DE2739704C3 - Verfahren zur Herstellung kubischer Calciumcarbonatkristalle - Google Patents
Verfahren zur Herstellung kubischer CalciumcarbonatkristalleInfo
- Publication number
- DE2739704C3 DE2739704C3 DE2739704A DE2739704A DE2739704C3 DE 2739704 C3 DE2739704 C3 DE 2739704C3 DE 2739704 A DE2739704 A DE 2739704A DE 2739704 A DE2739704 A DE 2739704A DE 2739704 C3 DE2739704 C3 DE 2739704C3
- Authority
- DE
- Germany
- Prior art keywords
- crystals
- calcium carbonate
- cubic
- suspension
- size
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 title claims description 123
- 239000013078 crystal Substances 0.000 title claims description 96
- 229910000019 calcium carbonate Inorganic materials 0.000 title claims description 61
- 238000004519 manufacturing process Methods 0.000 title claims description 7
- 238000000034 method Methods 0.000 title description 31
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 54
- 239000000725 suspension Substances 0.000 description 37
- 239000000920 calcium hydroxide Substances 0.000 description 36
- 235000011116 calcium hydroxide Nutrition 0.000 description 36
- 238000006243 chemical reaction Methods 0.000 description 34
- 239000001569 carbon dioxide Substances 0.000 description 27
- 229910002092 carbon dioxide Inorganic materials 0.000 description 27
- 239000007900 aqueous suspension Substances 0.000 description 24
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 24
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 24
- 239000000203 mixture Substances 0.000 description 21
- 238000003763 carbonization Methods 0.000 description 18
- 239000000047 product Substances 0.000 description 11
- 239000007787 solid Substances 0.000 description 11
- 239000011248 coating agent Substances 0.000 description 10
- 238000000576 coating method Methods 0.000 description 10
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 5
- 229910052791 calcium Inorganic materials 0.000 description 5
- 239000011575 calcium Substances 0.000 description 5
- 238000002156 mixing Methods 0.000 description 5
- 239000007921 spray Substances 0.000 description 5
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 4
- 239000000049 pigment Substances 0.000 description 4
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 3
- 229910052783 alkali metal Inorganic materials 0.000 description 3
- -1 alkali metal bicarbonate Chemical class 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 238000002425 crystallisation Methods 0.000 description 3
- 230000008025 crystallization Effects 0.000 description 3
- 238000009826 distribution Methods 0.000 description 3
- 238000000227 grinding Methods 0.000 description 3
- 239000003973 paint Substances 0.000 description 3
- 229920003002 synthetic resin Polymers 0.000 description 3
- 239000000057 synthetic resin Substances 0.000 description 3
- 238000004438 BET method Methods 0.000 description 2
- 238000004220 aggregation Methods 0.000 description 2
- 230000002776 aggregation Effects 0.000 description 2
- 229920000180 alkyd Polymers 0.000 description 2
- 244000052616 bacterial pathogen Species 0.000 description 2
- 239000002585 base Substances 0.000 description 2
- 239000011324 bead Substances 0.000 description 2
- 239000013065 commercial product Substances 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000000945 filler Substances 0.000 description 2
- 238000009472 formulation Methods 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 235000017557 sodium bicarbonate Nutrition 0.000 description 2
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 description 1
