DE1173242B - Verfahren zur Herstellung von waessrigen Dispersionen - Google Patents
Verfahren zur Herstellung von waessrigen DispersionenInfo
- Publication number
- DE1173242B DE1173242B DEF35873A DEF0035873A DE1173242B DE 1173242 B DE1173242 B DE 1173242B DE F35873 A DEF35873 A DE F35873A DE F0035873 A DEF0035873 A DE F0035873A DE 1173242 B DE1173242 B DE 1173242B
- Authority
- DE
- Germany
- Prior art keywords
- polymer
- percent
- solution
- polyacrylamide
- emulsifiers
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000006185 dispersion Substances 0.000 title claims description 27
- 238000000034 method Methods 0.000 title claims description 11
- 238000004519 manufacturing process Methods 0.000 title description 5
- 239000003995 emulsifying agent Substances 0.000 claims description 20
- 229920000642 polymer Polymers 0.000 claims description 20
- 229920002401 polyacrylamide Polymers 0.000 claims description 13
- 239000003795 chemical substances by application Substances 0.000 claims description 7
- 239000002245 particle Substances 0.000 claims description 7
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims description 5
- 239000005977 Ethylene Substances 0.000 claims description 5
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 claims description 5
- 239000002253 acid Substances 0.000 claims description 3
- 150000007513 acids Chemical class 0.000 claims description 3
- 125000000217 alkyl group Chemical group 0.000 claims description 3
- 125000004432 carbon atom Chemical group C* 0.000 claims description 3
- 239000000084 colloidal system Substances 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 claims description 3
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 claims description 3
- 230000001681 protective effect Effects 0.000 claims description 3
- 125000001453 quaternary ammonium group Chemical group 0.000 claims description 3
- 150000003839 salts Chemical class 0.000 claims description 3
- 150000003512 tertiary amines Chemical class 0.000 claims description 3
- 150000001412 amines Chemical class 0.000 claims description 2
- 229920001577 copolymer Polymers 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims description 2
- 239000004711 α-olefin Substances 0.000 claims description 2
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 21
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 18
- 239000000243 solution Substances 0.000 description 15
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 9
- 229920000126 latex Polymers 0.000 description 8
- 239000004816 latex Substances 0.000 description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- 235000011054 acetic acid Nutrition 0.000 description 6
- 239000007864 aqueous solution Substances 0.000 description 6
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 5
- 239000007859 condensation product Substances 0.000 description 5
- 239000008346 aqueous phase Substances 0.000 description 4
- 125000002091 cationic group Chemical group 0.000 description 4
- NNBZCPXTIHJBJL-UHFFFAOYSA-N decalin Chemical compound C1CCCC2CCCCC21 NNBZCPXTIHJBJL-UHFFFAOYSA-N 0.000 description 4
- 238000000926 separation method Methods 0.000 description 4
- 210000002966 serum Anatomy 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000003960 organic solvent Substances 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- QGLWBTPVKHMVHM-KTKRTIGZSA-N (z)-octadec-9-en-1-amine Chemical compound CCCCCCCC\C=C/CCCCCCCCN QGLWBTPVKHMVHM-KTKRTIGZSA-N 0.000 description 2
- REYJJPSVUYRZGE-UHFFFAOYSA-N Octadecylamine Chemical compound CCCCCCCCCCCCCCCCCCN REYJJPSVUYRZGE-UHFFFAOYSA-N 0.000 description 2
- 239000002585 base Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000005345 coagulation Methods 0.000 description 2
- 230000015271 coagulation Effects 0.000 description 2
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 description 2
- 239000004815 dispersion polymer Substances 0.000 description 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 1
- FHVDTGUDJYJELY-UHFFFAOYSA-N 6-{[2-carboxy-4,5-dihydroxy-6-(phosphanyloxy)oxan-3-yl]oxy}-4,5-dihydroxy-3-phosphanyloxane-2-carboxylic acid Chemical compound O1C(C(O)=O)C(P)C(O)C(O)C1OC1C(C(O)=O)OC(OP)C(O)C1O FHVDTGUDJYJELY-UHFFFAOYSA-N 0.000 description 1
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 description 1
- 241000270730 Alligator mississippiensis Species 0.000 description 1
- 108091030071 RNAI Proteins 0.000 description 1
- DHKHKXVYLBGOIT-UHFFFAOYSA-N acetaldehyde Diethyl Acetal Natural products CCOC(C)OCC DHKHKXVYLBGOIT-UHFFFAOYSA-N 0.000 description 1
- 150000001241 acetals Chemical class 0.000 description 1
- VJHCJDRQFCCTHL-UHFFFAOYSA-N acetic acid 2,3,4,5,6-pentahydroxyhexanal Chemical compound CC(O)=O.OCC(O)C(O)C(O)C(O)C=O VJHCJDRQFCCTHL-UHFFFAOYSA-N 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 229940072056 alginate Drugs 0.000 description 1
- 229920000615 alginic acid Polymers 0.000 description 1
- 235000010443 alginic acid Nutrition 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 235000011114 ammonium hydroxide Nutrition 0.000 description 1
- 125000000129 anionic group Chemical group 0.000 description 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
- 239000004327 boric acid Substances 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 150000008280 chlorinated hydrocarbons Chemical class 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000007720 emulsion polymerization reaction Methods 0.000 description 1
- 239000005038 ethylene vinyl acetate Substances 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 235000019253 formic acid Nutrition 0.000 description 1
