DE69634930D1 - Verfahren zur herstellung von polyoxyalkylenpolyolen, mit einem niedrigen gehalt an übergangsmetallen, die unter verwendung von doppelmetallcyanidkomplexkatalysatoren hergestellt wunden - Google Patents

Verfahren zur herstellung von polyoxyalkylenpolyolen, mit einem niedrigen gehalt an übergangsmetallen, die unter verwendung von doppelmetallcyanidkomplexkatalysatoren hergestellt wunden

Info

Publication number
DE69634930D1
DE69634930D1 DE69634930T DE69634930T DE69634930D1 DE 69634930 D1 DE69634930 D1 DE 69634930D1 DE 69634930 T DE69634930 T DE 69634930T DE 69634930 T DE69634930 T DE 69634930T DE 69634930 D1 DE69634930 D1 DE 69634930D1
Authority
DE
Germany
Prior art keywords
transition metals
low content
metal cyanide
double metal
cyanide complex
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69634930T
Other languages
English (en)
Other versions
DE69634930T2 (de
Inventor
Yiannakis Televantos
Bi Le-Khac
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bayer Antwerpen NV
Original Assignee
Bayer Antwerpen NV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=24310993&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=DE69634930(D1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Bayer Antwerpen NV filed Critical Bayer Antwerpen NV
Publication of DE69634930D1 publication Critical patent/DE69634930D1/de
Application granted granted Critical
Publication of DE69634930T2 publication Critical patent/DE69634930T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645—Metals or compounds thereof, e.g. salts
    • C08G65/2663—Metal cyanide catalysts, i.e. DMC's
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/04—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers only
    • C08G65/06—Cyclic ethers having no atoms other than carbon and hydrogen outside the ring
    • C08G65/08—Saturated oxiranes
    • C08G65/10—Saturated oxiranes characterised by the catalysts used
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts
DE69634930T 1995-12-22 1996-12-19 Verfahren zur herstellung von polyoxyalkylenpolyolen, mit einem niedrigen gehalt an übergangsmetallen, die unter verwendung von doppelmetallcyanidkomplexkatalysatoren hergestellt wunden Expired - Lifetime DE69634930T2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US577986 1990-09-05
US08/577,986 US5767323A (en) 1995-12-22 1995-12-22 Process for preparing polyoxyalkylene polyether polyols having low levels of transition metals through double metal cyanide complex polyoxyalkylation
PCT/EP1996/005708 WO1997023544A1 (en) 1995-12-22 1996-12-19 Process for the preparation of polyoxyalkylene polyether polyols having low levels of transition metals, prepared using double metal cyanide complex catalyst

Publications (2)

Publication Number Publication Date
DE69634930D1 true DE69634930D1 (de) 2005-08-18
DE69634930T2 DE69634930T2 (de) 2006-04-20

Family

ID=24310993

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69634930T Expired - Lifetime DE69634930T2 (de) 1995-12-22 1996-12-19 Verfahren zur herstellung von polyoxyalkylenpolyolen, mit einem niedrigen gehalt an übergangsmetallen, die unter verwendung von doppelmetallcyanidkomplexkatalysatoren hergestellt wunden

Country Status (16)

Country Link
US (1) US5767323A (de)
EP (1) EP0868468B1 (de)
JP (1) JP4102902B2 (de)
KR (1) KR100483237B1 (de)
CN (1) CN1083853C (de)
AR (1) AR005181A1 (de)
AU (1) AU715766B2 (de)
BR (1) BR9612255A (de)
CZ (1) CZ293882B6 (de)
DE (1) DE69634930T2 (de)
ES (1) ES2243955T3 (de)
MX (1) MX9804568A (de)
PL (1) PL186302B1 (de)
RU (1) RU2178426C2 (de)
TW (1) TW420690B (de)
WO (1) WO1997023544A1 (de)