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- 239000004606 Fillers/Extenders Substances 0.000 description 1
- 235000019738 Limestone Nutrition 0.000 description 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
- 235000010678 Paulownia tomentosa Nutrition 0.000 description 1
- 240000002834 Paulownia tomentosa Species 0.000 description 1
- HUGKFZUKOLGVHG-UHFFFAOYSA-N [Ca][Ca][Ca] Chemical compound [Ca][Ca][Ca] HUGKFZUKOLGVHG-UHFFFAOYSA-N 0.000 description 1
- MJUDLWQWPKWWPB-UHFFFAOYSA-K [OH-].[Ca+2].[Ca+2].[O-]C([O-])=O Chemical compound [OH-].[Ca+2].[Ca+2].[O-]C([O-])=O MJUDLWQWPKWWPB-UHFFFAOYSA-K 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 239000000976 ink Substances 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000011147 inorganic material Substances 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 238000004898 kneading Methods 0.000 description 1
- 239000004816 latex Substances 0.000 description 1
- 229920000126 latex Polymers 0.000 description 1
- 239000006028 limestone Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000010907 mechanical stirring Methods 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 238000010899 nucleation Methods 0.000 description 1
- 230000006911 nucleation Effects 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 239000001254 oxidized starch Substances 0.000 description 1
- 235000013808 oxidized starch Nutrition 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 229940088417 precipitated calcium carbonate Drugs 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0036—Crystallisation on to a bed of product crystals; Seeding
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F11/00—Compounds of calcium, strontium, or barium
- C01F11/18—Carbonates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/30—Particle morphology extending in three dimensions
- C01P2004/38—Particle morphology extending in three dimensions cube-like
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Paper (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11881076A JPS5343694A (en) | 1976-10-01 | 1976-10-01 | Process for producing cubic calcium carbonate having 0*111*0micron size |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2739704A1 DE2739704A1 (de) | 1978-04-06 |
| DE2739704B2 DE2739704B2 (de) | 1979-06-07 |
| DE2739704C3 true DE2739704C3 (de) | 1980-01-31 |
Family
ID=14745680
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2739704A Expired DE2739704C3 (de) | 1976-10-01 | 1977-09-02 | Verfahren zur Herstellung kubischer Calciumcarbonatkristalle |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US4124688A (OSRAM) |
| JP (1) | JPS5343694A (OSRAM) |
| DE (1) | DE2739704C3 (OSRAM) |
| FR (1) | FR2366224A1 (OSRAM) |
| GB (1) | GB1545412A (OSRAM) |
Families Citing this family (26)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4244933A (en) * | 1978-04-05 | 1981-01-13 | Shiraishi Kogyo Kaisha, Ltd. | Calcium carbonate particles and processes for preparing same |
| JPS54149399A (en) * | 1978-05-15 | 1979-11-22 | Shiraishi Kogyo Kaisha Ltd | Manufacture of cubic calcium carbonate |
| JPS5540849A (en) * | 1978-09-13 | 1980-03-22 | Shiraishi Kogyo Kaisha Ltd | Internally filled paper |
| JPS5893736A (ja) * | 1981-12-01 | 1983-06-03 | Idemitsu Petrochem Co Ltd | 樹脂組成物 |
| JPS59138259A (ja) * | 1983-01-29 | 1984-08-08 | Kanegafuchi Chem Ind Co Ltd | 硬化性組成物 |
| JPS59216996A (ja) * | 1983-05-18 | 1984-12-07 | 神崎製紙株式会社 | キャスト塗被紙の製造方法 |
| FR2729133A1 (fr) * | 1995-01-11 | 1996-07-12 | Solvay | Procede de coproduction de carbonate de calcium et d'hydroxyde de sodium |
