DE19781988T1 - Verfahren zur Herstellung von Methacrylsäureestern oder Acrylsäureestern - Google Patents

Verfahren zur Herstellung von Methacrylsäureestern oder Acrylsäureestern

Info

Publication number
DE19781988T1
DE19781988T1 DE19781988T DE19781988T DE19781988T1 DE 19781988 T1 DE19781988 T1 DE 19781988T1 DE 19781988 T DE19781988 T DE 19781988T DE 19781988 T DE19781988 T DE 19781988T DE 19781988 T1 DE19781988 T1 DE 19781988T1
Authority
DE
Germany
Prior art keywords
acid esters
preparation
acrylic acid
methacrylic acid
methacrylic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
DE19781988T
Other languages
English (en)
Other versions
DE19781988B4 (de
Inventor
Tatsuo Yamaguchi
Hiroshige Okamoto
Kiyoshi Asamura
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Asahi Kasei Corp
Asahi Chemical Industry Co Ltd
Original Assignee
Asahi Chemical Industry Co Ltd
Asahi Kasei Kogyo KK
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Asahi Chemical Industry Co Ltd, Asahi Kasei Kogyo KK filed Critical Asahi Chemical Industry Co Ltd
Publication of DE19781988T1 publication Critical patent/DE19781988T1/de
Pending legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/36—Pervaporation; Membrane distillation; Liquid permeation
    • B01D61/362—Pervaporation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/52—Esters of acyclic unsaturated carboxylic acids having the esterified carboxyl group bound to an acyclic carbon atom
    • C07C69/533—Monocarboxylic acid esters having only one carbon-to-carbon double bond
    • C07C69/54—Acrylic acid esters; Methacrylic acid esters
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1893—Membrane reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/005—Separating solid material from the gas/liquid stream
    • B01J8/006—Separating solid material from the gas/liquid stream by filtration
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/39—Preparation of carboxylic acid esters by oxidation of groups which are precursors for the acid moiety of the ester
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094—Jackets

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Water Supply & Treatment (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DE19781988T 1996-09-10 1997-09-09 Verfahren zur Herstellung von Methacrylsäureestern oder Acrylsäureestern Pending DE19781988T1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP23886396 1996-09-10
PCT/JP1997/003173 WO1998011050A1 (fr) 1996-09-10 1997-09-09 Procede de preparation d'esters methacryliques ou acryliques

Publications (1)

Publication Number Publication Date
DE19781988T1 true DE19781988T1 (de) 1999-08-12

Family

ID=17036388

Family Applications (2)

Application Number Title Priority Date Filing Date
DE19781988A Expired - Fee Related DE19781988B4 (de) 1996-09-10 1997-09-09 Verfahren zur Herstellung von Methacrylsäureestern oder Acrylsäureestern
DE19781988T Pending DE19781988T1 (de) 1996-09-10 1997-09-09 Verfahren zur Herstellung von Methacrylsäureestern oder Acrylsäureestern

Family Applications Before (1)

Application Number Title Priority Date Filing Date
DE19781988A Expired - Fee Related DE19781988B4 (de) 1996-09-10 1997-09-09 Verfahren zur Herstellung von Methacrylsäureestern oder Acrylsäureestern

Country Status (8)

Country Link
US (1) US6107515A (de)
JP (1) JP4057063B2 (de)
KR (1) KR100288998B1 (de)
CN (1) CN1087014C (de)
AU (1) AU4137097A (de)
DE (2) DE19781988B4 (de)
TW (1) TW385304B (de)
WO (1) WO1998011050A1 (de)