Families Citing this family (41)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AR019107A1 (es) * 1998-04-27 2001-12-26 Dow Global Technologies Inc Polioles de alto peso molecular, proceso para su preparacion y uso de los mismos.
DE19917897A1 (de) * 1999-04-20 2000-10-26 Basf Ag Verfahren zur Herstellung von Polyurethanen
US6423662B1 (en) 1999-07-09 2002-07-23 Dow Global Technologies Inc. Incipient wetness method for making metal-containing cyanide catalysts
US6376645B1 (en) * 1999-07-09 2002-04-23 The Dow Chemical Company Complexing agent-modified hexacyanometallate hexanitrometallate catalysts
DE19937114C2 (de) 1999-08-06 2003-06-18 Bayer Ag Verfahren zur Herstellung von Polyetherpolyolen
DE19949091A1 (de) * 1999-10-12 2001-04-26 Basf Ag Polyester-Polyetherblockcopolymere
DE10008635A1 (de) † 2000-02-24 2001-09-06 Basf Ag Verfahren zur Herstellung von Polyetherpolyolen
JP2003525328A (ja) 2000-02-29 2003-08-26 ビーエーエスエフ アクチェンゲゼルシャフト 多金属シアニド化合物の製造方法
US6642171B2 (en) 2000-04-28 2003-11-04 Synuthane International, Inc. Double metal cyanide catalysts containing polyglycol ether complexing agents
US6429166B1 (en) 2000-05-19 2002-08-06 Dow Global Technologies Inc. Method for preparing metal cyanide catalyst/polyol initiator slurries
US6635737B1 (en) 2000-05-26 2003-10-21 Williamette Valley Company Polymers derived from low unsaturation polyamines
DE10137628A1 (de) * 2001-08-03 2003-02-27 Basf Ag Verfahren zur Herstellung von Polyurethan-Weichschaumstoffen
DE10142747A1 (de) * 2001-08-31 2003-03-20 Bayer Ag Doppelmetallcyanid-Katalysatoren für die Herstellung von Polyetherpolyolen
US6716788B2 (en) * 2002-06-14 2004-04-06 Shell Oil Company Preparation of a double metal cyanide catalyst
US6977236B2 (en) * 2002-06-14 2005-12-20 Shell Oil Company Preparation of a double metal cyanide catalyst
US6835801B2 (en) * 2002-07-19 2004-12-28 Bayer Antwerp, N.V. Activated starter mixtures and the processes related thereto
ZA200506576B (en) * 2003-03-07 2006-12-27 Dow Global Technologies Inc Continuous process and system of producing polyether polyols
EP1632517B1 (de) * 2003-06-04 2009-07-22 Asahi Glass Company Ltd. Mischmetallcyanidkomplexkatalysator, herstellungsverfahren dafür und verwendung davon
JP4273876B2 (ja) * 2003-08-25 2009-06-03 旭硝子株式会社 ポリエーテルモノオールまたはポリエーテルポリオールおよびその製造方法
DE602004025022D1 (de) 2003-10-06 2010-02-25 Kaneka Corp Haftklebemittel
JP2007284586A (ja) * 2006-04-18 2007-11-01 Asahi Glass Co Ltd ポリエーテルモノオールの製造方法
US8093351B2 (en) * 2006-08-24 2012-01-10 Cornell Research Foundation, Inc. Copolymerization of propylene oxide and carbon dioxide and homopolymerization of propylene oxide
WO2008026657A1 (fr) 2006-08-31 2008-03-06 Asahi Glass Company, Limited Procédé de purification d'un composé polyéther
DE102007057147A1 (de) 2007-11-28 2009-06-04 Evonik Goldschmidt Gmbh Verfahren zur Alkoxylierung mit DMC-Katalysatoren im Schlaufenreaktor mit Strahlsauger
JP5716668B2 (ja) 2009-09-30 2015-05-13 旭硝子株式会社 イソシアネート基末端プレポリマーの製造方法およびポリウレタン樹脂の製造方法
AU2010304291A1 (en) 2009-10-05 2012-05-03 Asahi Glass Company, Limited Polyethers and method for producing the same
DE102009046269A1 (de) 2009-10-30 2011-05-05 Henkel Ag & Co. Kgaa Harnstoffgebundende Alkoxysilane zum Einsatz in Dicht- und Klebstoffen
WO2012114357A1 (en) * 2011-02-23 2012-08-30 Council Of Scientific & Industrial Research Process for preparing hyperbranched polyestersfield of the invention
EP2548907A1 (de) * 2011-07-18 2013-01-23 Bayer MaterialScience AG Verfahren zur Herstellung von Polyetherpolyolen
US10358404B2 (en) 2012-06-21 2019-07-23 Covestro Llc Process for the production of low molecular weight impact polyethers
EP2703425A1 (de) * 2012-08-27 2014-03-05 Bayer MaterialScience AG Verfahren zur Herstellung von Polyethercarbonatpolyolen
US9890100B2 (en) * 2013-03-14 2018-02-13 Covestro Llc Continuous process for the production of low molecular weight polyethers with a DMC catalyst
US9051412B2 (en) 2013-03-14 2015-06-09 Bayer Materialscience Llc Base-catalyzed, long chain, active polyethers from short chain DMC-catalyzed starters
US10669368B2 (en) 2013-03-15 2020-06-02 Covestro Llc Method to increase the resistance of double metal cyanide catalysts to deactivation
KR20180044908A (ko) 2015-08-26 2018-05-03 코베스트로 도이칠란트 아게 고분자량 폴리옥시알킬렌 폴리올의 제조 방법
KR20210005600A (ko) 2018-04-25 2021-01-14 헨켈 아게 운트 코. 카게아아 히드록실-관능화된 폴리에테르-폴리실록산 블록 공중합체의 제조 방법
EP3810677A1 (de) 2018-06-19 2021-04-28 Henkel AG & Co. KGaA Hochaktive doppelmetallcyanid-verbindungen
EP3663371B1 (de) 2018-12-06 2024-03-13 Henkel AG & Co. KGaA Herstellung von polysiloxan-polyalkyleneglycol-bürsten-copolymeren
EP3663372B1 (de) 2018-12-06 2024-03-13 Henkel AG & Co. KGaA Härtbare zusammensetzung mit polysiloxan-polyalkylenglycol-bürstencopolymeren
EP3932973A1 (de) 2020-07-01 2022-01-05 Henkel AG & Co. KGaA Bifunktionalisierte polysiloxanbürstencopolymere
WO2022160078A1 (zh) * 2021-01-26 2022-08-04 万华化学集团股份有限公司 一种用于环氧化物连续聚合的诱导体系、诱导剂以及环氧化物连续聚合的方法

