DE1520061A1 - Verfahren zur Herstellung von haertbaren Polyesterimidharzen - Google Patents
Verfahren zur Herstellung von haertbaren PolyesterimidharzenInfo
- Publication number
- DE1520061A1 DE1520061A1 DE19621520061 DE1520061A DE1520061A1 DE 1520061 A1 DE1520061 A1 DE 1520061A1 DE 19621520061 DE19621520061 DE 19621520061 DE 1520061 A DE1520061 A DE 1520061A DE 1520061 A1 DE1520061 A1 DE 1520061A1
- Authority
- DE
- Germany
- Prior art keywords
- equivalents
- bifunctional
- alcohols
- acids
- polyfunctional
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
- 229920005989 resin Polymers 0.000 title claims description 14
- 239000011347 resin Substances 0.000 title claims description 14
- 238000000034 method Methods 0.000 title claims description 9
- 238000004519 manufacturing process Methods 0.000 title claims description 8
- 229920003055 poly(ester-imide) Polymers 0.000 title claims description 4
- 239000002253 acid Substances 0.000 claims description 9
- 230000001588 bifunctional effect Effects 0.000 claims description 9
- 150000001298 alcohols Chemical class 0.000 claims description 8
- RLSSMJSEOOYNOY-UHFFFAOYSA-N m-cresol Chemical compound CC1=CC=CC(O)=C1 RLSSMJSEOOYNOY-UHFFFAOYSA-N 0.000 claims description 8
- 150000007513 acids Chemical class 0.000 claims description 6
- -1 aromatic carboxylic acids Chemical class 0.000 claims description 6
- 239000002904 solvent Substances 0.000 claims description 4
- 125000003118 aryl group Chemical group 0.000 claims description 2
- 150000004985 diamines Chemical class 0.000 claims description 2
- 150000001875 compounds Chemical class 0.000 claims 3
- 150000001414 amino alcohols Chemical class 0.000 claims 2
- 239000000470 constituent Substances 0.000 claims 2
- 238000010438 heat treatment Methods 0.000 claims 2
- 150000004653 carbonic acids Chemical class 0.000 claims 1
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 26
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 10
- SRPWOOOHEPICQU-UHFFFAOYSA-N trimellitic anhydride Chemical compound OC(=O)C1=CC=C2C(=O)OC(=O)C2=C1 SRPWOOOHEPICQU-UHFFFAOYSA-N 0.000 description 10
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 description 8
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 7
- 238000006243 chemical reaction Methods 0.000 description 6
- 235000011187 glycerol Nutrition 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- 150000008064 anhydrides Chemical class 0.000 description 4
- 238000009833 condensation Methods 0.000 description 4
- WOZVHXUHUFLZGK-UHFFFAOYSA-N dimethyl terephthalate Chemical compound COC(=O)C1=CC=C(C(=O)OC)C=C1 WOZVHXUHUFLZGK-UHFFFAOYSA-N 0.000 description 4
- 229920000768 polyamine Polymers 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 230000005494 condensation Effects 0.000 description 3
- CYIDZMCFTVVTJO-UHFFFAOYSA-N pyromellitic acid Chemical class OC(=O)C1=CC(C(O)=O)=C(C(O)=O)C=C1C(O)=O CYIDZMCFTVVTJO-UHFFFAOYSA-N 0.000 description 3
- 239000011541 reaction mixture Substances 0.000 description 3
- QTWJRLJHJPIABL-UHFFFAOYSA-N 2-methylphenol;3-methylphenol;4-methylphenol Chemical compound CC1=CC=C(O)C=C1.CC1=CC=CC(O)=C1.CC1=CC=CC=C1O QTWJRLJHJPIABL-UHFFFAOYSA-N 0.000 description 2
- 239000004642 Polyimide Substances 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 229930003836 cresol Natural products 0.000 description 2
- 230000032050 esterification Effects 0.000 description 2
- 238000005886 esterification reaction Methods 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 238000005187 foaming Methods 0.000 description 2
- 150000003949 imides Chemical class 0.000 description 2
- 239000000155 melt Substances 0.000 description 2
- 229920005575 poly(amic acid) Polymers 0.000 description 2
- 229920001721 polyimide Polymers 0.000 description 2
