DE2659295C2 - Verfahren zur Erhöhung der Reaktivität von Phosphorpentasulfid - Google Patents
Verfahren zur Erhöhung der Reaktivität von PhosphorpentasulfidInfo
- Publication number
- DE2659295C2 DE2659295C2 DE2659295A DE2659295A DE2659295C2 DE 2659295 C2 DE2659295 C2 DE 2659295C2 DE 2659295 A DE2659295 A DE 2659295A DE 2659295 A DE2659295 A DE 2659295A DE 2659295 C2 DE2659295 C2 DE 2659295C2
- Authority
- DE
- Germany
- Prior art keywords
- reactivity
- cooling
- phosphorus
- increasing
- cooling device
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 230000009257 reactivity Effects 0.000 title claims description 24
- CYQAYERJWZKYML-UHFFFAOYSA-N phosphorus pentasulfide Chemical compound S1P(S2)(=S)SP3(=S)SP1(=S)SP2(=S)S3 CYQAYERJWZKYML-UHFFFAOYSA-N 0.000 title claims description 10
- 238000000034 method Methods 0.000 title claims description 9
- 238000001816 cooling Methods 0.000 claims description 21
- 239000007788 liquid Substances 0.000 claims description 9
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 3
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 3
- 239000007795 chemical reaction product Substances 0.000 claims description 3
- 229910052698 phosphorus Inorganic materials 0.000 claims description 3
- 239000011574 phosphorus Substances 0.000 claims description 3
- 229910052717 sulfur Inorganic materials 0.000 claims description 3
- 239000011593 sulfur Substances 0.000 claims description 3
- 230000008018 melting Effects 0.000 claims description 2
- 238000002844 melting Methods 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000010791 quenching Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 238000007711 solidification Methods 0.000 description 2
- 230000008023 solidification Effects 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- NMRPBPVERJPACX-UHFFFAOYSA-N (3S)-octan-3-ol Natural products CCCCCC(O)CC NMRPBPVERJPACX-UHFFFAOYSA-N 0.000 description 1
- YIWUKEYIRIRTPP-UHFFFAOYSA-N 2-ethylhexan-1-ol Chemical compound CCCCC(CC)CO YIWUKEYIRIRTPP-UHFFFAOYSA-N 0.000 description 1
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000005496 tempering Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/14—Sulfur, selenium, or tellurium compounds of phosphorus
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Processing Of Solid Wastes (AREA)
- Furan Compounds (AREA)
Priority Applications (11)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2659295A DE2659295C2 (de) | 1976-12-29 | 1976-12-29 | Verfahren zur Erhöhung der Reaktivität von Phosphorpentasulfid |
| ES463016A ES463016A1 (es) | 1976-12-29 | 1977-10-07 | Procedimiento para aumentar una reactividad establecida de pentasulfuro de fosforo. |
| CH1547077A CH632978A5 (de) | 1976-12-29 | 1977-12-15 | Verfahren zur erhoehung der reaktivitaet von phosphorpentasulfid. |
| US05/863,081 US4173621A (en) | 1976-12-29 | 1977-12-22 | Process for improving the reactivity of phosphorus pentasulfide |
| GB53669/77A GB1554092A (en) | 1976-12-29 | 1977-12-23 | Process for the reactivity of phosphorus pentasulphide |
| IT52388/77A IT1092249B (it) | 1976-12-29 | 1977-12-28 | Procedimento per aumentare la reattivita' di pentasolfuro di fosforo |
| BE183914A BE862410A (fr) | 1976-12-29 | 1977-12-28 | Procede pour ameliorer la reactivite du pentasulfure de phosphore |
| DK582377A DK148916C (da) | 1976-12-29 | 1977-12-28 | Fremgangsmaade til foroegelse af reaktiviteten af phosphorpentasulfid |
| BR7708693A BR7708693A (pt) | 1976-12-29 | 1977-12-28 | Processo para aumentar uma dada reatividade de pentassulfeto de fosforo |
| FR7739712A FR2376070A1 (fr) | 1976-12-29 | 1977-12-29 | Procede pour ameliorer la reactivite du pentasulfure de phosphore |
| CA294,048A CA1079479A (en) | 1976-12-29 | 1977-12-29 | Process for improving the reactivity of phosphorus pentasulfide |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2659295A DE2659295C2 (de) | 1976-12-29 | 1976-12-29 | Verfahren zur Erhöhung der Reaktivität von Phosphorpentasulfid |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2659295A1 DE2659295A1 (de) | 1978-07-06 |
| DE2659295C2 true DE2659295C2 (de) | 1982-10-28 |
Family
ID=5996891
