enthaltenden katalytisch aktiven multielementoxids
CN120379761A (zh) 2022-12-20 2025-07-25 日本化药株式会社 催化剂和使用该催化剂的化合物的制造方法
KR20250160945A (ko) 2023-03-23 2025-11-14 닛뽄 가야쿠 가부시키가이샤 불포화 카본산 제조용 촉매
KR20260073347A (ko) 2023-09-15 2026-05-21 닛뽄 가야쿠 가부시키가이샤 불포화 카본산 제조용 촉매 및 불포화 카본산의 제조 방법
WO2025125092A1 (de) 2023-12-14 2025-06-19 Basf Se Verfahren zur herstellung eines die elemente mo, w, v, cu und sb enthaltenden katalytisch aktiven multielementoxids

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BR9605919A (pt) 1997-11-18
EP1375466A1 (en) 2004-01-02
JPH08299797A (ja) 1996-11-19
EP0758562A4 (en) 1997-11-05
TW372888B (cg-RX-API-DMAC7.html) 1999-11-01
EP0758562B1 (en) 2006-06-07
CN1087658C (zh) 2002-07-17
MX198952B (cg-RX-API-DMAC7.html) 2000-10-06
WO1996027437A1 (en) 1996-09-12
EP0758562A1 (en) 1997-02-19
MY113436A (en) 2002-02-28
US5959143A (en) 1999-09-28
DE69636206D1 (de) 2006-07-20
JP3786297B2 (ja) 2006-06-14
CN1148352A (zh) 1997-04-23
MX9605309A (es) 1998-07-31

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