DE1289524B - Verfahren und Vorrichtung zur Herstellung einer waessrigen 0, 5- bis 7gewichtsprozentigen Peressigsaeureloesung - Google Patents

Verfahren und Vorrichtung zur Herstellung einer waessrigen 0, 5- bis 7gewichtsprozentigen Peressigsaeureloesung

Info

Publication number
DE1289524B
DE1289524B DEF47556A DEF0047556A DE1289524B DE 1289524 B DE1289524 B DE 1289524B DE F47556 A DEF47556 A DE F47556A DE F0047556 A DEF0047556 A DE F0047556A DE 1289524 B DE1289524 B DE 1289524B
Authority
DE
Germany
Prior art keywords
peracetic acid
hydrogen peroxide
reaction
acetic anhydride
reaction vessel
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
DEF47556A
Other languages
German (de)
English (en)
Inventor
Oringer Kenneth
Easton Bernard Kestner
Bunin Donald Sander
Gallagher Gerald Thomas
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
FMC Corp
Original Assignee
FMC Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by FMC Corp filed Critical FMC Corp
Publication of DE1289524B publication Critical patent/DE1289524B/de
Pending legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B01J19/243—Tubular reactors spirally, concentrically or zigzag wound
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J14/00—Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C407/00—Preparation of peroxy compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00054—Controlling or regulating the heat exchange system
    • B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00069—Flow rate measurement
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00099—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor the reactor being immersed in the heat exchange medium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00162—Controlling or regulating processes controlling the pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00164—Controlling or regulating processes controlling the flow
    • B01J2219/00166—Controlling or regulating processes controlling the flow controlling the residence time inside the reactor vessel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00177—Controlling or regulating processes controlling the pH

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
DEF47556A 1964-11-03 1965-10-29 Verfahren und Vorrichtung zur Herstellung einer waessrigen 0, 5- bis 7gewichtsprozentigen Peressigsaeureloesung Pending DE1289524B (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US40848664A 1964-11-03 1964-11-03

Publications (1)

Publication Number Publication Date
DE1289524B true DE1289524B (de) 1969-02-20

Family

ID=23616479

Family Applications (1)

Application Number Title Priority Date Filing Date
DEF47556A Pending DE1289524B (de) 1964-11-03 1965-10-29 Verfahren und Vorrichtung zur Herstellung einer waessrigen 0, 5- bis 7gewichtsprozentigen Peressigsaeureloesung

Country Status (10)

Country Link
US (1) US3432546A (enExample)
AT (1) AT265229B (enExample)
BE (1) BE671777A (enExample)
CH (1) CH471067A (enExample)
DE (1) DE1289524B (enExample)
ES (1) ES319142A1 (enExample)
FI (1) FI42711B (enExample)
GB (2) GB1117336A (enExample)
NL (1) NL6513939A (enExample)
SE (1) SE324758B (enExample)