Family Cites Families (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3427256A (en) * 1963-02-14 1969-02-11 Gen Tire & Rubber Co Double metal cyanide complex compounds
US3427334A (en) * 1963-02-14 1969-02-11 Gen Tire & Rubber Co Double metal cyanides complexed with an alcohol aldehyde or ketone to increase catalytic activity
US3427335A (en) * 1963-02-14 1969-02-11 Gen Tire & Rubber Co Double metal cyanides complexed with an acyclic aliphatic saturated monoether,an ester and a cyclic ether and methods for making the same
US3393243A (en) * 1964-09-24 1968-07-16 Jefferson Chem Co Inc Process of preparing polyoxypropylene polyether polyols
US3829505A (en) * 1970-02-24 1974-08-13 Gen Tire & Rubber Co Polyethers and method for making the same
US3941849A (en) * 1972-07-07 1976-03-02 The General Tire & Rubber Company Polyethers and method for making the same
DE2900167C2 (de) * 1979-01-03 1983-02-10 Vsesojuznyj naučno-issledovatel'skij institut sintetičeskich smol, Vladimir Kontinuierliches Verfahren zur Herstellung von Polyäthern
US4239879A (en) * 1979-06-25 1980-12-16 The General Tire & Rubber Company Thermoplastic polyurethane prepared from a poly-1,2-propylene ether glycol, a low molecular weight glycol and 2,4-tolylene diisocyanate
US4282387A (en) * 1979-12-26 1981-08-04 The Dow Chemical Company Process for preparing polyols
CA1155871A (en) * 1980-10-16 1983-10-25 Gencorp Inc. Method for treating polypropylene ether and poly-1,2- butylene ether polyols
AU552988B2 (en) * 1982-03-31 1986-06-26 Shell Internationale Research Maatschappij B.V. Polymerizing epoxides and catalyst suspensions for this
AU551979B2 (en) * 1982-03-31 1986-05-15 Shell Internationale Research Maatschappij B.V. Epoxy polymerisation catalysts
US4721818A (en) * 1987-03-20 1988-01-26 Atlantic Richfield Company Purification of polyols prepared using double metal cyanide complex catalysts
US5010187A (en) * 1988-11-18 1991-04-23 Dow Chemical Company Production of polyether polyols with reduced unsaturation
US5114619A (en) * 1989-07-14 1992-05-19 The Dow Chemical Company Production of polyether polyols with reduced unsaturation
US4987271A (en) * 1989-02-17 1991-01-22 Asahi Glass Company, Ltd. Method for purifying a polyoxyalkylene alcohol
US5010047A (en) * 1989-02-27 1991-04-23 Arco Chemical Technology, Inc. Recovery of double metal cyanide complex catalyst from a polymer
JP2995568B2 (ja) * 1989-05-09 1999-12-27 旭硝子株式会社 ポリアルキレンオキシド誘導体の製造法
JP2595766B2 (ja) * 1990-05-25 1997-04-02 旭硝子株式会社 ポリオキシアルキレンアルコールの製造方法
JP3025312B2 (ja) * 1990-12-18 2000-03-27 旭硝子株式会社 ポリエーテル類の製造法
US5158922A (en) * 1992-02-04 1992-10-27 Arco Chemical Technology, L.P. Process for preparing metal cyanide complex catalyst
JPH05247199A (ja) * 1992-03-04 1993-09-24 Asahi Glass Co Ltd ポリエーテル類の製造方法
US5248833A (en) * 1992-09-22 1993-09-28 Arco Chemical Technology, L.P. Process for purifying polyols made with double metal cyanide catalysts
JP3357110B2 (ja) * 1993-02-03 2002-12-16 旭硝子株式会社 ポリマー分散ポリオールの製造方法
US5470813A (en) * 1993-11-23 1995-11-28 Arco Chemical Technology, L.P. Double metal cyanide complex catalysts
US5482908A (en) * 1994-09-08 1996-01-09 Arco Chemical Technology, L.P. Highly active double metal cyanide catalysts
US5627122A (en) * 1995-07-24 1997-05-06 Arco Chemical Technology, L.P. Highly active double metal cyanide complex catalysts

