DE1157392B - Verfahren zur Reinigung polymerisierter Aminocarbonsaeuren - Google Patents
Verfahren zur Reinigung polymerisierter AminocarbonsaeurenInfo
- Publication number
- DE1157392B DE1157392B DEB63759A DEB0063759A DE1157392B DE 1157392 B DE1157392 B DE 1157392B DE B63759 A DEB63759 A DE B63759A DE B0063759 A DEB0063759 A DE B0063759A DE 1157392 B DE1157392 B DE 1157392B
- Authority
- DE
- Germany
- Prior art keywords
- washing
- polymerized
- aminocarboxylic acids
- washing treatment
- purification
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 8
- KXDHJXZQYSOELW-UHFFFAOYSA-N Carbamic acid Chemical class NC(O)=O KXDHJXZQYSOELW-UHFFFAOYSA-N 0.000 title claims description 4
- 238000000746 purification Methods 0.000 title claims 2
- 238000005406 washing Methods 0.000 claims description 36
- 239000004952 Polyamide Substances 0.000 claims description 18
- 239000007788 liquid Substances 0.000 claims description 18
- 229920002647 polyamide Polymers 0.000 claims description 18
- 238000011282 treatment Methods 0.000 claims description 17
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 16
- 239000011261 inert gas Substances 0.000 claims description 9
- 229910052757 nitrogen Inorganic materials 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 10
- 239000007789 gas Substances 0.000 description 4
- 230000003647 oxidation Effects 0.000 description 4
- 238000007254 oxidation reaction Methods 0.000 description 4
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- 239000001301 oxygen Substances 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 229920000642 polymer Polymers 0.000 description 3
- SLXKOJJOQWFEFD-UHFFFAOYSA-N 6-aminohexanoic acid Chemical compound NCCCCCC(O)=O SLXKOJJOQWFEFD-UHFFFAOYSA-N 0.000 description 2
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 2
- 229960002684 aminocaproic acid Drugs 0.000 description 2
- 238000007664 blowing Methods 0.000 description 2
- 239000003638 chemical reducing agent Substances 0.000 description 2
- 229910001873 dinitrogen Inorganic materials 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 238000005201 scrubbing Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- DWAQJAXMDSEUJJ-UHFFFAOYSA-M Sodium bisulfite Chemical compound [Na+].OS([O-])=O DWAQJAXMDSEUJJ-UHFFFAOYSA-M 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 230000002730 additional effect Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000013505 freshwater Substances 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 235000010267 sodium hydrogen sulphite Nutrition 0.000 description 1
- 238000004383 yellowing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/46—Post-polymerisation treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyamides (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL255216A NL255216A (en:Method) | 1960-08-24 | 1960-08-24 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1157392B true DE1157392B (de) | 1963-11-14 |
Family
ID=19752530
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEB63759A Pending DE1157392B (de) | 1960-08-24 | 1961-08-23 | Verfahren zur Reinigung polymerisierter Aminocarbonsaeuren |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US3149095A (en:Method) |
| BE (1) | BE607356A (en:Method) |
| CH (1) | CH392885A (en:Method) |
| DE (1) | DE1157392B (en:Method) |
| ES (1) | ES270061A1 (en:Method) |
| FR (1) | FR1298294A (en:Method) |
| GB (1) | GB942691A (en:Method) |
| NL (2) | NL255216A (en:Method) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4231288A1 (de) * | 1992-09-18 | 1994-03-24 | Chema Balcke Duerr Verfahrenst | Verfahren zur Verbesserung der Extraktion von Polyamidgranulat |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1398342A (fr) * | 1963-06-11 | 1965-05-07 | Asahi Chemical Ind | Perfectionnements apportés aux procédés pour la pulvérisation de polymères |
| US3335115A (en) * | 1963-09-11 | 1967-08-08 | Schwarza Chemiefaser | Method of removing monomeric components from polycaprolactam |
| US3627733A (en) * | 1964-06-10 | 1971-12-14 | Asahi Chemical Ind | Method for particularizing thermoplastic polyesters |
| US3374207A (en) * | 1964-11-12 | 1968-03-19 | Inventa Ag | Continuous process for the extraction of monomers and oligomers from highly polymerized caprolactam granules |
| US3373145A (en) * | 1965-04-29 | 1968-03-12 | Allied Chem | Washing of polymer particulates by regular periodic ebb and flow of aqueous solvent |
| US4145521A (en) * | 1977-05-23 | 1979-03-20 | Inventa Ag Fur Forschung Und Patentverwertung, Zurich | Method of discharging and metering solids in liquids |
| CN115449070B (zh) * | 2021-06-09 | 2024-02-23 | 上海凯赛生物技术股份有限公司 | 一种聚酰胺树脂及其制备方法、组合物、纤维制品 |
| CN116144019B (zh) * | 2021-11-19 | 2025-07-11 | 上海凯赛生物技术股份有限公司 | 一种聚酰胺树脂、组合物及其在工程塑料中的应用 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL181713B (nl) * | 1953-07-25 | Elf Aquitaine | Werkwijze voor de regeling van een kolom met atmosferische destillatie van ruwe aardolie. | |
| NL97197C (en:Method) * | 1953-12-31 | |||
| BE548810A (en:Method) * | 1955-07-23 | |||
| US3015651A (en) * | 1956-09-28 | 1962-01-02 | Du Pont | Increasing viscosity of polycaprolactam by removing extractables with solvents and further solid phase polymerizing the polymer |
| FR1188817A (fr) * | 1957-03-20 | 1959-09-25 | Bayer Ag | Procédé pour améliorer les polyamides par traitement de tournures de polyamide avec de l'eau contenant de l'hydrazine |
| BE567584A (en:Method) * | 1957-05-17 | |||
| US3047565A (en) * | 1958-11-20 | 1962-07-31 | Inventa Ag | Process for extraction of monomeric caprolactam from its polymer |
| FR1243538A (fr) * | 1959-09-24 | 1960-10-14 | Machine à laver la vaisselle et les objets fragiles |
-
0
- NL NL125467D patent/NL125467C/xx active
-
1960
- 1960-08-24 NL NL255216A patent/NL255216A/xx unknown
-
1961
- 1961-08-07 US US129570A patent/US3149095A/en not_active Expired - Lifetime
- 1961-08-21 BE BE607356A patent/BE607356A/nl unknown
- 1961-08-21 CH CH971261A patent/CH392885A/de unknown
- 1961-08-22 GB GB30294/61A patent/GB942691A/en not_active Expired
- 1961-08-23 DE DEB63759A patent/DE1157392B/de active Pending
- 1961-08-23 ES ES0270061A patent/ES270061A1/es not_active Expired
- 1961-08-24 FR FR871501A patent/FR1298294A/fr not_active Expired
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4231288A1 (de) * | 1992-09-18 | 1994-03-24 | Chema Balcke Duerr Verfahrenst | Verfahren zur Verbesserung der Extraktion von Polyamidgranulat |
| DE4231288C2 (de) * | 1992-09-18 | 1999-07-01 | Holger Dipl Ing Kleim | Verfahren zur Verbesserung der Extraktion von Polyamidgranulat |
Also Published As
| Publication number | Publication date |
|---|---|
| BE607356A (nl) | 1961-12-18 |
| GB942691A (en) | 1963-11-27 |
| NL255216A (en:Method) | |
| FR1298294A (fr) | 1962-07-06 |
| US3149095A (en) | 1964-09-15 |
| ES270061A1 (es) | 1962-01-01 |
| NL125467C (en:Method) | |
| CH392885A (de) | 1965-05-31 |
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