Families Citing this family (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2462425A1 (fr) * 1979-08-01 1981-02-13 Air Liquide Procede de fabrication de solutions diluees stables de peracides carboxyliques aliphatiques
GB8628441D0 (en) * 1986-11-27 1986-12-31 Unilever Plc Disinfectant dilution
US5977403A (en) * 1997-08-04 1999-11-02 Fmc Corporation Method for the production of lower organic peracids
JP5305230B2 (ja) * 2006-10-18 2013-10-02 三菱瓦斯化学株式会社 モノ過硫酸の製造方法及びモノ過硫酸連続製造装置
AU2012201470B8 (en) * 2006-10-18 2013-10-31 Mitsubishi Gas Chemical Company, Inc. Method for producing peroxymonosulfuric acid and apparatus for continuously producing peroxymonosulfuric acid
WO2009023492A2 (en) * 2007-08-10 2009-02-19 Fmc Corporation Dilute stabilized peracetic acid production and treatment process
US8647510B2 (en) * 2007-12-28 2014-02-11 3M Innovative Properties Company Method of making zirconia-containing nanoparticles
US20100113692A1 (en) * 2008-11-04 2010-05-06 Mcguire Jr James E Apparatus for Continuous Production of Partially Polymerized Compositions
EP3357337B1 (en) * 2010-12-29 2025-10-22 Ecolab USA Inc. Generation of peroxycarboxylic acids at alkaline ph, and their use as textile bleaching and antimicrobial agents
US8889900B2 (en) * 2010-12-29 2014-11-18 Ecolab Usa Inc. Sugar ester peracid on site generator and formulator
US8877254B2 (en) 2010-12-29 2014-11-04 Ecolab Usa Inc. In situ generation of peroxycarboxylic acids at alkaline pH, and methods of use thereof
WO2012128734A1 (en) 2011-03-24 2012-09-27 Enviro Tech Chemical Services, Inc. Methods and compositions for the generation of peracetic acid on site at the point-of-use
US8546449B2 (en) 2011-03-24 2013-10-01 Enviro Tech Chemical Services, Inc. Methods and compositions for the generation of peracetic acid on site at the point-of-use
US9321664B2 (en) 2011-12-20 2016-04-26 Ecolab Usa Inc. Stable percarboxylic acid compositions and uses thereof
EP2831000A4 (en) 2012-03-30 2016-03-30 Ecolab Usa Inc USE OF PERCONDIC ACID / HYDROGEN PEROXIDE AND PEROXIDE REDUCERS FOR THE TREATMENT OF DRILLING LIQUIDS, FRACKING LIQUIDS, REFILL WATER AND DISPOSAL WATER
US8822719B1 (en) 2013-03-05 2014-09-02 Ecolab Usa Inc. Peroxycarboxylic acid compositions suitable for inline optical or conductivity monitoring
US10165774B2 (en) 2013-03-05 2019-01-01 Ecolab Usa Inc. Defoamer useful in a peracid composition with anionic surfactants
US20140256811A1 (en) 2013-03-05 2014-09-11 Ecolab Usa Inc. Efficient stabilizer in controlling self accelerated decomposition temperature of peroxycarboxylic acid compositions with mineral acids
CA2971416C (en) 2014-12-18 2024-01-23 Ecolab Usa Inc. Methods for forming peroxyformic acid and uses thereof
US11040902B2 (en) 2014-12-18 2021-06-22 Ecolab Usa Inc. Use of percarboxylic acids for scale prevention in treatment systems
MX2017008062A (es) 2014-12-18 2018-01-09 Ecolab Usa Inc Generacion de acido peroxiformico a traves de formiato de alcohol polihidrico.
CN105541688B (zh) * 2016-01-19 2018-03-09 黎明化工研究设计院有限责任公司 一种合成高浓度无水过氧乙酸溶液联产乙酰脲的方法
US9907305B2 (en) 2016-03-22 2018-03-06 Solvay Sa Production of disinfecting solutions
US10081784B2 (en) 2016-05-13 2018-09-25 Eltron Research & Development, LLC Process for the continuous on-site production of percarboxycilic acid solutions and device for its implementation
CA3033671A1 (en) * 2016-08-12 2018-02-15 Eltron Water Systems, LLC Systems and methods for the continuous on-site production of peroxycarboxcylic acid solutions
EP3806637A1 (en) 2018-06-15 2021-04-21 Ecolab USA Inc. On site generated performic acid compositions for teat treatment
WO2020041545A1 (en) 2018-08-22 2020-02-27 Ecolab Usa Inc. Hydrogen peroxide and peracid stabilization with molecules based on a pyridine carboxylic acid at c-3, -4 or -5
WO2021026410A1 (en) 2019-08-07 2021-02-11 Ecolab Usa Inc. Polymeric and solid-supported chelators for stabilization of peracid-containing compositions
CN111233728A (zh) * 2020-03-18 2020-06-05 中国天辰工程有限公司 一种快速制备高浓过氧乙酸的方法
CN111333559A (zh) * 2020-03-18 2020-06-26 中国天辰工程有限公司 一种连续流快速制备过氧乙酸的方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH230678A (de) * 1940-07-08 1944-01-31 Degussa Mittel zur Herstellung von Lösungen zum Bleichen von Baumwolle und Baumwollwaren.
AT203454B (de) * 1956-06-15 1959-05-25 Haemmerle Fa F M Verfahren zur sauren Peroxydbleiche von Textilfasern
DE1158956B (de) * 1957-11-25 1963-12-12 Degussa Verfahren zur Herstellung von Peressigsaeure bzw. deren Salze enthaltenden waessrigen Bleichloesungen