- 238000009432 framing Methods 0.000 description 1
- 238000010528 free radical solution polymerization reaction Methods 0.000 description 1
- 239000003502 gasoline Substances 0.000 description 1
- 238000003197 gene knockdown Methods 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 229920001200 poly(ethylene-vinyl acetate) Polymers 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 235000019260 propionic acid Nutrition 0.000 description 1
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 238000009988 textile finishing Methods 0.000 description 1
- 210000001215 vagina Anatomy 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
- C08J3/03—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media
- C08J3/07—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media from polymer solutions
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2323/00—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers
- C08J2323/02—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers not modified by chemical after treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Colloid Chemistry (AREA)
Priority Applications (8)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BE627665D BE627665A (en:Method) | 1962-01-27 | ||
| DEF35873A DE1173242B (de) | 1962-01-27 | 1962-01-27 | Verfahren zur Herstellung von waessrigen Dispersionen |
| US253274A US3294728A (en) | 1962-01-27 | 1963-01-23 | Process for preparing dispersions of olefin polymers containing positively charged particles with tertiary or quaternary ammonium ethoxylated fatty amines |
| AT59263A AT243502B (de) | 1962-01-27 | 1963-01-25 | Verfahren zur Herstellung von wässerigen Dispersionen mit positiv geladenen Teilchen |
| SE827/63A SE303603B (en:Method) | 1962-01-27 | 1963-01-25 | |
| CH92763A CH439718A (de) | 1962-01-27 | 1963-01-25 | Verfahren zur Herstellung von wässrigen Dispersionen |
| GB3509/63A GB1001948A (en) | 1962-01-27 | 1963-01-28 | Process for the preparation of dispersions of olefine homo-and copolymers containingpositively charged polymer particles, and dispersions prepared by this process |
| FR922821A FR1346005A (fr) | 1962-01-27 | 1963-01-28 | Dispersions d'homopolymères ou de copolymères d'oléfines et leur préparation |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEF35873A DE1173242B (de) | 1962-01-27 | 1962-01-27 | Verfahren zur Herstellung von waessrigen Dispersionen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1173242B true DE1173242B (de) | 1964-07-02 |
Family
ID=7096196
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEF35873A Pending DE1173242B (de) | 1962-01-27 | 1962-01-27 | Verfahren zur Herstellung von waessrigen Dispersionen |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US3294728A (en:Method) |
| AT (1) | AT243502B (en:Method) |
| BE (1) | BE627665A (en:Method) |
| CH (1) | CH439718A (en:Method) |
| DE (1) | DE1173242B (en:Method) |
| GB (1) | GB1001948A (en:Method) |
| SE (1) | SE303603B (en:Method) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AT332351B (de) * | 1970-06-30 | 1976-09-27 | Pfersee Chem Fab | Verfahren zur herstellung von emulsionen von organopolysiloxanen, die an silicium gebundene wasserstoffatome enthalten |
| US3819548A (en) * | 1971-12-03 | 1974-06-25 | Basf Ag | An electrocoating composition containing an acid binder present as the salt of an arylamine, alkynyl amine, quaternary ammonium hydroxide or phosphonium hydroxide |
| US4102841A (en) * | 1975-11-28 | 1978-07-25 | The B. F. Goodrich Company | Heat sensitive latices |
| DE3337640A1 (de) * | 1983-10-17 | 1985-04-25 | Henkel KGaA, 4000 Düsseldorf | Verwendung von oberflaechenaktiven tertiaeren alkylaminen als polymerisationsemulgatoren |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE862513C (de) * | 1949-09-28 | 1953-01-12 | Ici Ltd | Verfahren zur Herstellung von waessrigen Polyaethylendispersionen |
| US2892732A (en) * | 1956-06-28 | 1959-06-30 | Louis B Rockland | Aerated solid wax composition and process of making it |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB460146A (en) * | 1935-07-16 | 1937-01-18 | Ig Farbenindustrie Ag | Improvements in the manufacture and production of quaternary ammonium compounds |
| NL50503C (en:Method) * | 1937-04-22 | |||
| US2803171A (en) * | 1953-08-26 | 1957-08-20 | Patent & Licensing Corp | Process for producing a water vapor impermeable board |
| CH427287A (de) * | 1956-12-08 | 1966-12-31 | Hoechst Ag | Verfahren zur Herstellung von wässrigen Dispersionen von Polyvinylestern oder Vinylester-Mischpolymerisaten |
-
0
- BE BE627665D patent/BE627665A/xx unknown
-
1962
- 1962-01-27 DE DEF35873A patent/DE1173242B/de active Pending
-
1963
- 1963-01-23 US US253274A patent/US3294728A/en not_active Expired - Lifetime
- 1963-01-25 CH CH92763A patent/CH439718A/de unknown
- 1963-01-25 AT AT59263A patent/AT243502B/de active
- 1963-01-25 SE SE827/63A patent/SE303603B/xx unknown
- 1963-01-28 GB GB3509/63A patent/GB1001948A/en not_active Expired
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE862513C (de) * | 1949-09-28 | 1953-01-12 | Ici Ltd | Verfahren zur Herstellung von waessrigen Polyaethylendispersionen |
| US2892732A (en) * | 1956-06-28 | 1959-06-30 | Louis B Rockland | Aerated solid wax composition and process of making it |
Also Published As
| Publication number | Publication date |
|---|---|
| US3294728A (en) | 1966-12-27 |
| SE303603B (en:Method) | 1968-09-02 |
| AT243502B (de) | 1965-11-10 |
| BE627665A (en:Method) | |
| CH439718A (de) | 1967-07-15 |
| GB1001948A (en) | 1965-08-18 |
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