- 239000002243 precursor Substances 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- LYCAIKOWRPUZTN-NMQOAUCRSA-N 1,2-dideuteriooxyethane Chemical compound [2H]OCCO[2H] LYCAIKOWRPUZTN-NMQOAUCRSA-N 0.000 description 1
- VLDPXPPHXDGHEW-UHFFFAOYSA-N 1-chloro-2-dichlorophosphoryloxybenzene Chemical compound ClC1=CC=CC=C1OP(Cl)(Cl)=O VLDPXPPHXDGHEW-UHFFFAOYSA-N 0.000 description 1
- CDAWCLOXVUBKRW-UHFFFAOYSA-N 2-aminophenol Chemical class NC1=CC=CC=C1O CDAWCLOXVUBKRW-UHFFFAOYSA-N 0.000 description 1
- YBRVSVVVWCFQMG-UHFFFAOYSA-N 4,4'-diaminodiphenylmethane Chemical compound C1=CC(N)=CC=C1CC1=CC=C(N)C=C1 YBRVSVVVWCFQMG-UHFFFAOYSA-N 0.000 description 1
- 241000239290 Araneae Species 0.000 description 1
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
- 208000004350 Strabismus Diseases 0.000 description 1
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 description 1
- LEHOTFFKMJEONL-UHFFFAOYSA-N Uric Acid Chemical compound N1C(=O)NC(=O)C2=C1NC(=O)N2 LEHOTFFKMJEONL-UHFFFAOYSA-N 0.000 description 1
- 150000008065 acid anhydrides Chemical class 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 125000005907 alkyl ester group Chemical group 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 125000003277 amino group Chemical group 0.000 description 1
- 210000000481 breast Anatomy 0.000 description 1
- 150000001718 carbodiimides Chemical class 0.000 description 1
- 125000002843 carboxylic acid group Chemical group 0.000 description 1
- 150000001735 carboxylic acids Chemical class 0.000 description 1
- DERZBLKQOCDDDZ-JLHYYAGUSA-N cinnarizine Chemical compound C1CN(C(C=2C=CC=CC=2)C=2C=CC=CC=2)CCN1C\C=C\C1=CC=CC=C1 DERZBLKQOCDDDZ-JLHYYAGUSA-N 0.000 description 1
- 238000003776 cleavage reaction Methods 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- CZZYITDELCSZES-UHFFFAOYSA-N diphenylmethane Chemical compound C=1C=CC=CC=1CC1=CC=CC=C1 CZZYITDELCSZES-UHFFFAOYSA-N 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 150000002169 ethanolamines Chemical class 0.000 description 1
- 125000000524 functional group Chemical group 0.000 description 1
- 150000004678 hydrides Chemical class 0.000 description 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- OJURWUUOVGOHJZ-UHFFFAOYSA-N methyl 2-[(2-acetyloxyphenyl)methyl-[2-[(2-acetyloxyphenyl)methyl-(2-methoxy-2-oxoethyl)amino]ethyl]amino]acetate Chemical compound C=1C=CC=C(OC(C)=O)C=1CN(CC(=O)OC)CCN(CC(=O)OC)CC1=CC=CC=C1OC(C)=O OJURWUUOVGOHJZ-UHFFFAOYSA-N 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 239000002798 polar solvent Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000012066 reaction slurry Substances 0.000 description 1
- 230000007017 scission Effects 0.000 description 1
- 235000017281 sodium acetate Nutrition 0.000 description 1
- 239000001632 sodium acetate Substances 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- KKEYFWRCBNTPAC-UHFFFAOYSA-L terephthalate(2-) Chemical compound [O-]C(=O)C1=CC=C(C([O-])=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-L 0.000 description 1
- ARCGXLSVLAOJQL-UHFFFAOYSA-N trimellitic acid Chemical class OC(=O)C1=CC=C(C(O)=O)C(C(O)=O)=C1 ARCGXLSVLAOJQL-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/68—Polyesters containing atoms other than carbon, hydrogen and oxygen
- C08G63/685—Polyesters containing atoms other than carbon, hydrogen and oxygen containing nitrogen
- C08G63/6854—Polyesters containing atoms other than carbon, hydrogen and oxygen containing nitrogen derived from polycarboxylic acids and polyhydroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
- C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
- C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
- C08G73/16—Polyester-imides
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B3/00—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
- H01B3/18—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances
- H01B3/30—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes
- H01B3/303—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups H01B3/38 or H01B3/302
- H01B3/306—Polyimides or polyesterimides
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B3/00—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
- H01B3/18—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances
- H01B3/30—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes
- H01B3/42—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes polyesters; polyethers; polyacetals
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B3/00—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
- H01B3/18—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances
- H01B3/30—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes
- H01B3/42—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes polyesters; polyethers; polyacetals
- H01B3/421—Polyesters
Landscapes
- Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
- Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEH0047121 | 1962-10-11 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1520061A1 true DE1520061A1 (de) | 1969-07-17 |
Family
ID=7156330
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19621520061 Ceased DE1520061A1 (de) | 1962-10-11 | 1962-10-11 | Verfahren zur Herstellung von haertbaren Polyesterimidharzen |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US3382203A (en, 2012) |
| AT (1) | AT242957B (en, 2012) |
| CH (1) | CH450718A (en, 2012) |
| DE (1) | DE1520061A1 (en, 2012) |
| DK (1) | DK109795C (en, 2012) |
| FI (1) | FI42380B (en, 2012) |
| GB (1) | GB1067541A (en, 2012) |
| NL (3) | NL145871B (en, 2012) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1494457A1 (de) * | 1965-06-01 | 1969-12-11 | Herberts & Co Gmbh Dr Kurt | Verfahren zur Herstellung von isolierenden UEberzuegen auf elektrischen Leitern |
| US3853817A (en) * | 1971-06-17 | 1974-12-10 | Gen Electric | Tin containing esterimide polymer resins and method of forming |
Families Citing this family (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3929714A (en) * | 1961-11-02 | 1975-12-30 | Karl Schmidt | Polyester resins |
| US4145334A (en) * | 1961-11-02 | 1979-03-20 | Dr. Beck & Co., A.G. | Polyester imide resins |
| US3852246A (en) * | 1964-06-09 | 1974-12-03 | Beck & Co Gmbh | Polyesterimide resins |
| FR1596487A (en, 2012) * | 1967-07-05 | 1970-06-22 | ||
| PL72684B1 (en, 2012) * | 1969-07-23 | 1974-08-30 | Dr Kurt Herberts & Covorm Otto Louis Herberts | |
| US3833411A (en) * | 1971-10-18 | 1974-09-03 | Bell Telephone Labor Inc | Articles coated with alkali-soluble polyester-type resins and method of producing them |
| US3922252A (en) * | 1972-06-23 | 1975-11-25 | Gen Electric | Polyamideimide compositions |
| US4038254A (en) * | 1973-03-01 | 1977-07-26 | Dynamit Nobel Aktiengesellschaft | Process for the manufacture of wire insulation varnish resins suitable chiefly for application in the melted state |
| US3994863A (en) * | 1974-03-15 | 1976-11-30 | Basf Aktiengesellschaft | Process for the manufacture of polyester imides using melamine as the polyamine reactant |
| GB1559254A (en) * | 1976-04-20 | 1980-01-16 | Hitachi Chemical Co Ltd | Polyester and polyesterimide resins and insulating resins compositions prepared therefrom |
| US4119608A (en) * | 1977-02-22 | 1978-10-10 | Schenectady Chemicals, Inc. | Solutions of polyester-imides |
| US4269752A (en) * | 1979-05-18 | 1981-05-26 | General Electric Company | Polyester imide wire enamels |
| US4267231A (en) * | 1979-06-29 | 1981-05-12 | General Electric Company | Polyester imide wire enamels |
| US4305847A (en) * | 1979-07-26 | 1981-12-15 | Acheson Industries, Inc. | Copper coating composition for shielding electronic equipment and the like |
| US4382981A (en) * | 1979-07-26 | 1983-05-10 | Acheson Industries, Inc. | Method for shielding electronic equipment by coating with copper containing composition |