Families Citing this family (32)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4860065B2 (ja) * 2001-08-03 2012-01-25 旭化成ケミカルズ株式会社 反応器への重合禁止剤と鉛の供給方法
CN1305835C (zh) * 2005-04-12 2007-03-21 天津市天骄化工有限公司 多元醇丙烯酸酯的制备方法
JP2006315991A (ja) * 2005-05-12 2006-11-24 Yamaguchi Univ エステルの製造方法
CA2632998C (en) 2006-06-28 2011-02-08 Sakai Chemical Industry Co., Ltd. Polycondensation catalyst for producing polyester and method for producing polyester using the same
KR101477491B1 (ko) * 2006-09-15 2014-12-31 알케마 인코포레이티드 아크릴산의 제조방법
EP1994978A1 (de) * 2007-05-25 2008-11-26 Evonik Röhm GmbH Verfahren zur Herstellung von Methylmethacrylat durch Veresterung während der Oxidation
CN101148406B (zh) * 2007-11-02 2011-04-20 中国科学院过程工程研究所 一种以醛、醇和氧化剂为原料制备羧酸酯的新方法
JP2012214387A (ja) * 2011-03-31 2012-11-08 National Institute Of Advanced Industrial Science & Technology エステルの製造方法
JP2013056879A (ja) * 2011-06-20 2013-03-28 Sumitomo Chemical Co Ltd カルボン酸エステルの製造方法
US8865950B2 (en) * 2011-08-10 2014-10-21 Saudi Arabian Oil Company Olefin hydration process with an integrated membrane reactor
FR2980475B1 (fr) * 2011-09-27 2013-08-30 Arkema France Procede de production d'esters acryliques
JP2013144663A (ja) * 2011-12-14 2013-07-25 Sumitomo Chemical Co Ltd メチオニンの製造方法
CN108164417B (zh) 2013-04-19 2021-07-06 罗姆化学有限责任公司 制备甲基丙烯酸甲酯的方法
TW201509522A (zh) 2013-07-29 2015-03-16 Rohm & Haas 氧化酯化催化劑
TW201509901A (zh) 2013-07-29 2015-03-16 Rohm & Haas 氧化酯化方法
TW201512168A (zh) * 2013-07-29 2015-04-01 Rohm & Haas 氧化酯化方法
US9487469B2 (en) * 2013-08-09 2016-11-08 Gas Technology Institute Process for purification of methyl methacrylate using molecular sieve membranes
CN105683142B (zh) 2013-10-28 2018-11-13 罗门哈斯公司 用于分离甲基丙烯醛的方法
MX2017004880A (es) 2014-10-31 2017-07-05 Rohm & Haas Proceso de esterificacion oxidativa para elaboracion de metacrilato de metilo.
KR102428000B1 (ko) * 2014-10-31 2022-08-02 다우 글로벌 테크놀로지스 엘엘씨 커플링된 반응기-증류 시스템을 이용한 산화적 에스테르화 반응으로부터의 동일계내 물 제거 방법
CN107074729B (zh) 2014-10-31 2020-08-04 陶氏环球技术有限责任公司 分离方法
TW201627267A (zh) * 2014-10-31 2016-08-01 陶氏全球科技公司 用於從氧化性酯化反應中原位水移除的方法使用經耦合的反應器－蒸餾系統
US10144698B2 (en) 2014-10-31 2018-12-04 Dow Global Technologies Llc Breaking a methanol/methyl methacrylate azeotrope using pressure swing distillation
FR3048697B1 (fr) 2016-03-10 2019-09-27 Arkema France Procede de production d'esters (meth)acryliques
CN105944641A (zh) * 2016-05-30 2016-09-21 浙江凯色丽科技发展有限公司 恒定固液比云母包覆装置
US10836698B2 (en) 2017-05-25 2020-11-17 Rohm And Haas Company Process for preparing methacrolein
CA3064431A1 (en) 2017-05-25 2018-11-29 Rohm And Haas Company Process for preparing methacrolein
EP3658533B1 (de) 2017-07-28 2024-03-20 Dow Global Technologies LLC Verfahren zur herstellung von methylmethacrylat durch oxidative veresterung unter verwendung eines heterogenen katalysators
BR112020001603A2 (pt) 2017-07-28 2020-07-21 Rohm And Haas Company método para preparar metil metacrilato de metacroleína e metanol.
JP7268007B2 (ja) * 2017-09-19 2023-05-02 ダウ グローバル テクノロジーズ エルエルシー 不均一触媒を使用する酸化的エステル化によるメタクリル酸メチルを生成するための方法
CN111744435B (zh) * 2020-07-06 2022-04-01 浙江汇翔新材料科技股份有限公司 一种羟化物的酯化工艺
CN112452341B (zh) * 2020-11-24 2022-08-26 上海华谊（集团）公司 负载型金镍催化剂及其制备方法

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS521930A (en) * 1975-06-24 1977-01-08 Katetsukusu Kk Method of constructing covered pavement body
JPS58198442A (ja) * 1982-05-14 1983-11-18 Asahi Chem Ind Co Ltd メタクリル酸メチル又はアクリル酸メチルの改良製造方法
DE3333653C1 (de) * 1983-09-17 1985-03-14 Danfoss A/S, Nordborg Elektronische Schaltvorrichtung
JPH02730A (ja) * 1988-01-29 1990-01-05 Nippon Seirou Kk エステルの製造方法
US5152898A (en) * 1989-10-23 1992-10-06 Texaco Inc. Separation of organic oxygenates
JPH0478626A (ja) * 1990-07-13 1992-03-12 Morisawa & Co Ltd 自動車の停車時間計測表示装置
US5248427A (en) * 1990-09-15 1993-09-28 Basf Aktiengesellschaft Removal of water from mixtures with alcohols and/or carboxylic acids and/or carboxylic esters
DE4029349A1 (de) * 1990-09-15 1992-03-19 Basf Ag Verfahren zur abtrennung von wasser aus einem wasser und alkohole und/oder carbonsaeuren und/oder cabonsaeureester enthaltenden gemisch
JPH05201930A (ja) * 1992-01-24 1993-08-10 Daicel Chem Ind Ltd ジアルキルカーボネートの製造法

Also Published As

Publication number Publication date
WO1998011050A1 (fr) 1998-03-19
DE19781988B4 (de) 2004-09-16
JP4057063B2 (ja) 2008-03-05
AU4137097A (en) 1998-04-02
KR20000035985A (ko) 2000-06-26
US6107515A (en) 2000-08-22
TW385304B (en) 2000-03-21
CN1087014C (zh) 2002-07-03
CN1230169A (zh) 1999-09-29
KR100288998B1 (ko) 2001-04-16

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