Also Published As

Publication number Publication date
PL186302B1 (pl) 2003-12-31
CZ196598A3 (cs) 1999-01-13
MX9804568A (es) 1998-09-30
ES2243955T3 (es) 2005-12-01
US5767323A (en) 1998-06-16
CZ293882B6 (cs) 2004-08-18
CN1208426A (zh) 1999-02-17
JP4102902B2 (ja) 2008-06-18
WO1997023544A1 (en) 1997-07-03
TW420690B (en) 2001-02-01
EP0868468B1 (de) 2005-07-13
EP0868468A1 (de) 1998-10-07
AU1302797A (en) 1997-07-17
DE69634930T2 (de) 2006-04-20
KR19990071642A (ko) 1999-09-27
JP2000513389A (ja) 2000-10-10
AR005181A1 (es) 1999-04-14
AU715766B2 (en) 2000-02-10
CN1083853C (zh) 2002-05-01
BR9612255A (pt) 1999-07-13
KR100483237B1 (ko) 2005-11-16
PL327313A1 (en) 1998-12-07
RU2178426C2 (ru) 2002-01-20

Similar Documents

Publication Publication Date Title
DE69634930D1 (de) Verfahren zur herstellung von polyoxyalkylenpolyolen, mit einem niedrigen gehalt an übergangsmetallen, die unter verwendung von doppelmetallcyanidkomplexkatalysatoren hergestellt wunden
ATE199094T1 (de) Verfahren zur herstellung von ethylenoxid verkappten polyolen aus doppelmetallcyanid katalysierten polyolen
DE69609958D1 (de) Verfahren zur herstellung von produkten, die bisalze der ameisensäure enthalten
DE349277T1 (de) Verfahren zur herstellung von synthetischem schmieroel durch olefinoligomerisation.
DE3876732T2 (de) Verfahren zur herstellung eines kohlenstoff-kohlenstoff-verbundkoerpers von hoher festigkeit.
DE69315161T2 (de) Verfahren zur Reinigung von Polyolen, die mit Doppelmetallcyanidkatalysatoren hergestellt wurden
DE69500993T2 (de) Verfahren zur herstellung von metallcarbidpulvern
DE59703441D1 (de) Verfahren zur herstellung von geträgerten übergangsmetallkatalysatoren
DE69628421D1 (de) Verfahren zur herstellung von tetraazacycloalkanen.
ATE223364T1 (de) Verfahren zur kondensation von cyanwasserstoff mit einem aldehyd
DE59602619D1 (de) Verfahren zur herstellung von tetrahydrofuranpolymeren
ATE253407T1 (de) Verfahren zur herstellung eines katalysators für die bereitung von vinylacetat
DE69418581D1 (de) Verfahren zur herstellung dünner bleche, geeignet für die anfertigung von dosenteilen
DE3876071T2 (de) Verfahren zur herstellung von edelmetalloxydations-katalysatoren.
DE59001349D1 (de) Verfahren zur herstellung katalytisch wirksamer beschichtigungen fuer die cyanwasserstoffherstellung.
DE68916418T2 (de) Verfahren zur herstellung von übergangsmetallnitridwhiskern.
DE68902702D1 (de) Verfahren zur herstellung von synthetischem schmieroel durch olefinoligomerisation.
DE69001319D1 (de) Verfahren zur herstellung eines katalysators fuer die demerisation von butadien.
DE69015150T2 (de) Verfahren zur herstellung gesinterten karbids oder cermetlegierung.
DE69610421T2 (de) Verfahren zur herstellung von alpha,beta-ungesättigten nitrilen
DE69617713D1 (de) Übergangsmetallkomplexe, katalysatoren für die olefinpolymerisation und verfahren zur herstellung von olefinpolymeren
AT399885B (de) Verfahren zur herstellung von zellinien, die monoklonale antikörper produzieren
DE69621628T2 (de) Verfahren zur herstellung von ammoxidationskatalysatoren
DE3861839D1 (de) Verfahren zur herstellung von alkalimetallnitraten.
DE3585269D1 (de) Verfahren zur herstellung eines thermoplastischen harzes.

Legal Events

Date Code Title Description
8363 Opposition against the patent