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2314385A (en) * 1940-02-21 1943-03-23 Celanese Corp Preparation of aliphatic peracids by oxidation of aldehydes
US2377038A (en) * 1941-09-15 1945-05-29 Du Pont Manufacture of peracids
FR1183067A (fr) * 1956-07-31 1959-07-02 Union Carbide Corp Procédé de fabrication de peracides
NL289739A (enExample) * 1962-03-08

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH230678A (de) * 1940-07-08 1944-01-31 Degussa Mittel zur Herstellung von Lösungen zum Bleichen von Baumwolle und Baumwollwaren.
AT203454B (de) * 1956-06-15 1959-05-25 Haemmerle Fa F M Verfahren zur sauren Peroxydbleiche von Textilfasern
DE1158956B (de) * 1957-11-25 1963-12-12 Degussa Verfahren zur Herstellung von Peressigsaeure bzw. deren Salze enthaltenden waessrigen Bleichloesungen

Also Published As

Publication number Publication date
FI42711B (enExample) 1970-06-30
ES319142A1 (es) 1966-08-01
NL6513939A (enExample) 1966-05-04
CH471067A (de) 1969-05-30
GB1117337A (en) 1968-06-19
SE324758B (enExample) 1970-06-15
BE671777A (enExample) 1966-03-01
AT265229B (de) 1968-10-10
GB1117336A (en) 1968-06-19
US3432546A (en) 1969-03-11

Similar Documents

Publication Publication Date Title
DE1289524B (de) Verfahren und Vorrichtung zur Herstellung einer waessrigen 0, 5- bis 7gewichtsprozentigen Peressigsaeureloesung
DE69123753T2 (de) Peroxosäureherstellung
DE69218657T2 (de) Verfahren und Vorrichtung zum Erzeugen von Peroxysäuren
DE2622608B2 (de) Verfahren zur Herstellung von kolloidalem Antimonpentoxid
EP0235841A1 (de) Verfahren zur Herstellung von Kupferhydroxid
DE60005631T2 (de) Verfahren zur herstellung wässeriger lösungen von ungesättigten quartären ammoniumsalzen
DE1518419C3 (de) Verfahren zur kontinuierlichen Herstellung von Cholinchlorid
DE2454910A1 (de) Verfahren und vorrichtung zum herstellen von loesungen oder suspensionen von cyanurchlorid in wasserhaltigen organischen loesungsmitteln
DE2141756A1 (de) Verfahren zur Herstellung von Chlorisocyanursäuren
DE3833230A1 (de) Verfahren zum loesen hochschmelzender erzeugnisse in tiefsiedenden fluessigkeiten als loesungsmittel, insbesondere mit simultaner bleiche
DE3202292C2 (de) Verfahren zur kontinuierlichen Bildung eines Säurefluorids
AT368910B (de) Verfahren und vorrichtung zur kontinuierlichen fuehrung von insbesondere zwischen fluessigkeit-gas-phasen, fluessigkeit-fluessigkeits-phasen und innerhalb von fluessigkeitsphasen ablaufenden chemischen reaktionen
EP0012837A1 (de) Verfahren zur Herstellung von Ammoniumsulfamat
DE3850424T2 (de) Verfahren zur Herstellung von epsilon-Caprolactam.
DE3437717C2 (enExample)
CH617102A5 (en) Method and appliance for mixing liquids, especially of liquid reaction components.
DE1088939B (de) Verfahren zur Herstellung von Hydrazin
DE906096C (de) Verfahren zur Herstellung von Hexamethylentetramin
DE933749C (de) Verfahren zur kontinuierlichen Herstellung verduennter, waessriger Ammoniumcarbonatloesungen
DE2736943C2 (de) Verfahren zur kontinuierlichen Herstellung von Thioharnstoffdioxid
DE1908679C3 (de) Verfahren zur Herstellung von Cyclohexandion-(1,2)-Hemihydrat
AT219044B (de) Verfahren zur Herstellung von neuen organischen Perhydratverbindungen
DE1023030B (de) Verfahren zur Herstellung von Tetraaethylthiuramdisulfid
DE1940074A1 (de) AEthylendiamintetraessigsaeuresalze
AT209864B (de) Verfahren zur Herstellung von Kaliummonopersulfat (KHSO5)