| US4273917A (en) * | 1979-12-04 | 1981-06-16 | General Electric Company | Acid-terminated polyester imide wire enamels |
| US4480007A (en) * | 1980-09-03 | 1984-10-30 | General Electric Company | Enamel having improved coatability and insulated electrical articles produced therefrom |
| US4485127A (en) * | 1980-09-03 | 1984-11-27 | General Electric Company | Enamel having improved coatability and insulated electrical articles produced therefrom |
| US4404331A (en) * | 1980-09-03 | 1983-09-13 | General Electric Company | Enamel having improved coatability and insulated electrical articles produced therefrom |
| US4873268A (en) * | 1984-02-22 | 1989-10-10 | Sloss Industries Corporation | Digestion products of polyalkylene terephthalate polymers and polycarboxylic acid-containing polyols and polymeric foams obtained therefrom |
| US4539341A (en) * | 1984-02-22 | 1985-09-03 | Jim Walter Resources, Inc. | Digestion products of polyalkylene terephthalate polymers and polycarboxylic acid-containing polyols and polymeric foams obtained therefrom |
| MX2022001715A (es) * | 2019-08-09 | 2022-03-11 | Huntsman Int Llc | Poliol de poliester que comprende una porcion de imida y metodos de fabricacion del mismo. |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB621977A (en) * | 1946-12-16 | 1949-04-25 | James Gordon Napier Drewitt | Improvements in the production of poly-ester-amides |
| US2917414A (en) * | 1955-11-21 | 1959-12-15 | Dow Corning | Electrical conductors coated with titanate-modified alkyd resins |
| US2856385A (en) * | 1956-05-10 | 1958-10-14 | Eastman Kodak Co | Polyester-amides of n,n'-bis-(p-carboxybenzoyl) alkylenediamines, glycols and diamines |
| US3053783A (en) * | 1958-09-19 | 1962-09-11 | Standard Oil Co | Water soluble polyesters of benzene polycarboxylic acids |
| US3179634A (en) * | 1962-01-26 | 1965-04-20 | Du Pont | Aromatic polyimides and the process for preparing them |
| US3238181A (en) * | 1960-11-03 | 1966-03-01 | Soto Chemical Coatings Inc De | Heat resistant polymers containing recurring cyclic imide groups connected by amide or ester linkages |
| US3211585A (en) * | 1961-06-16 | 1965-10-12 | Schenectady Chemical | Electric conductor coated with the reaction product of a dibasic polycarboxylic acid and tris(2-hydroxyethyl) isocyanurate together with an organic polyisocyanate or an alkyl titanate |
-
0
- NL NL299131D patent/NL299131A/xx unknown
-
1962
- 1962-10-11 DE DE19621520061 patent/DE1520061A1/de not_active Ceased
-
1963
- 1963-10-08 US US314636A patent/US3382203A/en not_active Expired - Lifetime
- 1963-10-10 CH CH1242263A patent/CH450718A/de unknown
- 1963-10-10 AT AT812863A patent/AT242957B/de active
- 1963-10-11 GB GB40250/63A patent/GB1067541A/en not_active Expired
- 1963-10-11 NL NL63299131A patent/NL145871B/xx not_active IP Right Cessation
- 1963-10-11 FI FI1973/63A patent/FI42380B/fi active
- 1963-10-11 DK DK480063AA patent/DK109795C/da active
-
1975
- 1975-04-03 NL NL7503965A patent/NL7503965A/xx unknown
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1494457A1 (de) * | 1965-06-01 | 1969-12-11 | Herberts & Co Gmbh Dr Kurt | Verfahren zur Herstellung von isolierenden UEberzuegen auf elektrischen Leitern |
| US3853817A (en) * | 1971-06-17 | 1974-12-10 | Gen Electric | Tin containing esterimide polymer resins and method of forming |
Also Published As
| Publication number | Publication date |
|---|---|
| NL299131A (en, 2012) | |
| NL7503965A (nl) | 1975-07-31 |
| AT242957B (de) | 1965-10-11 |
| NL145871B (nl) | 1975-05-15 |
| FI42380B (en, 2012) | 1970-03-31 |
| CH450718A (de) | 1968-01-31 |
| GB1067541A (en) | 1967-05-03 |
| US3382203A (en) | 1968-05-07 |
| DK109795C (da) | 1968-07-01 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| SH | Request for examination between 03.10.1968 and 22.04.1971 | ||
| OGA | New person/name/address of the applicant | ||
| 8131 | Rejection |