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2659295A Expired DE2659295C2 (de) | 1976-12-29 | 1976-12-29 | Verfahren zur Erhöhung der Reaktivität von Phosphorpentasulfid |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US4173621A (cg-RX-API-DMAC10.html) |
| BE (1) | BE862410A (cg-RX-API-DMAC10.html) |
| BR (1) | BR7708693A (cg-RX-API-DMAC10.html) |
| CA (1) | CA1079479A (cg-RX-API-DMAC10.html) |
| CH (1) | CH632978A5 (cg-RX-API-DMAC10.html) |
| DE (1) | DE2659295C2 (cg-RX-API-DMAC10.html) |
| DK (1) | DK148916C (cg-RX-API-DMAC10.html) |
| ES (1) | ES463016A1 (cg-RX-API-DMAC10.html) |
| FR (1) | FR2376070A1 (cg-RX-API-DMAC10.html) |
| GB (1) | GB1554092A (cg-RX-API-DMAC10.html) |
| IT (1) | IT1092249B (cg-RX-API-DMAC10.html) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2836502A1 (de) * | 1978-08-21 | 1980-03-06 | Hoechst Ag | Verfahren zur herstellung von phosphorpentasulfid bestimmter reaktivitaet |
| US5336272A (en) * | 1988-10-13 | 1994-08-09 | Mitsubishi Denki Kabushiki Kaisha | Method for molding a semiconductor package on a continuous leadframe |
| US5505885A (en) * | 1993-06-29 | 1996-04-09 | Bacardi; Jean M. | Granulation of phosphorus pentasulfide with a predetermined reactivity |
| US5464601A (en) * | 1994-03-29 | 1995-11-07 | Monsanto Company | Process for preparing sulfides of phosphorus |
| CN1141879A (zh) * | 1994-03-29 | 1997-02-05 | 孟山都公司 | 磷的硫化物的制备方法 |
| EP3148929A1 (en) * | 2014-06-02 | 2017-04-05 | Tubitak | Purification of phosphorus decasulfide (p4s10) |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA748800A (en) * | 1966-12-20 | H. Brown James | Process of preparing phosphorus sulfides | |
| US3146069A (en) * | 1959-05-27 | 1964-08-25 | Hooker Chemical Corp | Method of preparing phosphorus pentasulfide of controlled reactivity |
| US3023086A (en) * | 1959-05-27 | 1962-02-27 | Hooker Chemical Corp | Method of producing phosphorus pentasulfide of controlled reactivity |
| FR1293326A (fr) * | 1960-06-28 | 1962-05-11 | American Agricultural Chem Co | Procédé de préparation de sulfures de phosphore ayant une réactivité déterminée |
| US3282653A (en) * | 1963-02-25 | 1966-11-01 | Hooker Chemical Corp | Apparatus for three stage controlled cooling and solidification of phosphorous pentasulfide |
| FR1382814A (fr) * | 1963-03-28 | 1964-12-18 | Knapsack Ag | Procédé et appareil pour la préparation du pentasulfure de phosphore |
| DE1222480B (de) * | 1964-09-19 | 1966-08-11 | Knapsack Ag | Verfahren zur Herstellung von Phosphor-pentasulfid bestimmter Reaktionsfaehigkeit |
| US3800028A (en) * | 1971-11-12 | 1974-03-26 | Hooker Chemical Corp | Formation of highly reactive form of phosphorus pentasulfide |
| FR2216225B1 (cg-RX-API-DMAC10.html) * | 1973-01-31 | 1976-11-05 | Ugine Kuhlmann |
-
1976
- 1976-12-29 DE DE2659295A patent/DE2659295C2/de not_active Expired
-
1977
- 1977-10-07 ES ES463016A patent/ES463016A1/es not_active Expired
- 1977-12-15 CH CH1547077A patent/CH632978A5/de not_active IP Right Cessation
- 1977-12-22 US US05/863,081 patent/US4173621A/en not_active Expired - Lifetime
- 1977-12-23 GB GB53669/77A patent/GB1554092A/en not_active Expired
- 1977-12-28 IT IT52388/77A patent/IT1092249B/it active
- 1977-12-28 BR BR7708693A patent/BR7708693A/pt unknown
- 1977-12-28 DK DK582377A patent/DK148916C/da not_active IP Right Cessation
- 1977-12-28 BE BE183914A patent/BE862410A/xx not_active IP Right Cessation
- 1977-12-29 CA CA294,048A patent/CA1079479A/en not_active Expired
- 1977-12-29 FR FR7739712A patent/FR2376070A1/fr active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| FR2376070B1 (cg-RX-API-DMAC10.html) | 1982-03-26 |
| CH632978A5 (de) | 1982-11-15 |
| ES463016A1 (es) | 1978-07-16 |
| DK582377A (da) | 1978-06-30 |
| CA1079479A (en) | 1980-06-17 |
| BE862410A (fr) | 1978-06-28 |
| DE2659295A1 (de) | 1978-07-06 |
| BR7708693A (pt) | 1978-08-08 |
| FR2376070A1 (fr) | 1978-07-28 |
| DK148916C (da) | 1986-05-12 |
| DK148916B (da) | 1985-11-18 |
| US4173621A (en) | 1979-11-06 |
| GB1554092A (en) | 1979-10-17 |
| IT1092249B (it) | 1985-07-06 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8110 | Request for examination paragraph 44 | ||
| D2 | Grant after examination | ||
| 8363 | Opposition against the patent | ||
| 8331 | Complete revocation |