| KR0184847B1 (ko) * | 1996-02-02 | 1999-04-15 | 유규재 | 입경별 교질탄산칼슘의 제조방법 |
| KR0182788B1 (ko) * | 1996-02-02 | 1999-04-15 | 유규재 | 초미세 교질 탄산칼슘의 제조방법 |
| AT954U3 (de) * | 1996-04-03 | 1997-01-27 | Unitechnik Thurner Anlagenbaug | Verfahren zur kontinuierlichen erzeugung von gefälltem kalziumkarbonat |
| AT403043B (de) * | 1996-04-03 | 1997-10-27 | Unitechnik Thurner Anlagenbaug | Verfahren zur kontinuierlichen erzeugung von gefälltem kalziumkarbonat |
| KR100190596B1 (ko) * | 1996-05-03 | 1999-06-01 | 규 재 유 | 0.1-1.0 마이크로미터의 탄산칼슘 제조법 |
| FR2764521B1 (fr) * | 1997-06-16 | 1999-07-16 | Inst Francais Du Petrole | Dispositif de cristallisation par detente isentropique et son utilisation |
| US6336334B1 (en) * | 1997-06-16 | 2002-01-08 | Institut Francais De Petrole | Device for crystallization by isentropic expansion and its use |
| US5961941A (en) * | 1997-06-17 | 1999-10-05 | Thermo Fibergen, Inc. | Production of precipitated calcium carbonate from papermaking sludge and sludge-derived ash |
| FR2821095B1 (fr) * | 2001-02-16 | 2003-04-11 | Arjo Wiggins Sa | Procede d'obtention d'une feuille papetiere comportant de la calcite |
| FI124696B (fi) | 2008-03-07 | 2014-12-15 | Fp Pigments Oy | Pigmenttipartikkelikoostumus, menetelmä sen valmistamiseksi sekä sen käyttö |
| CN101362048B (zh) * | 2008-09-02 | 2011-01-26 | 李发修 | 用电石渣吸收利用二氧化碳的方法与专用二氧化碳吸收器 |
| DE102009045278B4 (de) * | 2009-10-02 | 2011-12-15 | Dirk Dombrowski | Mineralisches, granuliertes Entschwefelungsmittel auf Basis von Calciumhydroxid, Verfahren zu seiner Herstellung sowie seine Verwendung |
| JP5972173B2 (ja) | 2009-12-30 | 2016-08-17 | エイボン プロダクツ インコーポレーテッド | 高い被覆性及び自然らしさを有するカラー化粧品 |
| KR101395796B1 (ko) * | 2012-01-06 | 2014-05-19 | 주식회사 포스코 | 탄산화 장치 및 이를 이용한 탄산화 방법 |
| AU2013299456B2 (en) * | 2012-08-10 | 2016-04-28 | Sparstane Technologies LLC | Process for converting FGD gypsum to ammonium sulfate and calcium carbonate |
| JP6779435B2 (ja) | 2017-02-27 | 2020-11-04 | 株式会社白石中央研究所 | 炭酸カルシウム多孔質焼結体の製造方法 |
| CN110589862B (zh) * | 2019-09-09 | 2022-04-22 | 建德华明科技有限公司 | 液相为连续相的碳化法生产纳米级碳酸钙的多级串联方法 |
| CN112408450A (zh) * | 2020-11-27 | 2021-02-26 | 广西华纳新材料科技有限公司 | 一种类立方纳米碳酸钙的制备方法 |
| JP6985775B1 (ja) | 2021-07-28 | 2021-12-22 | 株式会社Tbm | 炭酸カルシウム粒子群、樹脂組成物、及び炭酸カルシウム粒子群の製造方法 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1188505A (en) * | 1915-12-13 | 1916-06-27 | Ind Chemical Company | Calcium-carbonate manufacture. |
| US1372193A (en) * | 1919-04-26 | 1921-03-22 | Equitable Trust Company | Manufacture of calcium carbonate |
| GB562544A (en) * | 1942-08-05 | 1944-07-06 | Du Pont | Manufacture of calcium carbonate |
| US2538802A (en) * | 1947-05-03 | 1951-01-23 | Ecusta Paper Corp | Method of manufacturing calcium carbonate |
-
1976
- 1976-10-01 JP JP11881076A patent/JPS5343694A/ja active Granted
-
1977
- 1977-08-24 US US05/827,218 patent/US4124688A/en not_active Expired - Lifetime
- 1977-09-02 DE DE2739704A patent/DE2739704C3/de not_active Expired
- 1977-09-02 GB GB36782/77A patent/GB1545412A/en not_active Expired
- 1977-09-05 FR FR7726798A patent/FR2366224A1/fr active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| DE2739704A1 (de) | 1978-04-06 |
| FR2366224B1 (OSRAM) | 1981-07-03 |
| JPS5343694A (en) | 1978-04-19 |
| JPS5428397B2 (OSRAM) | 1979-09-17 |
| GB1545412A (en) | 1979-05-10 |
| DE2739704B2 (de) | 1979-06-07 |
| FR2366224A1 (fr) | 1978-04-28 |
| US4124688A (en) | 1978-11-07 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OAP | Request for examination filed | ||
| OD | Request for examination | ||
| C3 | Grant after two publication steps (3rd publication) |